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WWorker
...

Registered: 09/09/07
Posts: 395
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I freeze precip and pour off that yellow naptha. I am left with a white-to-cream fluffy powder.
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bloodbrother778
Super Chimpanzee

Registered: 10/26/07
Posts: 418
Last seen: 2 months, 23 days
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Re: I want to try out DMT. [Re: clover606]
#7793529 - 12/23/07 07:11 PM (16 years, 1 month ago) |
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Quote:
clover606 said:
Quote:
bloodbrother778 said: its impossible to net that much from 1/2 lb, the DMT content of MHRB is like .57%, 2.5 g is about the amount you get from a pound, you must've had impurities in your crystals
MHRB can have alkaloid levels as high as 1%, they can range drastically but 2.5 g is definatly not /impossible/ to get out of a half pound. maybe hes just way better at extraction than you.
It's not just me, I've never heard of anyone ever getting that much out of a 1/2 pound, that's about the amount that people describe getting out of a pound......... Leading me to believe that his extraction was the inconsistency..... Unless perhaps he got the pink/purple bark which does have higher DMT content Also may I suggest sounding a bit less insulting when saying things like that, theres just no need for it
Also the method that I was talking about is the freeze/precip method, no need for defat, you're left with very pure white fluffy crystals, I would highly recommend using it
http://tribes.tribe.net/ethnobotany/thread/bddc25e3-aeca-418d-811b-a46bbbc5d603
Edited by bloodbrother778 (12/23/07 07:16 PM)
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clover606
Stranger

Registered: 08/13/07
Posts: 656
Last seen: 10 years, 4 months
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i didnt mean to sound insulting, and do apologize for any hurt feelings. i still dont think its impossible though. i personally always use the purple inner rootbark when i can, and have gotten as much as 2.1g out of 250 grams of bark. do you use whole bark? maybe thats your problem, whos your supplier?
-------------------- grassman said: I remember being in DARE when i was much younger and some of the stories they would tell you are not only ridiculous, but completely untrue. One story was that a woman was on LSD and thought her infant was a turkey so she baked it in the oven. Now I look back and think thats hilarious, but at the time I guess it scared me.
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Sra_sephiroth0
Malicious Puppet's clone


Registered: 12/11/07
Posts: 411
Last seen: 16 years, 6 days
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Re: I want to try out DMT. [Re: WWorker]
#7793868 - 12/23/07 09:30 PM (16 years, 1 month ago) |
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Quote:
WWorker said: I freeze precip and pour off that yellow naptha. I am left with a white-to-cream fluffy powder.
what do you mean pour it off,?
-------------------- "You all are just puppets... You have no heart...and cannot feel any pain..."" you may think thats pain you feel but you must have a heart to feel true pain and that pain wont be yours
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Robo
R Series 66Y
Registered: 05/08/07
Posts: 14,861
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Quote:
bloodbrother778 said:
Quote:
WWorker said: search mimosa hostilis on ebay. I got 1/2 pound of powder for 40 bucks....netted about 2.5g
its impossible to net that much from 1/2 lb, the DMT content of MHRB is like .57%, 2.5 g is about the amount you get from a pound, you must've had impurities in your crystals
I've seen at least 3 grams pulled from 1/2 lb. MHRB, it's not impossible.
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Divinatory
Rubber Tramp



Registered: 05/15/07
Posts: 690
Loc: Texas
Last seen: 10 years, 22 days
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Re: I want to try out DMT. [Re: waixingren]
#7794299 - 12/23/07 11:40 PM (16 years, 1 month ago) |
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Quote:
waixingren said: personally though i would skip the ammonia wash. ive heard so many bad stories of brown gunk left over after an ammonia wash.
I second that!!! I'm actually one of the people that got a fucked up result from ammonia. I started with I think 3.12 grams of impure, washed with ammonia which came out to be a light brownish/yellow goo, had re-extract and recrystalize which resulted in me losing almost or a little over a gram.. recrystalizing does wonders, stay away from ammonia.
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Sra_sephiroth0
Malicious Puppet's clone


Registered: 12/11/07
Posts: 411
Last seen: 16 years, 6 days
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Re: I want to try out DMT. [Re: Divinatory]
#7794389 - 12/24/07 12:10 AM (16 years, 1 month ago) |
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explain re extracting, did you just dislove in naptha again? or into a base?
-------------------- "You all are just puppets... You have no heart...and cannot feel any pain..."" you may think thats pain you feel but you must have a heart to feel true pain and that pain wont be yours
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Divinatory
Rubber Tramp



Registered: 05/15/07
Posts: 690
Loc: Texas
Last seen: 10 years, 22 days
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Re: I want to try out DMT. [Re: Christoph]
#7794397 - 12/24/07 12:14 AM (16 years, 1 month ago) |
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yes I dissolved it back into naphtha, super saturated the mix and then stuck it in the freezer to precipiated, I got good clean clean crystals after that
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andrewss
precariously aggrandized


Registered: 08/17/07
Posts: 8,725
Loc: ohio
Last seen: 1 month, 13 days
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Re: I want to try out DMT. [Re: Divinatory]
#7794401 - 12/24/07 12:16 AM (16 years, 1 month ago) |
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im about in the same boat you are... im thinkin about extractin some DMT... good luck to you
-------------------- Jesus loves you.
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Sra_sephiroth0
Malicious Puppet's clone


Registered: 12/11/07
Posts: 411
Last seen: 16 years, 6 days
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Re: I want to try out DMT. [Re: andrewss]
#7794423 - 12/24/07 12:23 AM (16 years, 1 month ago) |
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hmm i really need a freezer tho its cold enough out side these days
-------------------- "You all are just puppets... You have no heart...and cannot feel any pain..."" you may think thats pain you feel but you must have a heart to feel true pain and that pain wont be yours
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bloodbrother778
Super Chimpanzee

Registered: 10/26/07
Posts: 418
Last seen: 2 months, 23 days
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Re: I want to try out DMT. [Re: clover606]
#7794451 - 12/24/07 12:37 AM (16 years, 1 month ago) |
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Quote:
clover606 said: i didnt mean to sound insulting, and do apologize for any hurt feelings. i still dont think its impossible though. i personally always use the purple inner rootbark when i can, and have gotten as much as 2.1g out of 250 grams of bark. do you use whole bark? maybe thats your problem, whos your supplier?
ok yeah that makes sense, I was talking about whole bark, which is what I usually use due to its cheapness, the inner bark does have more DMT in it, so yeah you will get more from that, but more often than not regular bark is used, which is why I was referring to it
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Sra_sephiroth0
Malicious Puppet's clone


Registered: 12/11/07
Posts: 411
Last seen: 16 years, 6 days
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inner bark isnt that expensive
-------------------- "You all are just puppets... You have no heart...and cannot feel any pain..."" you may think thats pain you feel but you must have a heart to feel true pain and that pain wont be yours
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undergrounder
fluffy bunny



Registered: 11/10/06
Posts: 1,394
Loc: Sydney
Last seen: 1 year, 7 months
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Quote:
Sra_sephiroth0 said: seriously how come no one DEFATTS when i straight up defat my bark with the acid solution it pulls a whole mess of junk out the solution so where is that stuff thats pulled with you do your naptha pulls does that just settle out? tho it cant really steelt out of the naptha
My guess is at high enough pH levels the emulsions you usually get in a defat don't appear. From everything i've read you don't need to defat MHRB. People seem to be able to get good (better even) yield and potency from a straight base tek.
For clear crystals the key is to freeze precip, not evaporate all the way. Then redissolve the crystals in super-saturated warm naptha, pull out the yellow drops and freeze precip a final time.
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RIP Bigger and bolder and rougher and tougher in other words sucka there is no other...
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Sra_sephiroth0
Malicious Puppet's clone


Registered: 12/11/07
Posts: 411
Last seen: 16 years, 6 days
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ok thanks i have to agree for its only been pure white via freeze ing it tho lsa i did a evap and that was very clean pure. that you have to do as an acid base not for fats but to pull out other unwanted stuff I.E. the stuff that gives nausea, i really suggest anyone that has extracted dmt to extract LSA and have some of those sweet little crystals just dont OD
-------------------- "You all are just puppets... You have no heart...and cannot feel any pain..."" you may think thats pain you feel but you must have a heart to feel true pain and that pain wont be yours
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WWorker
...

Registered: 09/09/07
Posts: 395
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I use powdered inner bark that is pink/purple. The first time I did it I used naptha...freeze precip and ammoniia wash. The second time i did it I used naptha gfor extract, freeze precip, redissovle in bestine, and freeze precip.....almost pure white.
I will be using bestine and no ammonia from now on.
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Christoph
Stranger



Registered: 08/18/07
Posts: 23
Last seen: 10 years, 4 months
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Re: I want to try out DMT. [Re: WWorker]
#7847137 - 01/08/08 09:05 AM (16 years, 24 days ago) |
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Ok, so i tried to do an extraction. But i got some of the brown stuff in my naptha when i poured it to the evap-plate. Now it's almost all evaped. But does the fact that i got that brown stuff in it as well mean it's all contaminated?
I truly need your help, i might end up poisoning my self..=)
Peace
-------------------- The Shrooms i tells ya the SHROOOMS!!
Edited by Christoph (01/08/08 02:09 PM)
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Christoph
Stranger



Registered: 08/18/07
Posts: 23
Last seen: 10 years, 4 months
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Re: I want to try out DMT. [Re: Christoph]
#7848734 - 01/08/08 04:04 PM (16 years, 24 days ago) |
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Ok, i took some pictures of it for you to judge and help me=)
The pan is ~30cm across.


Here's where the main contams are

Least contaminations:

Last overview

peace
-------------------- The Shrooms i tells ya the SHROOOMS!!
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g00ru
lit pants tit licker



Registered: 08/09/07
Posts: 21,088
Loc: georgia, us
Last seen: 5 years, 1 month
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Re: I want to try out DMT. [Re: Christoph]
#7848868 - 01/08/08 04:31 PM (16 years, 24 days ago) |
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i just did it for the first time.
holy shit.
-------------------- check out my music! drowse in prison and your waking will be but loss
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Christoph
Stranger



Registered: 08/18/07
Posts: 23
Last seen: 10 years, 4 months
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Re: I want to try out DMT. [Re: g00ru]
#7848880 - 01/08/08 04:33 PM (16 years, 24 days ago) |
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Extracted or smoked?
Peace
-------------------- The Shrooms i tells ya the SHROOOMS!!
Edited by Christoph (01/08/08 04:40 PM)
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undergrounder
fluffy bunny



Registered: 11/10/06
Posts: 1,394
Loc: Sydney
Last seen: 1 year, 7 months
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Re: I want to try out DMT. [Re: Christoph]
#7849208 - 01/08/08 05:23 PM (16 years, 24 days ago) |
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Your spice pan looks fine Congrats 
Just avoid scraping up the yellow sticky stuff. That used to happen to me too, but its no big deal. If you smoke it it will be harsher and probably not very good for you but a little bit won't kill you. If you want to clean it up, redisolve all the crystals in a shotglass of naptha and the yellow will fall to the bottom.
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RIP Bigger and bolder and rougher and tougher in other words sucka there is no other...
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