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Botanerd
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HorrorFrank's PickleJar lasagna TEK - easy STB DMT extraction by me :)
#26974000 - 10/07/20 03:10 PM (3 years, 3 months ago) |
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Hey yall, I made a quick and dirty little DMT extraction TEK that is very easy with high yields. I made it mostly for myself but I was like why not share it here. Hope this is useful to someone  HorrorFrank's PickleJar TEK
Edited by Botanerd (10/09/20 08:06 AM)
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MentalPariah
Pariah of my mind


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Re: HorrorFrank's PickleJar lasagna TEK - easiest STB DMT extraction [Re: Botanerd]
#26974224 - 10/07/20 05:32 PM (3 years, 3 months ago) |
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I really appreciate how "official" you made this document, it satisfies the inner scientist. I have no experience with dmt extraction but just wanted to compliment the well thought out and designed layout.
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Botanerd
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Re: HorrorFrank's PickleJar lasagna TEK - easiest STB DMT extraction [Re: MentalPariah]
#26974242 - 10/07/20 05:46 PM (3 years, 3 months ago) |
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Thanks, I am a biochem student in my second year of uni so that was kind of what I was going for. Having a clear layout like this makes a lot more sense then a wall of text like some TEK's seem to be hahaha I am by no means an expert but this is how I personally do it so yea, pretty handy and it works Edit: and honestly being able to name this PickleJar lasagna TEK made it worth it to type it out LOL
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Edited by Botanerd (10/07/20 05:50 PM)
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Typerwritermonky
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Re: HorrorFrank's PickleJar lasagna TEK - easiest STB DMT extraction [Re: Botanerd]
#26974271 - 10/07/20 06:06 PM (3 years, 3 months ago) |
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What is the product yielded looking like off the back? Will heptane eventually all evap rather then just turn into an oil?
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Botanerd
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Re: HorrorFrank's PickleJar lasagna TEK - easiest STB DMT extraction [Re: Typerwritermonky]
#26974290 - 10/07/20 06:20 PM (3 years, 3 months ago) |
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Heptane will evaporate fast enough but in my TEK I say to deliberately leave a bit of heptane unevaporated when you see crystals have formed. If you let it all evaporate it will become yellowish and oily so you really want to go and figure out how long you want it to evap for. It all depends on the number of crystals you can see. Sadly my old phone was the only place I ever had pictures of my DMT on and it got destroyed but the closest image I could find to what I had is this https://wiki.dmt-nexus.me/w/images/0/02/Crystals.JPG It really were pure white densely packed crystal formations Hope this helps! The yield I ended up with was about 2.5 grams from the 250 grams of bark but I bet there was still a ton in there. I only had 2 bottles of naptha so I was kind of limited by that but still a good yield. The last evap I did yielded a more yellow product but that was just 10% of the total yield.
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Edited by Botanerd (10/08/20 12:55 PM)
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Typerwritermonky
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Re: HorrorFrank's PickleJar lasagna TEK - easiest STB DMT extraction [Re: Botanerd]
#26974437 - 10/07/20 08:10 PM (3 years, 3 months ago) |
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Id use heptane, use a warm water bath if possible while it's sitting for a few days, and freeze precip.
What I used to do was use those things used to keep food trays warm at buffets that have really warm water and heaters built in. That would be the warm water bath it would sit in all the time. Definitely helped a ton with yield, but made for a dirtier product.
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Botanerd
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Re: HorrorFrank's PickleJar lasagna TEK - easiest STB DMT extraction [Re: Typerwritermonky]
#26974942 - 10/08/20 05:22 AM (3 years, 3 months ago) |
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Oh those heaters do sound like a promising tool for extractions like this. thanks for sharing
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funky123
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Registered: 08/27/17
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Re: HorrorFrank's PickleJar lasagna TEK - easiest STB DMT extraction [Re: Botanerd]
#26975433 - 10/08/20 12:46 PM (3 years, 3 months ago) |
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Quote:
Botanerd said: Heptane will evaporate fast enough but in my TEK I say to deliberately leave a bit of heptane unevaporated when you see crystals have formed. If you let it all evaporate it will become yellowish and oily so you really want to go and figure out how long you want it to evap for. It all depends on the number of crystals you can see.
[...]
The yield I ended up with was about 1.5 grams from the 250 grams of bark but I bet there was still a ton in there. I only had 2 bottles of naptha so I was kind of limited by that but still a good yield. The last evap I did yielded a more yellow product but that was just 10% of the total yield.
Last time I did Cyb's Hybrid Salt Tek I ended up with some brown goo mixed with the crystals. Do you mean to say that I should have been less thorough with evaporating the Naphta to avoid this? Isn't it bad for you to leave Naphta in there and inhale it?
I don't follow with your statement of having extracted 1.5g from 250g of bark. I mean that is ridiculously bad! How is that to be understood?
What was the motivation for this Tek? Is it based on a known Tek and you felt like improving it a little?
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Botanerd
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Re: HorrorFrank's PickleJar lasagna TEK - easiest STB DMT extraction [Re: funky123]
#26975447 - 10/08/20 12:54 PM (3 years, 3 months ago) |
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This is completely based on my personal trial and error doing extractions back in the day. The last bit of naphtha (after you have lots of crystals) should be added back into the jar and topped off again with new naphtha. The oils then migrate back into the jar with the leftover solvent (like you speculated) Then the dish is left to dry completely so yea, no naphtha in the end product. As for the yield. I didn't measure exactly when I got my product back in the day so not even sure if it was 2.5 but it's just my estimate. You could say a 100% yield is always achievable by just continuing to do pulls. In most teks people seem to add a ridiculous amount of NaOH (up to 2M) and yea I felt like this tek could benefit beginners a lot because my solution with the 100g over 3.5l will give a concentration of between 0.7-0.8M well over the needed PH of 13. So basically just my own home-brew method that I find yields white crystals
Oh PS. Just noticed I had typed a yield of 1.5 in that post but I meant to type 2.5 First pull was for sure more than 1 gram
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Edited by Botanerd (10/08/20 04:08 PM)
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Botanerd
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Re: HorrorFrank's PickleJar lasagna TEK - easiest STB DMT extraction [Re: Botanerd]
#26976584 - 10/09/20 07:47 AM (3 years, 3 months ago) |
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Gonna try and extract a kilo of MHRB soon using this tek to the letter. prepping already and sourcing chemicals. Gonna be using heptane as it´s cheapish as fuck so yea. Will post results!
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Edited by Botanerd (10/09/20 07:48 AM)
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Typerwritermonky
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Re: HorrorFrank's PickleJar lasagna TEK - easiest STB DMT extraction [Re: Botanerd]
#26979170 - 10/10/20 09:53 PM (3 years, 3 months ago) |
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1.5g was his first pull, so he'd probably pull 2.5g from 250g. Which is like.. pretty reasonable with 1%.
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Botanerd
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Re: HorrorFrank's PickleJar lasagna TEK - easiest STB DMT extraction [Re: Typerwritermonky]
#26979699 - 10/11/20 09:21 AM (3 years, 3 months ago) |
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Yea, in my TEK the crystalline product is purest in the first pull and gradually turns more yellow. In my recollection, I must have had more than 2 grams of pure white DMT. Sadly I dropped the vial one day and lost a ton :'( When I do my next extraction I plan to do a 1H-NMR and IR spectrogram and maybe a GC analysis if my school gives me access to it. I plan to post the extrapolated results here so people can see if it's pure or not.
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