Home | Community | Message Board


This site includes paid links. Please support our sponsors.


Welcome to the Shroomery Message Board! You are experiencing a small sample of what the site has to offer. Please login or register to post messages and view our exclusive members-only content. You'll gain access to additional forums, file attachments, board customizations, encrypted private messages, and much more!

Kraken Kratom Shop: Red Vein Kratom

Jump to first unread post Pages: 1
Some of these posts are very old and might contain outdated information. You may wish to search for newer posts instead.
OfflineDr. Seuss
The Cat in the Hat


Registered: 11/07/09
Posts: 174
Loc: Seussville
Last seen: 12 years, 8 months
Recrystallization?
    #11542326 - 11/28/09 11:18 AM (14 years, 2 months ago)

I've been helping a colleague of mine with his research project on DMT. Sadly, the user I discussed this topic with deleted all of his posts, thus I cannot refer to them for reference.

Which leads me to this already answered, yet lost question:

Recrystallization of DMT with n-heptane (Bestine)? Please explain.


--------------------
Today you are you, that is truer than true.
There is no one alive who is youer than you.

LOAD UNIVERSE INTO CANNON
AIM AT BRAIN
FIRE


Extras: Filter Print Post Top
OfflineDr.Myco87
Im a "Reader"
Male User Gallery

Registered: 12/23/08
Posts: 1,690
Loc: Land of the greedy! Flag
Last seen: 7 months, 21 days
Re: Recrystallization? [Re: Dr. Seuss]
    #11542414 - 11/28/09 11:38 AM (14 years, 2 months ago)

Dissolve spice in minimal amount of heptane and evap. I always do a first round that lets the nasties seperate to the bottom, which is plant fats and mostly DMT N-Oxide, I think. Then you just pull all the liquid out without pulling up the goo from the bottom of the jar, and put in an evap dish. You can use the remaining goo to put onto some plant material also. Now just let the heptane from the dish evap and you'll have DMT, actually I always use a scratch free wine glass for the final evap and let it evap slow by setting a cd on top, you'll get massive shards(this is done in the DMT Handbook, where I picked it up from). Just make it worth your while and do at least a gram or 2, it gets beautiful when you start to put in more than 2 or 3 grams. :crazy2:


--------------------
"I don’t do drugs. I am drugs."                -Salvador Dali

"I’ve never had a problem with drugs. I’ve had problems with the police."                                          -Keith Richards

"Reality is a crutch for people who can’t cope with drugs."                                          -Lily Tomlin



Extras: Filter Print Post Top
OfflineDr. Seuss
The Cat in the Hat


Registered: 11/07/09
Posts: 174
Loc: Seussville
Last seen: 12 years, 8 months
Re: Recrystallization? [Re: Dr.Myco87]
    #11543113 - 11/28/09 01:51 PM (14 years, 2 months ago)

No heating required?


--------------------
Today you are you, that is truer than true.
There is no one alive who is youer than you.

LOAD UNIVERSE INTO CANNON
AIM AT BRAIN
FIRE


Extras: Filter Print Post Top
OfflineDr.Myco87
Im a "Reader"
Male User Gallery

Registered: 12/23/08
Posts: 1,690
Loc: Land of the greedy! Flag
Last seen: 7 months, 21 days
Re: Recrystallization? [Re: Dr. Seuss]
    #11543363 - 11/28/09 02:39 PM (14 years, 2 months ago)

Quote:

Dr. Seuss said:
No heating required?




I'm sorry about that, yes, heat it in a hot water bath, no fire though, just heat some water on the stove and then put the jar or whatever in their after the stove is off, just so theires no chance of an explosion.


--------------------
"I don’t do drugs. I am drugs."                -Salvador Dali

"I’ve never had a problem with drugs. I’ve had problems with the police."                                          -Keith Richards

"Reality is a crutch for people who can’t cope with drugs."                                          -Lily Tomlin



Extras: Filter Print Post Top
InvisibleWWorker
...

Registered: 09/09/07
Posts: 395
Re: Recrystallization? [Re: Dr.Myco87]
    #11544419 - 11/28/09 05:28 PM (14 years, 2 months ago)

Hey Seuss, I usually freeze precip.  That insures that you leave the nasties behind.  I freeze condensed(piss yellow) naptha at least once, sometimes re-x twice.  Then after the crystals are swirled around and poured out after 24 hours in the freezer, I dissolve once more in an ounce or two of heptane and freeze again.  You lose a little yield with each re-x but it is so worth it when you get those fluffy white crystals.

Just to clarify, I never evap a whole cup/tray down to crystals.  Doing that leaves any impurities in with your crystals after the solvent is gone.  By freezing, you separate the goodies from the nasties.

As an aside...never throw anything away until you are happy with your yield.  If your yield is light, then go back to one of your solvent jars..or basified goop and get it.  IT can't disappear.  It is always somewhere...


--------------------


Extras: Filter Print Post Top
OfflineDr.Myco87
Im a "Reader"
Male User Gallery

Registered: 12/23/08
Posts: 1,690
Loc: Land of the greedy! Flag
Last seen: 7 months, 21 days
Re: Recrystallization? [Re: WWorker]
    #11544500 - 11/28/09 05:39 PM (14 years, 2 months ago)

Quote:

WWorker said:
Hey Seuss, I usually freeze precip.  That insures that you leave the nasties behind.  I freeze condensed(piss yellow) naptha at least once, sometimes re-x twice.  Then after the crystals are swirled around and poured out after 24 hours in the freezer, I dissolve once more in an ounce or two of heptane and freeze again.  You lose a little yield with each re-x but it is so worth it when you get those fluffy white crystals.

Just to clarify, I never evap a whole cup/tray down to crystals.  Doing that leaves any impurities in with your crystals after the solvent is gone.  By freezing, you separate the goodies from the nasties.

As an aside...never throw anything away until you are happy with your yield.  If your yield is light, then go back to one of your solvent jars..or basified goop and get it.  IT can't disappear.  It is always somewhere...




Just to be clear, I always freeze precip also but even doing that the naptha will deposit some yuckies on the deemsters while pouring the solvent out, so I do a recrystalization after the freeze precip to get any remaining goo out, and the result is clear/white and fluffy deemsters.


--------------------
"I don’t do drugs. I am drugs."                -Salvador Dali

"I’ve never had a problem with drugs. I’ve had problems with the police."                                          -Keith Richards

"Reality is a crutch for people who can’t cope with drugs."                                          -Lily Tomlin



Extras: Filter Print Post Top
Jump to top Pages: 1

Kraken Kratom Shop: Red Vein Kratom


Similar ThreadsPosterViewsRepliesLast post
* marsofold tek - heptane, naphtha or DCM ( dichloromethane )? ionicle 5,469 3 11/03/17 05:26 PM
by Northerner
* Got Crystal ?
( 1 2 all )
lovepalace 8,144 24 02/20/06 06:28 PM
by Corporal Kielbasa
* Crystal Myth rikjoh 6,284 18 08/05/07 10:16 PM
by challenger
* DMT crystallization problem
( 1 2 3 all )
blitz007 10,479 44 09/07/08 04:31 PM
by Entropymancer
* Psilocybin crystal vodka extraction?
( 1 2 all )
wre 9,789 27 08/26/09 09:49 AM
by fireshaman
* Extraction Solvent question Endlessness 1,376 6 02/19/08 07:52 PM
by jizmaster
* washing hair/dust particles from dmt crystals..? ninetynine 2,087 4 01/28/05 06:10 PM
by dblaney
* Solvent-based Hash extraction Hix 3,320 18 03/10/06 10:50 AM
by coda

Extra information
You cannot start new topics / You cannot reply to topics
HTML is disabled / BBCode is enabled
Moderator: psilocybinjunkie, Rose, mushboy, LogicaL Chaos, Northerner, bodhisatta
2,218 topic views. 1 members, 47 guests and 10 web crawlers are browsing this forum.
[ Show Images Only | Sort by Score | Print Topic ]
Search this thread:

Copyright 1997-2024 Mind Media. Some rights reserved.

Generated in 0.018 seconds spending 0.004 seconds on 12 queries.