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OfflineShroomyTunes
psychedeliac

Registered: 07/10/04
Posts: 686
Loc: Ontario
Last seen: 10 years, 3 months
How to: Syrian Rue Extraction
    #5596686 - 05/06/06 01:14 AM (17 years, 8 months ago)

Hey,
Does anyone know how, or have a link to, making a syrian rue extraction to close to pure harmala?
thanks alot
ST


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Offlinestefan
work in progress

Registered: 04/11/01
Posts: 8,932
Loc: The Netherlands
Last seen: 3 years, 3 months
Re: How to: Syrian Rue Extraction [Re: ShroomyTunes]
    #5596938 - 05/06/06 03:57 AM (17 years, 8 months ago)



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InvisibleMezcal
Registered: 08/11/05
Posts: 1,980
Re: How to: Syrian Rue Extraction [Re: ShroomyTunes]
    #5597243 - 05/06/06 09:12 AM (17 years, 8 months ago)

I was looking for an opportunity to post this...


Take syrian rue seeds, put in coffee grinder


Grind until it reaches a fine consistency


Add water


Note the UV reactivity (yellow green tint)


Add NaOH


Filter and add aqueous solution to separatory funnel


Add nonpolar solvent, allow to mix well, then do several basic h20 washes to remove water soluble impurities


Salt out the alkaloids with dilute HCl and collect the aqueous product

Evaporate, scrape up, weigh, dose, enjoy.


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