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OfflineBigNautical
bodhisattva

Registered: 07/17/04
Posts: 37
Loc: Alberta Cana-duh
Last seen: 11 years, 9 months
My compilation of methods
    #3304615 - 11/01/04 02:28 PM (12 years, 10 months ago)

First off, Im not a chemist and have little experience. I knew of a person that extracted Morphine last summer but had unsatisfactory results. I want to know if this compilation of methods will work if somebody was to attempt it.

-Extract a given amount of crushed poppy straw in a Coldfinger apparatus using methanol at a PH of about 9.

-Remove the alcohol by distillation to leave a residue.

-Mix residue with an aqueous lye solution with a PH of atleast 11.

-Filter the solution and wash a small amount of the lye solution as a filter aid.

-Add table salt to the solution to prevent emulsion.

-Extract the solution twice or thrice with a water-immiscible solvent Preferably Tolulene(since it has the best results with absorbing and killing all codeine) separate in a separatory funnel and discard tolulene layer.

-Lower the PH of the solution to 9.1 with acetic acid and leave over night for all the morphine to precipitate.

-The next day filter the solution leaving the morphine, wash with water and leave out to dry....

This is my compilation of a practical way of extracting decent amounts of morphine in the comfort of your own home from various sources.The person I mentioned before supposedly had quite a debacle when attempting to do this last summer.

Can anybody think of any reasons this wouldnt work.


--------------------
"Believe me! The secret of reaping the greatest fruitfulness and the greatest enjoyment from life is to live dangerously!"


-- Friedrich Wilhelm Nietzsche



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General Interest >> Science and Technology

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