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looks like you pulled tannins with (not uncommon)all you really need to do is recrystalize...i use hot (almost boiling) naptha and my freezer to precipitate the crystals out...you will lose a little, but it will pull some a lot of the gak with it be careful
Have you measured what temperature your almost boiling naptha is? My friend has only been heating naptha up to around 45C, but figures he has a bunch more room. Freeze seperation still works, but it seems like there's a lot of room for improvement there.