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Extracting DMT - cloudy naptha?
    #13340646 -

i'm following the stb tek exactly. this is after about 2 hours of freezing the naptha




should it be this cloudy? should i dump it all back into the base solution and let it settle more?


--------------------
ONE-EYED WANT
-------------------------
knock a hoe out this dimension, continue my ascension
-bhad bhabie
rip. todcasil, acid sloth, st1llnox, shLong, ModestMouse, vinsue, big worm (sketch), tim

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Re: Extracting DMT - cloudy naptha? [Re: Envix]
    #13340650 -

if it wasn't that cloudy going into the freezer, i'd say the dmt is crashing out, put it back in the icebox.

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Re: Extracting DMT - cloudy naptha? [Re: Kisper]
    #13340802 -

I'm not familiar with that tek but did you defat before converting to freebase?


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"I mean, it's like a koala bear crapped a rainbow in my brain!"
-Captain Murphy

"Quit being a bitch and pill me up"
-Dr. Quinn

"Smoke that bitch"
"I am not Stormy, I am He who smokes Bitches!"
-Stormy

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Re: Extracting DMT - cloudy naptha? [Re: Gainer]
    #13340809 -

Gainer said:
I'm not familiar with that tek but did you defat before converting to freebase?


There is no need to do that with STB


Envix did you use distilled water I had the exact same thing happen to me when I attempted the tek with well water it went all cloudy and the DMT never precipitated out of the solution even after four days.


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War against a foreign country only happens when the moneyed classes think they are going to profit from it.-George Orwell-

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Re: Extracting DMT - cloudy naptha? [Re: Enigma of Ankou]
    #13340839 -

yes i used distilled water


could that be an emulsion though?


--------------------
ONE-EYED WANT
-------------------------
knock a hoe out this dimension, continue my ascension
-bhad bhabie
rip. todcasil, acid sloth, st1llnox, shLong, ModestMouse, vinsue, big worm (sketch), tim

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Re: Extracting DMT - cloudy naptha? [Re: Envix]
    #13340898 -

when i tip it upside down with the cap on it looks like a layer of naptha is frozen, stuck to the bottom of the glass. or is that crystals? whatever it is it is very yellow


--------------------
ONE-EYED WANT
-------------------------
knock a hoe out this dimension, continue my ascension
-bhad bhabie
rip. todcasil, acid sloth, st1llnox, shLong, ModestMouse, vinsue, big worm (sketch), tim

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Re: Extracting DMT - cloudy naptha? [Re: Envix] * 1
    #13341072 -

Cloudy is good, it means there's DMT in there and it's crashing out of solution. If it stays cloudy that means either your freezer isn't cold enough or the solution isn't saturated enough. Easy fix to both those problems would be to evaporate half the solvent and turn your freezer down to lowest temp possible.


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Re: Extracting DMT - cloudy naptha? [Re: FractalDust]
    #13341280 -

I've done the stb tek and my naptha never looked like that.  Good cloudy means you can see wisps of white stuff (crystals) floating throughout clear naptha.  Sorry I don't have any advice, just letting you know that mine never looked like that at any point during my extractions.

Edited by abore (10/15/10 06:11 PM)

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Re: Extracting DMT - cloudy naptha? [Re: abore]
    #13341303 -

okaay now the naptha in the base solution has become so dark the color is barely distinguishable from the base solution. is this bad?

how do i know if an emulsion has formed?


--------------------
ONE-EYED WANT
-------------------------
knock a hoe out this dimension, continue my ascension
-bhad bhabie
rip. todcasil, acid sloth, st1llnox, shLong, ModestMouse, vinsue, big worm (sketch), tim

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Re: Extracting DMT - cloudy naptha? [Re: Envix]
    #13341318 -

The frozen layer is probably the water.  I read that chopsticks are good for stirring and breaking emulsions, I just started reading about this stuff but it looks like you got some material in there.  Was it clear clear when it was pulled?

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Re: Extracting DMT - cloudy naptha? [Re: Enlightenedwon]
    #13341323 -

when it was pulled it was kinda clear but pretty damn yellow. the naptha in the base solution isn't even yellow anymore now it's just a barley lighter color than the solution itself. almost black


--------------------
ONE-EYED WANT
-------------------------
knock a hoe out this dimension, continue my ascension
-bhad bhabie
rip. todcasil, acid sloth, st1llnox, shLong, ModestMouse, vinsue, big worm (sketch), tim

Edited by Envix (10/15/10 06:31 PM)

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Re: Extracting DMT - cloudy naptha? [Re: Envix]
    #13341354 -

Not 100% on the colors because lime was used for a base in my book but it sounds like an emulsion a lot of people break them with a hot water bath or vibration, when I saw pulls they were barely tinted yellow almost not even noticeable.

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Re: Extracting DMT - cloudy naptha? [Re: Enlightenedwon]
    #13341360 -

nothin wrong with yellow naphta. just dont pull anything that's brown or purple


--------------------
:minifo:] "This promise constitutes the heart of my Christian beliefs and my call to natural-scientific research: we will attain to knowledge of the universe through the spirit of truth, and thereby to understanding of our being one with the deepest, most comprehensive reality, God."
-Albert Hofmann

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Re: Extracting DMT - cloudy naptha? [Re: Doctor_Dick]
    #13341363 -

the naptha in the base solution is brown/purple :uhoh:

will that clear up when i dump the freezer naptha back in it?


--------------------
ONE-EYED WANT
-------------------------
knock a hoe out this dimension, continue my ascension
-bhad bhabie
rip. todcasil, acid sloth, st1llnox, shLong, ModestMouse, vinsue, big worm (sketch), tim

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Re: Extracting DMT - cloudy naptha? [Re: Envix]
    #13341368 -

i don't understand what you mean naphta in base solution. if you shake it and wait a few hours it should be completely seperated

oh never mind i see what your saying, yah i'm not sure, i guess just dump it in and see if it clears up or not.


--------------------
:minifo:] "This promise constitutes the heart of my Christian beliefs and my call to natural-scientific research: we will attain to knowledge of the universe through the spirit of truth, and thereby to understanding of our being one with the deepest, most comprehensive reality, God."
-Albert Hofmann

Edited by Doctor_Dick (10/15/10 06:51 PM)

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Re: Extracting DMT - cloudy naptha? [Re: Doctor_Dick]
    #13341763 -

well i added some table salt to the base and that didn't really do anything. so i got as much of the naptha out of the top of the base water as i could and this is what i got



still see-through, but just barely


i added 75ml of clean naptha to the base solution but it's still pretty dark like the old naptha i just took out


--------------------
ONE-EYED WANT
-------------------------
knock a hoe out this dimension, continue my ascension
-bhad bhabie
rip. todcasil, acid sloth, st1llnox, shLong, ModestMouse, vinsue, big worm (sketch), tim

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Re: Extracting DMT - cloudy naptha? [Re: Envix]
    #13341776 -

what kind of naptha and lye did you use?, that is where your problem may lie :strokebeard2:


--------------------
War against a foreign country only happens when the moneyed classes think they are going to profit from it.-George Orwell-

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Re: Extracting DMT - cloudy naptha? [Re: Enigma of Ankou]
    #13341785 -

i used rooto 100% lye and vm&p naptha. but the root bark i used wwas very very very finely powdered


--------------------
ONE-EYED WANT
-------------------------
knock a hoe out this dimension, continue my ascension
-bhad bhabie
rip. todcasil, acid sloth, st1llnox, shLong, ModestMouse, vinsue, big worm (sketch), tim

Edited by Envix (10/15/10 08:56 PM)

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Re: Extracting DMT - cloudy naptha? [Re: Envix]
    #13341819 -

Well thats no emulsion you have there, it could be that the dark purplish tint of the mimosa migrated into the naptha tainting it.

I have never seen or heard of this problem before, you could crank your freezer way way down like the other person said and leave it in there for a few days solid, but other then that my only other suggestion would be throw it out and start anew :shrug:


--------------------
War against a foreign country only happens when the moneyed classes think they are going to profit from it.-George Orwell-

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Re: Extracting DMT - cloudy naptha? [Re: Enigma of Ankou]
    #13341905 -

It's might be tiny particles since it was so fine, let it sit and see if the brown settles out than you can decant into another container.  If that doesn't work you might have to do an a/b on it.

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