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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: darklcd] 1
#6958019 - 05/23/07 06:31 PM (16 years, 8 months ago) |
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So would grinding the bark into powder first, make a large difference? Seems like an easy and quick step to do, and no mushy bark mess to work with.
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: coAsTal]
#7066380 - 06/19/07 04:32 PM (16 years, 7 months ago) |
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I would not suggest using the lye from ACE hardware. It's about 30 dollars for a one lb container.
Froogle search "rooto lye" you'll find it for a LOT cheaper (3-5 bucks per container) This has replaced the red devil brand at ACE.
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: coAsTal]
#7104804 - 06/28/07 08:10 PM (16 years, 7 months ago) |
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I have a question about washing. In this tek i have (not sure what it's called) It says after you have your crystals, to wash with chilled ammonia (janitor strength non sudsy) I did this, and my crystals melted and turned dark. What happened?
here are pictures of my finished product prior to washing. I was stoked about getting these looking this nice, only to lose them all to a dark colored gunk.


Also a question about the cold freeze cycle, what's the best way to do that? To get the crystal shown above, i just removed my naptha layer after a 3hour seperation period, put it in a glass pan and stuck it in the freezer, by morning i had a pan full of crystals.
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: shirley knott]
#7107456 - 06/29/07 02:19 PM (16 years, 6 months ago) |
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Quote:
shirley knott said: don't throw away that gunk, redissolve it in fresh naphtha. i think you probably removed a bunch of crap from your elfspice but at the same time melted it - mebbe you warmed it up?
in my multiple steps at purification, i kept freezing and getting orangey crap come out of solution. by gentle warming followed by holding the sealed jar under hot running water to heat it up, i was able to remove a load of dark orange crap and repeat.
if you're not absolutely sure, you'll lose nothing by redissolving, heating, shaking and letting gravity collect the crap.
I let it dry out, but it was still ugly. I was reading on the dmt nexus forum about recrystallization, so i gave it a shot. I dissolved a gram into some naptha, let my glass container sit in a bowl of hot water until it all dissolved, poured off the clear solvent then i let it cool to room temp, Now i guess do a cool freeze cycle a few times and i'll be good. it looks much better now.
Here is the "brown sugar" i ended up with after ammonia wash.

And after dissolving in heated solvent, and then left to cool to room temp overnight, this is what i awoke to.

btw, this is kinda fun! lol.
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: shirley knott]
#7107896 - 06/29/07 03:59 PM (16 years, 6 months ago) |
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I got them going in the cool freeze cycle now. Although i work 6-7 hours a day, so my timeframes are a bit longer.
and yea, it's some amazing stuff alright, lol. Like an entire mushroom peak packed into 5 minutes, lol.
I like listening to sphongle, tales of the inexpressible, track #3 (a new way to say hooray) The music just seems to set the pace for the trip, everything that happened was right in beat with the tunes. very cool.
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: Knoa6]
#7114392 - 07/01/07 08:40 AM (16 years, 6 months ago) |
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Done with the CFC, here is the finished product. It was super easy to get these, if you are doing dmt extractions and not getting nice crystals like this, you need to check your approach, it's just too easy!
Mine aren't super pure or anything, but it's a lot nicer then some orange/brown goo, lol
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: coAsTal]
#7114999 - 07/01/07 01:29 PM (16 years, 6 months ago) |
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Quote:
coAsTal said: That is some grade-a fucking gorgeous spice brother!!!
     for you
Thanks man, I actually followed the marsfold tek, but i took a few tips from this one we are posting in.
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: shirley knott] 1
#7115251 - 07/01/07 02:45 PM (16 years, 6 months ago) |
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The photo above, still wet with solvent
Here is ONE completely dry crystal, about the size of a dime
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: The_Kman]
#7180305 - 07/15/07 06:38 PM (16 years, 6 months ago) |
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Quote:
The_Kman said: Im currently having a go at my first ever DMT extraction using this method. Ill let everyone know how it goes. did have a half pound of MHRB, but have split that in half to give me two separate runs at it.
Ill see how it goes.
Good luck, be sure to post up your results
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: MYSTIQUE]
#7186811 - 07/17/07 05:55 AM (16 years, 6 months ago) |
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Quote:
MYSTIQUE said: Is this something that if it worries me to do it I probably shouldn't like making acid or am I cool just being a hobbyist with no college in chemistry just what Iv seen in books and tried out myself? Like I guess If I get the separation of the two layers right and give it enough time to dry I should be fine? BTW I cant fine any lye in Canada where I live I checked out local soap supply stores and the closest one is 6 hours away that has it. They stopped selling the red devil kind and that one with the lion on it that starts with a B. They have huge ass trains full of it down at the docks my friend burnt his leg on it pretty bad maybe I can go grab some of that lol. Is there anything else I can Use as a base?
It's very simple and only takes a few hours to do. You could always purchse your lye online.
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: shirley knott]
#7233907 - 07/28/07 02:26 PM (16 years, 6 months ago) |
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was it sitting in a warmer then normal spot? did you freeze precip those? Did you do a defat or any recrystallization steps?
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: shirley knott]
#7234304 - 07/28/07 04:38 PM (16 years, 6 months ago) |
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hmm...i'm not real sure what happened then. how old is it?
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: shirley knott]
#7236825 - 07/29/07 03:37 PM (16 years, 6 months ago) |
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i have no clue, i'd say try to recrystalize it again, and use it soon, lol
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: optyks]
#9172134 - 11/02/08 12:03 PM (15 years, 2 months ago) |
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doesn't look like you got much there^ lol.
and x2 on the yellow color of spice. Evaporation will usually give you a yellow spice, even if you clean it and recrystallize it, the yellow will remain. It doesn't mean you have impurities or poor quality stuff though. Just aesthetic IMO. The gunk you get from recrystallizing is usually a dark orange color, and the spice that dissolves in the hot solvent will maintain an even brighter yellow shade then before cleaning.
(and i've smoked spice ranging from dirty brown last pull stuff, to pure synthetic, the quality does seem to effect the trip. shitty spice=shitty trip, and likewise).
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: SLiCeR] 1
#13943793 - 02/11/11 06:10 AM (12 years, 11 months ago) |
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Man, some of you guys are seemingly making a simple process into a compliated one. Just need to slow down, and follow some tema before trying to alter things.
Here is some work done using simple an extractions with powdered bark (I never use stb with powder)

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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: SLiCeR]
#14008671 - 02/22/11 05:10 PM (12 years, 11 months ago) |
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Either of those should work fine, they are basically a combination of solvents. I've heard varsol may give you some trouble freeze precipitating, so a slow evap may be needed.
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: SLiCeR]
#14008775 - 02/22/11 05:29 PM (12 years, 11 months ago) |
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Can you not find bestine up there? Check art supply and craft shops. They should have it. You could extract with that alone, but it is pretty pricy. Would work great to recrystallize with though.
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: SLiCeR]
#14013305 - 02/23/11 12:39 PM (12 years, 11 months ago) |
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Suggest you use 2x the h20/lye solution than recommended for powdered bark. If you get an emulsion layer and have problem with the solvent separating, you just add more water
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: SLiCeR]
#14013750 - 02/23/11 01:54 PM (12 years, 11 months ago) |
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It should be basic water, so add lye. Otherwise you will lower the ph level
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enesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: fbi365]
#14026529 - 02/25/11 05:06 PM (12 years, 10 months ago) |
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Yes, it works great, buts its way expensive compared to naphtha. You are fine off with extracting with naphtha and cleaning with the bestine
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