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InvisibleDoc_T
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: 2jew4u]
    #14574191 - 06/07/11 09:19 PM (11 years, 7 months ago)

Quote:

2jew4u said:
But 2 is completely doable?




I believe it is. Never tried it, but it should be just fine.


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OfflineSomeGuy
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: Doc_T]
    #14574225 - 06/07/11 09:27 PM (11 years, 7 months ago)

Quote:

Doc_T said:
Quote:

2jew4u said:
But 2 is completely doable?




I believe it is. Never tried it, but it should be just fine.



I agree, the MOST you could hope to get is 25 mg of actives off of 2 grams, and that would easily fit in a ml, it would prob. even stay in solution at room temp.


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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: SomeGuy]
    #14574231 - 06/07/11 09:28 PM (11 years, 7 months ago)

I feel an experiment coming on...


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Offline2jew4u
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: Doc_T]
    #14574440 - 06/07/11 10:19 PM (11 years, 7 months ago)

Ok, so how many Ml of ethanol should be put in the flask- for 30g of mush- Is 100ml fine?  And how long should it be in the Sohxlet  for(is the term reflux?)  then evaporate down to 15ml and that should be 2 grams of concentrated mush to 1 ml right?


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Invisibledrr
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: 2jew4u]
    #14575092 - 06/08/11 12:37 AM (11 years, 7 months ago)

Quote:

2jew4u said:
But 2 is completely doable? like my doses in 2's don't really like odd numbers-



LOL fer reals?

I think you should just challenge yourself and take one single dose of 2.54673 (for example) grams, honestly. You're going to have to get over that superstitious nonsense at some point. Or not I guess. LOL


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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: 2jew4u]
    #14577190 - 06/08/11 07:26 AM (11 years, 7 months ago)

Quote:

2jew4u said:
Ok, so how many Ml of ethanol should be put in the flask- for 30g of mush- Is 100ml fine?  And how long should it be in the Sohxlet  for(is the term reflux?)  then evaporate down to 15ml and that should be 2 grams of concentrated mush to 1 ml right?




My sohxlet holds 20g of dry mushroom powder. You'll need well over 2x the volume of the cup, 250-500 or so. Fill the vessel about 2/3 if you can.
I extract for an hour or so, but I don't know if you need to go that long. It's just fun.
Then reconfigure for solvent recovery with fractionation and a drying tube and get most of the alc off it.
Add fresh solvent if needed to bring final product up to desired volume, 15mL or whatever you like.


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OfflineDollieBizzaree
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: Doc_T]
    #14578833 - 06/08/11 06:25 PM (11 years, 7 months ago)

"wash the residue that adheres to the inside of the glass back into the solution."

can anyone help with exactly what this means?
like use a syringe of everclear and get it off the sides
and redry it?


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see if that dont put some fizz on your bubblegum


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Offline2jew4u
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: DollieBizzaree]
    #14579193 - 06/08/11 08:00 PM (11 years, 7 months ago)

Is it supposed to be a dark goo? Or did it get burned?


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Offlinegornyhuy
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: 2jew4u]
    #14591140 - 06/11/11 12:23 AM (11 years, 7 months ago)

Just finished a sexy 200ml mini-bottle full of ethanol extraction of a full ounce of cubes. (Actually 225 ml if you fill the bottle up to the rim)  It was about 20g of older cubes I had lying around and just over 8 grams of very potent PE mixed together.  Hoping to test it out this weekend... maybe tonight!

I don't have any sexy lab glassware like Doc_T, but hopefully my ghetto grind, heat, shake, soak, filter process works well.  Should be roughly 1.4 grams per 10 mls at this concentration level.


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OfflineSomeGuy
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: gornyhuy]
    #14591251 - 06/11/11 12:51 AM (11 years, 7 months ago)

HELL YA! It'll work. Did you only do one extraction? It hits you WAY faster this way. 15 minutes or less:thumbup:


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InvisibleMoo456
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: kingfish4200]
    #14591374 - 06/11/11 01:20 AM (11 years, 7 months ago)

Don't know if this has been asked, but can this be done with isopropyl alcohol and full evaporation?


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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: Moo456]
    #14591393 - 06/11/11 01:26 AM (11 years, 7 months ago)

not really. Isopropyl alcahol is generally never 100% so what else is in there? water. The alcahol evaporates, leaving the water, which evaporates, but the shelf life of psilocin is so short, it would be ruined by the time it was dry. Thats mt opinion


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Offlinegornyhuy
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: SomeGuy]
    #14595549 - 06/11/11 08:30 PM (11 years, 7 months ago)

Quote:

paducahovoids said:
HELL YA! It'll work. Did you only do one extraction? It hits you WAY faster this way. 15 minutes or less:thumbup:




Sweeet! Didn't try it yet. Wound up vaping MJ and drinking bourbon instead.
IT was an awesome night anyway.

So - I did 2 extractions and then a rinse.  First extraction was almost 2 weeks soaking and shaking many times per day with a shot or two of lemon juice in there too, then a heat/shake at the end.  Second extraction was straight 200 proof ethanol soaked and shaken for a couple days, almost a week.  Then I did a quick soak and rinse in more ethanol just enough to kind of rinse the mush and squeeze out anything that was left.

I ran the liquid through a tight gold mesh coffee filter several times, and then ran that through a t-shirt.  It is almost entirely liquid, though there is a tiny bit of "dust" sediment in there. Its also a rich burgundy goldish color and it glows under black light.

I have high hopes!


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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: gornyhuy]
    #14596679 - 06/12/11 12:56 AM (11 years, 7 months ago)

Quote:

gornyhuy said:
it glows under black light.





ZOMG! :mushroom2:


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Offlinemetall
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: Doc_T]
    #14596762 - 06/12/11 01:18 AM (11 years, 7 months ago)

i have read some things saying black light is bad for psilo some saying good what is it :P


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Offlinek00laid
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: metall]
    #14597522 - 06/12/11 04:24 AM (11 years, 7 months ago)

we dont know


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OfflineSomeGuy
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: k00laid]
    #14597545 - 06/12/11 04:31 AM (11 years, 7 months ago)

well, there is no way it could be GOOD. Could it be bad? who knows


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InvisibleMoo456
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: k00laid]
    #14597550 - 06/12/11 04:32 AM (11 years, 7 months ago)

Hmm, what is that actual advantage to this over mushroom tea? Is it really worth wasting everclear?


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OfflineSomeGuy
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: Moo456]
    #14597557 - 06/12/11 04:34 AM (11 years, 7 months ago)

It evaporates faster. Easy concentration for powerful doses. Search for "wok-still" it is a super simple device that would allow you to recoer the everclear


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InvisibleMoo456
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Re: ALCOHOL EXTRACTION OF PSILOCYBIN [Re: SomeGuy]
    #14597601 - 06/12/11 04:44 AM (11 years, 7 months ago)

Ehh, mushrooms are already such an easy drug for me to consume. May as well save the everclear for a mescaline tincture.


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