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Offlineshirley knott
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: coAsTal]
    #7060887 - 06/18/07 10:36 AM (16 years, 7 months ago)

this explains why my lovely white-yellow extract melted in a warm room:




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buh


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Offlineenesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: coAsTal]
    #7104804 - 06/28/07 08:10 PM (16 years, 7 months ago)

I have a question about washing. In this tek i have (not sure what it's called) It says after you have your crystals, to wash with chilled ammonia (janitor strength non sudsy) I did this, and my crystals melted and turned dark. What happened?

here are pictures of my finished product prior to washing. I was stoked about getting these looking this nice, only to lose them all to a dark colored gunk.





Also a question about the cold freeze cycle, what's the best way to do that? To get the crystal shown above, i just removed my naptha layer after a 3hour seperation period, put it in a glass pan and stuck it in the freezer, by morning i had a pan full of crystals.


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Offlineenesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: shirley knott]
    #7107456 - 06/29/07 02:19 PM (16 years, 6 months ago)

Quote:

shirley knott said:
don't throw away that gunk, redissolve it in fresh naphtha. i think you probably removed a bunch of crap from your elfspice but at the same time melted it - mebbe you warmed it up?

in my multiple steps at purification, i kept freezing and getting orangey crap come out of solution. by gentle warming followed by holding the sealed jar under hot running water to heat it up, i was able to remove a load of dark orange crap and repeat.

if you're not absolutely sure, you'll lose nothing by redissolving, heating, shaking and letting gravity collect the crap.




I let it dry out, but it was still ugly. I was reading on the dmt nexus forum about recrystallization, so i gave it a shot. I dissolved a gram into some naptha, let my glass container sit in a bowl of hot water until it all dissolved, poured off the clear solvent then i let it cool to room temp, Now i guess do a cool freeze cycle a few times and i'll be good. it looks much better now.


Here is the "brown sugar" i ended up with after ammonia wash.



And after dissolving in heated solvent, and then left to cool to room temp overnight, this is what i awoke to.




btw, this is kinda fun! lol.


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Offlineshirley knott
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: enesi]
    #7107546 - 06/29/07 02:45 PM (16 years, 6 months ago)

Quote:

I dissolved a gram into some naptha, let my glass container sit in a bowl of hot water until it all dissolved, poured off the clear solvent then i let it cool to room temp


well the DMT nexus sounds like it should know what's going on. same deal as i described, but cleaner and much easier method.

those crystals look way cool, try the 3h fridge/3h freezer/repeat method to see how big they can go. you tried smoking it yet? you won't be disappointed.



--------------------
buh


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Offlineenesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: Knoa6]
    #7114392 - 07/01/07 08:40 AM (16 years, 6 months ago)

Done with the CFC, here is the finished product. It was super easy to get these, if you are doing dmt extractions and not getting nice crystals like this, you need to check your approach, it's just too easy!

Mine aren't super pure or anything, but it's a lot nicer then some orange/brown goo, lol



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Offlineshirley knott
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: enesi]
    #7115220 - 07/01/07 02:33 PM (16 years, 6 months ago)

Quote:

enesi said:


holy shit :crazy2:


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buh


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Offlineenesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: shirley knott] * 1
    #7115251 - 07/01/07 02:45 PM (16 years, 6 months ago)

The photo above, still wet with solvent

Here is ONE completely dry crystal, about the size of a dime


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Offlineshirley knott
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: enesi]
    #7233667 - 07/28/07 01:06 PM (16 years, 6 months ago)

Quote:




man i'm so jealous :thumbup:

maybe someone can help me explain this - my lovely vial of white matter (actually, about half of this amount) turned itself into this vial of yellow goop-




--------------------
buh


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Offlineoptyks
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: darklcd]
    #9159637 - 10/30/08 03:11 PM (15 years, 2 months ago)

I started this tek today! Though I only had 56 g of MHRB, so I used 50 of it and divided everything else by 10. Right now the MHRB powder is chillin in the lye solution, its all brown and mucky lookin.

heres a pic.


Question though. I thought my digital postal scale was pretty accurate, but now i'm kind of questioning it... what would be the worst case scenario if I got too much/too little lye and/or too much bark/not enough bark?

ANywya, Ill let you know how it goes!


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Offlineoptyks
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: optyks]
    #9170112 - 11/01/08 09:33 PM (15 years, 2 months ago)

Well, found a bunch of crystals in a container tonight. I have no idea how dense the stuff is so I have no idea an approximate mass but heres a pic compared to a jelly bean



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Offlinepiracetam
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: optyks]
    #9654471 - 01/21/09 07:20 PM (15 years, 9 days ago)



--------------------
"Experiments are the only means of attaining knowledge at our disposal. The rest is just poetry, imagination." ~Max Planck


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Offlineoptyks
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: SurReality]
    #9673109 - 01/24/09 08:22 PM (15 years, 6 days ago)

Excellent. I was pretty unorthodox with this most recent little process, merely eyeballing everything, every ingredient that I added. Sure sure, slap me on the wrist. It seemed to have turned out pretty well. This is the first real pull off maybe 30 or 40 grams MHRB.

:awesome:


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Offlineticklemonster4u
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: optyks]
    #10038329 - 03/25/09 11:37 AM (14 years, 10 months ago)

Ok, well we did a heat bath and a 20 minute extraction just to see if it made a difference and it gave us this


I'm guessing a longer bath will give us more?


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Offlinebirdisaword
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: Dr.Myco87]
    #10039129 - 03/25/09 02:14 PM (14 years, 10 months ago)

Do smaller batches for greater efficiency...





Edited by birdisaword (03/25/09 02:17 PM)


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Offlinehoodbran
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: tektonic]
    #10087145 - 04/01/09 01:12 PM (14 years, 9 months ago)

Quote:

tektonic said:
did the bark turn black from the lye?
it should look like black sludge if there is enough lye
and naptha has a hard time pulling anything if it's cold




This is my second time at a DMT extraction, here's the result of my first using this tek: (note the coin is the weight +1g)



The spice weighed in at a nice 1.0g from 50 finely powdered MHRB.

Thanks to Entropymancer for your knowledge on this!

In the quote above, using a warm solution for pulling, I heated up my basified water / mimosa mix in a warm bath for ~15 minutes and then added the naptha (in my case zippo fluid) - which according to plenty of research is naptha.. hey it worked last time! see results above:)

I plan on doing the same tonight, do you think warming up the entire mix this way is the same as warming up the naptha?


--------------------
Not all drugs are good, Some are great.





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Offlinehoodbran
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: Nature Boy]
    #10092652 - 04/02/09 07:14 AM (14 years, 9 months ago)

This guy's friendly alien went From this (1 hour in):



To this:



in 18 hours using the CFC method, reclaimed nps for another extract! Wooo!!

Btw, used ~ 125g MHRB.
--
Trip Report: Afternoon of DMT and falling in Love


Edited by TerryTibbs (04/02/09 04:05 PM)


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Offlinehoodbran
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: UK Explorer]
    #13003114 - 08/04/10 06:28 PM (13 years, 5 months ago)

naptha can be found sold as zippo brand fuel (not ronsonol) at timpsons £2.49 a can, get 3 cans... heres my extracts using this, but you need to do a STB tek with such limited options.  Going to chemical distributors will  only cause you a headache! - if you are careful you can reuse the naptha time after time.



--------------------
Not all drugs are good, Some are great.





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InvisibleRobMarley420
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: Snoogansflip]
    #13869940 - 01/29/11 08:29 AM (13 years, 1 day ago)

Extracted this DMT using this tek.

The stuff in the jar is the 2nd pull after freeze precip.

The stuff on the mirror is the 3rd pull before freeze precip.



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Offlineenesi
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: SLiCeR] * 1
    #13943793 - 02/11/11 06:10 AM (12 years, 11 months ago)

Man, some of you guys are seemingly making a simple process into a compliated one. Just need to slow down, and follow some tema before trying to alter things.

Here is some work done using simple an extractions with powdered bark (I never use stb with powder)





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OfflineMr E Guest
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Re: DMT extraction...rootbark to smokeable in roughly 3-4 hours...no grinding, powdering, freezing, [Re: SLiCeR]
    #14014253 - 02/23/11 03:00 PM (12 years, 11 months ago)

Screw naphtha its...

the *water only* tek!
  • Make hot mimosa tea using tap water.
  • Filter out all solids.
  • Add lye.
  • Put aside in a warm place for a couple of hours.
  • Transfer to fridge for 3 or 4 days.
  • Collect DMT freebase from surface of liquid.
  • Rinse with tepid water.
  • Purify using solvent of your choice. Or vacuum sublimation.

A picture of what should (or might) happen after adding the lye:

Credit: Dagger, of the Nexus

Sorry, no quantities, that'll have to be your homework!

Edit: water rinse added.


Edited by Mr E Guest (02/27/11 05:54 AM)


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