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OfflineMuppet69_420
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High Quality Extraction
    #4573416 - 08/24/05 01:41 AM (12 years, 3 months ago)

I'm currently making a 73.7g salvia extract. I was wondering if anyone likes the way I did it. Im following Salvinorum or another users guide.

I currently put 73.7g in a beaker with acetone that covered the leaves entirely. I stirred three times for three minutes ( I poured the acetone off three times into a flat oval plate, which is medium in size.) The liquid was very green and once I finaly poured the third batch of acetone off I let the leaves get a little less wet but still very wet. I then poured the leaves into the oval shaped plate full of acetone and salvinorum? I then sealed the top with a non sticky aluminum foil. I then placed the huge batch into the fridge not freezer and will let it stay there for 12-24 hours so all the tannin sediments settle out in the fluid.

Ok thats where im at so far Im wondering if im doing everything right and if it will evaporate etc.


--------------------
Quote:

I live to learn and learn to live.

forget w/e was here b4 it was meth gibberish.... :meff: :rail2: :rail: ....thats as old as my account...

On that note fart in public and grin. :publicfart:

Hail Shroomery!




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OfflineMuppet69_420
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Re: High Quality Extraction [Re: Muppet69_420]
    #4574730 - 08/24/05 02:17 PM (12 years, 3 months ago)

I need to know if putting the oval shape plate full of acetone and salvinorum with leaves in it in the fridge is ok and not to cold (It says put in a cool area thats dark and so acetone will evaporate slowly. Im using 73.7g of salvia crushed n powdered. I know the fridge is cold and dark am I doing this right?).


--------------------
Quote:

I live to learn and learn to live.

forget w/e was here b4 it was meth gibberish.... :meff: :rail2: :rail: ....thats as old as my account...

On that note fart in public and grin. :publicfart:

Hail Shroomery!




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Invisibleredgreenvines
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Re: High Quality Extraction [Re: Muppet69_420]
    #4575671 - 08/24/05 07:05 PM (12 years, 2 months ago)

just put it in a ventilated area without sunlight.
the fridge is too small and the fumes will be bad for everything


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OfflineMuppet69_420
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Re: High Quality Extraction [Re: redgreenvines]
    #4575876 - 08/24/05 08:00 PM (12 years, 2 months ago)

Since I didnt get a reply soon enough I already used fridge ( let it set in there for good 13-15 hours) and I ate some stew I made with potatoes in it.... I drank alot of water, I hope ill be fine..... I also poured off and evaporated it removed brown tannins (crude salvinorum). Im now putting it in oven at 150 F. (all solvent has been previously evaporated and no hint of solvent left) hopefully it will dry soon. Then after I dry it I will dissolve it in Iso. 99% Alcohol so I can purify it. I could also wash it in water before doing that to further purify it.


--------------------
Quote:

I live to learn and learn to live.

forget w/e was here b4 it was meth gibberish.... :meff: :rail2: :rail: ....thats as old as my account...

On that note fart in public and grin. :publicfart:

Hail Shroomery!




Edited by Savako (08/24/05 08:02 PM)


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OfflineMuppet69_420
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Re: High Quality Extraction [Re: Muppet69_420]
    #4575945 - 08/24/05 08:17 PM (12 years, 2 months ago)

I had left my leaves in the whole time even after evaporation.. I mnow drying them in oven at 150 F with all solvenmt evaporated except a little bit of water. Will this still be ok with leaves and everything?

1. Let it sit in firdge for 13-15 hours.

2. Poured off into another oval bowl.

3. I seperated crude salvinorum with coffe filters.

4. Let evaporate (with a little bit of the leaves from the extraction not even half of what is left).

5. Put it into the oven at 150 F. to dry off leaves and extract.

Anything further is what I will be doing after oven drying.

6*. I will remove dried leaves and scrap bowl of waxy liquids, and then put all dried leaves into bowl and powder if any.

7*. I will pour Iso. Alcohol 99% into the evaporation bowl (with leaves) and finely move it around erasing the clumps and such to purify it.

8*. I will add water or more Iso. Alcohol 99% to furthe rpurify the extract and leaves?

Will there be any chance of this working and still getting high quality extract?


--------------------
Quote:

I live to learn and learn to live.

forget w/e was here b4 it was meth gibberish.... :meff: :rail2: :rail: ....thats as old as my account...

On that note fart in public and grin. :publicfart:

Hail Shroomery!




Edited by Savako (08/24/05 08:18 PM)


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OfflineSucellos
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Re: High Quality Extraction [Re: Muppet69_420]
    #4576274 - 08/24/05 09:31 PM (12 years, 2 months ago)

you wanted to bring the acetone's temperature to its lowest point before you pour it on the leaves because the tannins and all the shit you don't want is less soluble in the cold acetone. Thearea you had it evaporating in had very little air flow. A better idea would be to put it in a dark room with a fan over th surface.


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OfflineMuppet69_420
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Re: High Quality Extraction [Re: Sucellos]
    #4576367 - 08/24/05 10:08 PM (12 years, 2 months ago)

I know a fan would be abetter but I dont have a fant outside only in my house and I wont evaporate acetone in my house. I couldve used fan outside in the dark but thought fridge would be better.

I also just took out the dried leaves in the oven. I took about 2-4 grams aside for my smoking pleasure if this cleaning method im using dont work.

Im going to pour Iso. Alcohol 99% 2oz instead of 4oz because this isnt Naptha its Iso. Alcohol 99%. I stirred the leaves before putting them in the Alcohol and made sure any fine powder didnt have clumps.

I stirred the leaves and Alcohol for 2 minutes and iam now leaving it
to sit for an houre or more. I will repeat this as many times needed till the color of the leaf or extract doesnt change. I might do further purification if all goes well if not then I doubt i'll do anything more.


THE QUESTIONS

1. With the leaves being with the extract will I still be able to get any purification of salvinorum?

2. The 2-4 grams of finely crushed leaves I took out before adding Alcohol for purification has small glittering specs. The last batch of 5x I made didnt have these glittering specs. Does this mean the leaves are more potent because of the glittering specs? I'm thinking those are crystals.

3. Would it have been possible due to slow evaporation and being put in the fridge to chill over night have anything to do with having crystals( glittering specs)? Could it be possible that this isnt 5x leaf instead 10x or perhaps more because of the glittering specs on the finely crushed leaves.


--------------------
Quote:

I live to learn and learn to live.

forget w/e was here b4 it was meth gibberish.... :meff: :rail2: :rail: ....thats as old as my account...

On that note fart in public and grin. :publicfart:

Hail Shroomery!




Post Extras: Print Post  Remind Me! Notify Moderator
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Amazon Shop: Lab Glassware, Salvia

Mushrooms, Mycology and Psychedelics >> The Psychedelic Experience

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