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Offlineskoeip
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how to seperate DMT and gramine
    #3436085 - 12/02/04 05:51 AM (12 years, 8 months ago)

is there anybody that knows how to extract dmt from phragmites australis/Phragmites communis whit out the gramine? ive been searching the net, but its realy hard to find info about how to get the gramine out of the DMT


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Offlinestefan
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Re: how to seperate DMT and gramine [Re: skoeip]
    #3436100 - 12/02/04 06:27 AM (12 years, 8 months ago)

hmm, I've never heard of gramine in dmt..?


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Invisiblefreakygurl
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Re: how to seperate DMT and gramine *DELETED* [Re: skoeip]
    #3436392 - 12/02/04 10:10 AM (12 years, 8 months ago)

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Offlinegnrm23
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Re: how to seperate DMT and gramine [Re: freakygurl]
    #3436935 - 12/02/04 01:05 PM (12 years, 8 months ago)

hmmm....

well, there's column chromatography --- just check out the Rf(s) for the various indolic compounds & pick a workable solvent pair...

& maybe playing with a/b phase extractions (& variable solubilities of several salts & solvents at different pH values...)

& then there's vacuum distillation (sublimation of DMT under reduced pressures...)(this might be "the easiest" method, 'cause i'm sure that dmt & gramine would sublime at different temps under 0.1 Torr, or 0.01 Torr...)

& i'm sure there's other possibilities (these just offa top o' me head...) - have you checked dmtworld? or any of the many references in books by ott, shulgin, mckenna (dennis), or cadwallater?
or articles in "the journals" (y'know, JNP, lloydia, j.chromatog. etc...)
(there was an excellent article on TLCs run on phalaris extraction - a shitload of alkaloids, resolved by rotating the TLC plate 90 deg. & changing solvent mix... cool beans, dude... & the TLC info would surely give the enterprising young experimenter some ideas as to how to set up chroma-columns...)


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Mushrooms, Mycology and Psychedelics >> The Psychedelic Experience

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