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Cannashroom
Smoke two Joints


Registered: 10/25/07
Posts: 2,141
Loc: Everywhere
Last seen: 6 years, 9 months
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Yeah, my friend and I are having so much fun just doing the extraction, we both take chem but hes in organic chem which i will take next year. We already got around .1grams of crystal but we messed up and let a lot redissolve into solution, so were adding that solvent to the stuff from the second pull and going for a second freeze precipitation tonight, so excited to try out my first hit of DMT tonight, We got off white crystals, look amazing!
-------------------- "A human being is part of the whole, called by us 'Universe'; a part limited in time and space. He experiences himself, his thoughts and feelings as something separated from the rest -- a kind of optical delusion of his consciousness. This delusion is a kind of prison for us, restricting us to our personal desires and affection for a few persons nearest us. Our task must be to free ourselves from this prison by widening our circle of compassion to embrace all living creatures and the whole nature in its beauty. Nobody is able to achieve this completely but striving for such achievement is, in itself, a part of the liberation and a foundation for inner security." Albert Einstein
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Entropymancer


Registered: 07/16/05
Posts: 10,207
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Re: Powder mimosa/water covering jar [Re: Cannashroom]
#8047753 - 02/20/08 03:15 PM (15 years, 11 months ago) |
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More will come out of solution the less naphtha there is. If you can, put it in front of a fan (or use some other safe method to reduce the volume) for a while today before letting it freeze-precip tonight.
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Cannashroom
Smoke two Joints


Registered: 10/25/07
Posts: 2,141
Loc: Everywhere
Last seen: 6 years, 9 months
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Re: Powder mimosa/water covering jar [Re: Entropymancer]
#8048470 - 02/20/08 06:10 PM (15 years, 11 months ago) |
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I already took the naphtha from the second pull and mixed it with the first, let it evaporate to just above half and then I put it outside. Crystals have been growing all day but in the last hour seemed to have stopped/slowed their growth(-13C outside by weather report). I think it has reached equilibrium. My friends and I are eager to try it out and we don't have enough from the first pull so we are going to take the crystals out soon, then the solution back outside(maybe evaporate some). It is supposed to go down to -18 at 5am so more will come out then.
I estimate combined these two pulls will total in .2-.4 grams of DMT so I should be able to get more of it from the mimosa with another pull since it was 90gams of powder to start. I have a question, could too high of a pH, 14 or above cause the DMT to be destroyed?
-------------------- "A human being is part of the whole, called by us 'Universe'; a part limited in time and space. He experiences himself, his thoughts and feelings as something separated from the rest -- a kind of optical delusion of his consciousness. This delusion is a kind of prison for us, restricting us to our personal desires and affection for a few persons nearest us. Our task must be to free ourselves from this prison by widening our circle of compassion to embrace all living creatures and the whole nature in its beauty. Nobody is able to achieve this completely but striving for such achievement is, in itself, a part of the liberation and a foundation for inner security." Albert Einstein
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TheShroomJew23
The Chemist


Registered: 11/29/07
Posts: 1,611
Loc: Temple
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Re: Powder mimosa/water covering jar [Re: Cannashroom]
#8049338 - 02/20/08 09:19 PM (15 years, 11 months ago) |
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I use 100 grams of bark and I get 1 to 2 grams of crystal. No Lie
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 You will be missed
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Entropymancer


Registered: 07/16/05
Posts: 10,207
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Re: Powder mimosa/water covering jar [Re: TheShroomJew23]
#8049382 - 02/20/08 09:25 PM (15 years, 11 months ago) |
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That means your rootbark gets up to more than three times as much DMT as is usually listed for the plant. (0.6% is the standard figure as I recall, though I know people's actual yields can tend to indicate closer to the 1% DMT mark)
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Cannashroom
Smoke two Joints


Registered: 10/25/07
Posts: 2,141
Loc: Everywhere
Last seen: 6 years, 9 months
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Re: Powder mimosa/water covering jar [Re: Entropymancer]
#8049511 - 02/20/08 09:41 PM (15 years, 11 months ago) |
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Yes, I am unsatisfied with my yield as of right now. I used around 90grams of bark and have gotten around 270mg +/- 50mg Id say (My scale in neither accurate nor precise )so far. But I still have the solution outside again, and it has become cloudy once more, so it should precipitate out some more crystals. Furthermore, I added more solvent to the jars and am going for a third pull.
This was my first extraction and I made mistakes, I'm getting pH papers for my next one and I hope to use my experience this time to help me get a better yield next time, but I'm excited to embark on my first spice journey very soon.
-------------------- "A human being is part of the whole, called by us 'Universe'; a part limited in time and space. He experiences himself, his thoughts and feelings as something separated from the rest -- a kind of optical delusion of his consciousness. This delusion is a kind of prison for us, restricting us to our personal desires and affection for a few persons nearest us. Our task must be to free ourselves from this prison by widening our circle of compassion to embrace all living creatures and the whole nature in its beauty. Nobody is able to achieve this completely but striving for such achievement is, in itself, a part of the liberation and a foundation for inner security." Albert Einstein
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TheShroomJew23
The Chemist


Registered: 11/29/07
Posts: 1,611
Loc: Temple
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Re: Powder mimosa/water covering jar [Re: Cannashroom]
#8049779 - 02/20/08 10:36 PM (15 years, 11 months ago) |
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get a digital pH tester that is +/- 0.1 accurate. I got mine for like 30.
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 You will be missed
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ReoSpeedwagon153


Registered: 02/04/06
Posts: 2,098
Loc: Chetumal, Mexico
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Re: Powder mimosa/water covering jar [Re: TheShroomJew23]
#8051066 - 02/21/08 09:22 AM (15 years, 11 months ago) |
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I will agree with you, shroomjew.
I was very confused about the kinds of yields I was geting compared to the listed potency of the plant.
Seriously, almost reliably two grams from a hundred grams plant matter.
-------------------- “I thought naming myself ‘ReoSpeedwagon153’ on a forum was a funny idea in 2006.”
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