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InvisibleKnoa6
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Registered: 04/25/07
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: enesi]
    #7108486 - 06/29/07 07:33 PM (16 years, 6 months ago)

those crystals look awesome dude, sphongle rocks as well! enjoy!


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Offlineenesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: Knoa6]
    #7114392 - 07/01/07 08:40 AM (16 years, 6 months ago)

Done with the CFC, here is the finished product. It was super easy to get these, if you are doing dmt extractions and not getting nice crystals like this, you need to check your approach, it's just too easy!

Mine aren't super pure or anything, but it's a lot nicer then some orange/brown goo, lol



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InvisiblecoAsTal
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: enesi]
    #7114976 - 07/01/07 01:18 PM (16 years, 6 months ago)

That is some grade-a fucking gorgeous spice brother!!!:yourock:

:mushroom2::mushroom2::mushroom2::mushroom2::mushroom2:
for you


--------------------
I am certain of nothing but the holiness of the Heart's affections and the truth of Imagination--  John Keats

Spore Trading List


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Offlineenesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: coAsTal]
    #7114999 - 07/01/07 01:29 PM (16 years, 6 months ago)

Quote:

coAsTal said:
That is some grade-a fucking gorgeous spice brother!!!:yourock:

:mushroom2::mushroom2::mushroom2::mushroom2::mushroom2:
for you



Thanks man, I actually followed the marsfold tek, but i took a few tips from this one we are posting in.  :smile:


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Offlineshirley knott
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: enesi]
    #7115220 - 07/01/07 02:33 PM (16 years, 6 months ago)

Quote:

enesi said:


holy shit :crazy2:


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buh


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Offlineenesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: shirley knott] * 1
    #7115251 - 07/01/07 02:45 PM (16 years, 6 months ago)

The photo above, still wet with solvent

Here is ONE completely dry crystal, about the size of a dime


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OfflineMr E Guest
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: BlueDruid]
    #7128719 - 07/04/07 01:55 PM (16 years, 6 months ago)

Quote:


Quote:
shirley knott said:
hey buddy - last time i was in a big B&Q i discovered that they sell naphtha near the barbecue section in huge 4l white plastic tubs. FUCK! i wish i'd known that before.



I've been looking about for naphtha as I can only find artists white spirit in tiny bottles & I think I saw the one you mean in B&Q - "Bartoline Paraffin premium BS2869.C1 contains naphtha (petroleum) hydrotreated heavy UN1223 Kerosene"
I wasn't sure about it as it says kerosene & I don't know what the numbers relate to. Does anyone? It'd be useful to compare it with another one I found
"Bartoline premium low odour white spirit contains naphtha (petroleum) hydrotreated heavy UN no 1268 petroleum distillates"
I thought this one might be purer as it refers to petroleum distillates rather than kerosens but if the UN numbers refer to a data sheet or list of contents and percentages it could be easy to tell.
D4D0C8



The UN numbers are for identification purposes; they refer to the United Nation list of hazardous substances and are used to help the emergency services in case of spillages and other accidents, so don't worry about them. Kerosene is a more specific grade of petroleum distillate; also it's considered a synonym for paraffin. And naphtha is just another term for various grades of petroleum distillate, too. PM me for more information about UN numbers.

The BS number refers to a British Standard. Looking up that reference number will afford you a bit more detail about the likely composition of your white spirit.

The main thing, I think it was stated on complementary DMT extraction thread, is to check for greasy/waxy residue by allowing a drop or two to evaporate from some suitable non-porous surface. White spirit has a fairly high bp but so long as it's sufficiently pure not to leave a greasy residue it should be ok. Also, I have a feeling that higher bp hydrocarbons might do a better job of extracting than the more volatile stuff. Although I could be entirely wrong on this matter. As Mark Twain once said "I like science because it gives such a wholesome return of conjecture from a trifling investment of fact." (Thanks to Alexander Shulgin for that one.)


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Be joyful. This could be the only chance you get.

All of the above posts are the fevered imaginings of a deluded mind, itself entirely the fictional creation of a somewhat peculiar author with a bizarre sense of humour.


Edited by Mr E Guest (07/04/07 01:59 PM)


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OfflineMr E Guest
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: Mr E Guest]
    #7128843 - 07/04/07 02:31 PM (16 years, 6 months ago)

Here are the approximate boiling ranges of some relevant petroleum distillates.

Gasoline: boiling range 40-180oC, 6-10 carbon atoms

Naphtha: boiling range 180-260oC, 10-14 carbon atoms

Kerosine: boiling range 260-340oC, 14-20 carbon atoms

And adding more lye (solution) to raise the pH, and if you wish, a bit of table salt (fine crystals) - a technique I believe is known as 'salting out' - definitely helps break down those annoying emulsions! I added a couple of ~150ml portions of 33% NaOH solution to my mix, plus about a tablespoon of NaCl sprinkled in, and each time got back an equal volume of hydrocarbon from the emulsion.:grin:

Love the pics, btw, guys - well done!  :thumbup: :mushroom2::mushroom2::mushroom2::mushroom2::mushroom2:
Shame I couldn't get any pics of mine.


--------------------
Be joyful. This could be the only chance you get.

All of the above posts are the fevered imaginings of a deluded mind, itself entirely the fictional creation of a somewhat peculiar author with a bizarre sense of humour.


Edited by Mr E Guest (07/06/07 06:12 PM)


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OfflineThe_Kman
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: Mr E Guest]
    #7180131 - 07/15/07 05:47 PM (16 years, 6 months ago)

Im currently having a go at my first ever DMT extraction using this method. Ill let everyone know how it goes. did have a half pound of MHRB, but have split that in half to give me two separate runs at it.

Ill see how it goes.


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Offlineenesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: The_Kman]
    #7180305 - 07/15/07 06:38 PM (16 years, 6 months ago)

Quote:

The_Kman said:
Im currently having a go at my first ever DMT extraction using this method. Ill let everyone know how it goes. did have a half pound of MHRB, but have split that in half to give me two separate runs at it.

Ill see how it goes.


Good luck, be sure to post up your results


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InvisibleOgla
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: enesi]
    #7180729 - 07/15/07 08:16 PM (16 years, 6 months ago)

Bad ass. Im attempting an extraction soon myself. Keep you updated


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OfflineMr E Guest
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: Ogla]
    #7184158 - 07/16/07 04:59 PM (16 years, 6 months ago)

Quote:

The_Kman said:
Im currently having a go at my first ever DMT extraction using this method. Ill let everyone know how it goes. did have a half pound of MHRB, but have split that in half to give me two separate runs at it.

Ill see how it goes.




Hope you're seeing your first gram of beautiful elf spice already! And an update on the solvent front - I've just found that photographic film and foil degreasing fluid is apparently ideal as a naphtha substitute. Check the label says something like '100% volatile aliphatic hydrocarbons'. Obtainable from your local photographic supplies store, but it might be expensive. Fortunately, I found mine just lying around!

It's highly volatile, evaporating (readily!) without trace. Beware! This makes it highly flammable - more so than any of the other solvents I've found so far. Also, it's virtually odourless, even compared to Coleman fuel.


--------------------
Be joyful. This could be the only chance you get.

All of the above posts are the fevered imaginings of a deluded mind, itself entirely the fictional creation of a somewhat peculiar author with a bizarre sense of humour.


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OfflineThe_Kman
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: Mr E Guest]
    #7185827 - 07/16/07 11:02 PM (16 years, 6 months ago)

I followed this tek loosely, infact very loosely. Im never one for measuring thing, caustic soda poured straight from the tub into a glass jar, water guestimated, bark added, stirred and left sit for a while (maybe 10 hours or so).

Used shellite as my solvent, again, straight from the container no measurement, stirred and let sit for another 3 or 4 hours.

let evap, and now how maybe half a gram of light yellow waxy DMT.

this was from only about 100g of bark too, cut into smaller pieces but not powdered. through a tiny bit in the pipe to check, yep, thats DMT.

Got to clean it up alittle, as this was just really a test run, but i am extremely happy with the results, and the ease of use of this tek.

When i order my next batch of bark, i will do a total dummies guide with pictures on the entire process.

Thanks for all the help, now off to turn this into sexy crystals!


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OfflineMYSTIQUE
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: The_Kman]
    #7185859 - 07/16/07 11:13 PM (16 years, 6 months ago)

Is this something that if it worries me to do it I probably shouldn't like making acid or am I cool just being a hobbyist with no college in chemistry just what Iv seen in books and tried out myself? Like I guess If I get the separation of the two layers right and give it enough time to dry I should be fine? BTW I cant fine any lye in Canada where I live I checked out local soap supply stores and the closest one is 6 hours away that has it. They stopped selling the red devil kind and that one with the lion on it that starts with a B. They have huge ass trains full of it down at the docks my friend burnt his leg on it pretty bad maybe I can go grab some of that lol. Is there anything else I can Use as a base?


--------------------
Dont know what the fuck I just said? READ THIS
http://www.shroomery.org/5122/The-Shroomery-Mushroom-Glossary
I ain't a hippy but I'm covered in dirt                         
Sippin lots of mushroom tea in a tye-dye shirt
Chasin' the Grateful Dead, no shoes on my feet
Beggin' in the parking lot for something to eat,

:onfire:DO NOT USE FIRE IN YOUR GLOVE BOX!!!!!!!:onfire:


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Offlineenesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: MYSTIQUE]
    #7186811 - 07/17/07 05:55 AM (16 years, 6 months ago)

Quote:

MYSTIQUE said:
Is this something that if it worries me to do it I probably shouldn't like making acid or am I cool just being a hobbyist with no college in chemistry just what Iv seen in books and tried out myself? Like I guess If I get the separation of the two layers right and give it enough time to dry I should be fine? BTW I cant fine any lye in Canada where I live I checked out local soap supply stores and the closest one is 6 hours away that has it. They stopped selling the red devil kind and that one with the lion on it that starts with a B. They have huge ass trains full of it down at the docks my friend burnt his leg on it pretty bad maybe I can go grab some of that lol. Is there anything else I can Use as a base?



It's very simple and only takes a few hours to do. You could always purchse your lye online.


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InvisibleEntersandman
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: enesi]
    #7187447 - 07/17/07 10:18 AM (16 years, 6 months ago)

oh oh oh....what a great and nice tek!
i can“t await to try it!

:mushroom2:


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Offlineeks
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: The_Kman]
    #7233143 - 07/28/07 09:31 AM (16 years, 6 months ago)

Is it safe to 'use' the yellow goo?

Why can't I just put the goo+solvent into the freezer? What happens if I skip the fridge step and put it straight to the freezer?


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Offlineundergrounder
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: eks]
    #7233193 - 07/28/07 09:53 AM (16 years, 6 months ago)

Whatever the goo is, NaOH, fats, other alkaloids you won't die from trying to smoke it but its not pure or even semi-pure DMT which is the only thing worth smoking.

I tried that, the goo froze solid in the freezer, crystals never formed.


--------------------
:igor: RIP :igor:

Bigger and bolder and rougher and tougher in other words sucka there is no other...
:pinkshroom: :supershroom: :mushroom2: :shroomer: :mushroom2: :supershroom: :pinkshroom:


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Offlineshirley knott
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: enesi]
    #7233667 - 07/28/07 01:06 PM (16 years, 6 months ago)

Quote:




man i'm so jealous :thumbup:

maybe someone can help me explain this - my lovely vial of white matter (actually, about half of this amount) turned itself into this vial of yellow goop-




--------------------
buh


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Offlineundergrounder
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: shirley knott]
    #7233811 - 07/28/07 01:47 PM (16 years, 6 months ago)

!!!

You've got me worried about my lovely vial of not-so-white crystals now.

That's weird.


--------------------
:igor: RIP :igor:

Bigger and bolder and rougher and tougher in other words sucka there is no other...
:pinkshroom: :supershroom: :mushroom2: :shroomer: :mushroom2: :supershroom: :pinkshroom:


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