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Left Coast Kratom Shop: Kratom Powder For Sale

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InvisibleiBruiseBlue
Stranger

Registered: 06/23/07
Posts: 98
Crude Mescaline Wash w/ Acetone?
    #7809751 - 12/29/07 04:20 AM (16 years, 1 month ago)

I was wondering if one could take the product of 99% isopropanol extraction of trichocereus cacti and wash the result with acetone to reduce the amount of impurities and perhaps have a cleaner product. I've heard that when you evaporate the alcohol you are left with mescaline carbonate, but others say mescaline freebase. Maybe you could add something like citric acid to your collected alcohol to convert the alkaloids to salt form so that the acetone won't dissolve the mescaline. Has anyone one tried something like this? Please don't tell me to just do an A/B extraction, I really don't have the time or a place to do it. Any help appreciated.


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Offlineimplee
Cyber Hippie
Male User Gallery

Registered: 07/27/06
Posts: 5,833
Loc: Houston, Texas. Flag
Last seen: 5 months, 19 days
Re: Crude Mescaline Wash w/ Acetone? [Re: iBruiseBlue]
    #7809771 - 12/29/07 04:49 AM (16 years, 1 month ago)

check out the new chemistry section


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InvisibleAfroshroomerican
Oprah's Minion
Male


Registered: 05/12/06
Posts: 891
Loc: Pennsylvania
Re: Crude Mescaline Wash w/ Acetone? [Re: iBruiseBlue]
    #7809780 - 12/29/07 04:58 AM (16 years, 1 month ago)

I wouldn't risk it, in my opinion.

Acetone washing in an A/B extraction is safe because salts (the mescaline BOUND to the acid/salt e.g. Mesc HCL) are insoluble in acetone, whereas many organic impurities are (this allows for such recrystallization).   

You just have free alkaloids--just eat it :froman:


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InvisibleiBruiseBlue
Stranger

Registered: 06/23/07
Posts: 98
Re: Crude Mescaline Wash w/ Acetone? [Re: Afroshroomerican]
    #7809812 - 12/29/07 05:50 AM (16 years, 1 month ago)

Thanks, I'll stick to just eating the tar. I read somewhere about someone using 99% iso and getting 4 grams of green solid material from 100 grams of dry cacti, but I always get sticky tar.


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OfflineShroomDoom
Friend of the Medicine
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Registered: 06/07/04
Posts: 4,435
Loc: A Psychedelic State Flag
Last seen: 1 year, 8 months
Re: Crude Mescaline Wash w/ Acetone? [Re: iBruiseBlue]
    #7810284 - 12/29/07 11:27 AM (16 years, 1 month ago)

if you dry out the 99% iso and the 1% of water, all that is left is a tacky green flaky tar, which can be crushed into powder even, or made into balls.


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