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cpw1971
Mr

Registered: 10/07/06
Posts: 5,611
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Re: Help me DMT [Re: Slimz]
#7553837 - 10/24/07 06:30 AM (16 years, 3 months ago) |
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you dont need lab equipment with this method. a sep funnel would get clogged I used a glass pitcher and just poured off the naptha layer
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Slimz
.-~*´`*·~-experience-~*´`*·~-.




Registered: 10/03/07
Posts: 3,588
Loc: Maryland
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Re: Help me DMT [Re: cpw1971]
#7553856 - 10/24/07 06:39 AM (16 years, 3 months ago) |
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Ill stick with my proven lab methods so i will be sure to end up with a high yield pure product.
-------------------- Lazy Drywall Tek (no powdery mess) This series will blow your mind and confirm what you already know to be true. The Pharmacratic Inquisition Best Thread Ever ! ! !
me if you have questions about lasers Although i may advise others in a general way regarding all types of mushroom grows, and may even post question from other forums about growing "active" mushrooms, i only grow non-"active" mushrooms and edibles. FeelFamily resident tech guru
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maggotz


Registered: 06/24/06
Posts: 7,539
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Re: Help me DMT [Re: cpw1971]
#7553860 - 10/24/07 06:41 AM (16 years, 3 months ago) |
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how clean is the end product?
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Slimz
.-~*´`*·~-experience-~*´`*·~-.




Registered: 10/03/07
Posts: 3,588
Loc: Maryland
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Re: Help me DMT [Re: maggotz]
#7553917 - 10/24/07 07:12 AM (16 years, 3 months ago) |
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I have read over the extractions and this is a standard salt/freebase/salt extraction.. i should have no problems with it at all... I will probably use hydrochloric acid as my acid and Sodium hydroxide as my base. ill whip up some chloroform for recrystallizing...
-------------------- Lazy Drywall Tek (no powdery mess) This series will blow your mind and confirm what you already know to be true. The Pharmacratic Inquisition Best Thread Ever ! ! !
me if you have questions about lasers Although i may advise others in a general way regarding all types of mushroom grows, and may even post question from other forums about growing "active" mushrooms, i only grow non-"active" mushrooms and edibles. FeelFamily resident tech guru
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cpw1971
Mr

Registered: 10/07/06
Posts: 5,611
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Re: Help me DMT [Re: maggotz]
#7554117 - 10/24/07 08:40 AM (16 years, 3 months ago) |
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light cream colored slimz do what you want but I have fucked up quite a few of the acid/ base extractions and after trying the new method I will never look back.
Edited by cpw1971 (10/24/07 10:06 AM)
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SDP
ChronicAficionado




Registered: 01/21/05
Posts: 1,297
Last seen: 5 months, 28 days
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Re: Help me DMT [Re: Slimz]
#7554184 - 10/24/07 09:08 AM (16 years, 3 months ago) |
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Check out this thread IN FULL, or at least the initial post + all my posts throughout the thread.
http://www.shroomery.org/forums/showflat.php/Cat/0/Number/6667657/page/0/fpart/1/vc/1
It covered a FULL technique discourse for extracting from MHRB as well as freeze precipitating, purifying & recrystallizing to get the purest product + optimal yield. Pouring off naphtha then using a turkey baster to suck the rest works as well as a seperatory funnel. You should find that thread very useful! Shirley did a pictorial of the process as well. Hope it helps!

-SDP
-------------------- Teonanacatl, open up my eyes This sacrament, this prayer, beyond the world of lies Guide me clearly through that which I dont understand Give me strength to find the path Help me fight any demons as you flow through me wholely This is my prayer, that you protect me from evil, and bring me closer to peace And open up my eyes, so i can see things as you do Amen
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Slimz
.-~*´`*·~-experience-~*´`*·~-.




Registered: 10/03/07
Posts: 3,588
Loc: Maryland
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Re: Help me DMT [Re: SDP]
#7554191 - 10/24/07 09:12 AM (16 years, 3 months ago) |
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Werd.. thanks...
-------------------- Lazy Drywall Tek (no powdery mess) This series will blow your mind and confirm what you already know to be true. The Pharmacratic Inquisition Best Thread Ever ! ! !
me if you have questions about lasers Although i may advise others in a general way regarding all types of mushroom grows, and may even post question from other forums about growing "active" mushrooms, i only grow non-"active" mushrooms and edibles. FeelFamily resident tech guru
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Robo
R Series 66Y
Registered: 05/08/07
Posts: 14,861
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Re: Help me DMT [Re: Slimz]
#7554570 - 10/24/07 11:28 AM (16 years, 3 months ago) |
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Quote:
Slimz said: I will probably use hydrochloric acid as my acid
Skip defat, no acid required.
Quote:
maggotz said: how clean is the end product?
Usually not that clean. But the end product can be washed with an ammonia soltution through a filter to give you clean white/off-white crystal.
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