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InvisibleOgla
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Registered: 02/16/04
Posts: 11,321
freezing DMT question
    #8762998 - 08/12/08 02:03 PM (15 years, 6 months ago)

ok, so i have some experince in DMT extraction.  too help save cost of material, i want to try to freeze the DMT.  So i'll throw jar with solvent in the freezer overnight  and is it ok to pour into a funnel with polyfil/cotton balls to catch the dmt? I've seen how the guy in the mescal tek uses cotton balls and funnel. i know coffee filter is recommended, but is difficult and dosen't seem to always work.

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OfflineNature Boy
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Registered: 07/09/07
Posts: 8,246
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Re: freezing DMT question [Re: Ogla]
    #8763581 - 08/12/08 04:32 PM (15 years, 6 months ago)

I don't find it necessary to filter at all.  Put your jar in the freezer for 2, maybe 3 days.  The crystals will precipitate out and adhere to the bottom mostly, and a tad on the sides.

I pour the solvent back into the basified MHRB solution and repeat the solvent extraction.  Dry the jar out thoroughly and scrape off and collect the DMT.  It is not until I get no crystal formation at all that I concentrate the DMT in solution via evaporation 4X.

In other words, if I pull off 100cc's of naptha that doesn't precipitate out any crystals, I'll reduce its volume via evaporation down to 25 cc's, and then re-freeze.  Viola.  Crystals.  The 25 cc's goes back AGAIN into the basified solution along with maybe another 50 cc's of naptha.

This procedure saves on solvent and gets all the DMT eventually via freeze-precipitation without filtration and associated losses.  I've gotten 1 to 1.25% depending on the quality of the bark.  I.E. I get 1 to 1.25 gram for 100 grams MHRB.

N.B.


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Edited by Nature Boy (08/12/08 04:34 PM)

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