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Revemu


Registered: 06/24/13
Posts: 151
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First mescaline extract 1
#26954382 - 09/25/20 11:56 AM (3 years, 4 months ago) |
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Hi guys,
I'm asking for some help on my first extraction.
I did an a/b extract on my cacti, then washed it with anhydrous acetone and got 300mg of this brown gooish product. I'm asking whether it's looking okay or not, I have never seen and never consumed mesc. I am curious about dosing it, I have a lot of experience with shrooms (50+ trips) and LSD (4 trip so far). I'm planning on taking it on a party since I don't really want to take pills nor drink or anything else. I am planning to take 100mg of this then keep the other 200 for later with different circumstances.
The pics I have seen on mesc were way cleaner than mine, so I'm curious where my extract gone wrong, so basically I'm just asking if it's 'safe' to take. However I was expecting more from it, but if you guys say it's okay to take this I'm fine with it.

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Pandemoon
Ἧeẍeᾐmeḭsṫeŗ ͛


Registered: 01/28/14 
Posts: 5,844
Loc: Europe
Last seen: 7 hours, 52 minutes
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Re: First mescaline extract [Re: Revemu]
#26954499 - 09/25/20 01:19 PM (3 years, 4 months ago) |
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What exactly did you do? Usually the endproduct from an a/b extraction turns out to be a dry, almost white, powder.
A brown sticky goo is very uncommon.
Also, 100mg won't do anything. Even for 100% pure mescaline this is a slighly above theshold dose. 300 to 400 mg of pure mescaline is a moderate dose comparable to 2.5g of shrooms or 150mics of lsd.
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Revemu


Registered: 06/24/13
Posts: 151
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Re: First mescaline extract [Re: Pandemoon]
#26954517 - 09/25/20 01:37 PM (3 years, 4 months ago) |
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Thanks for the reply,
I started with 30g dried peyote chips crumbled, started boiling with added 20% vinegar, did this 3 times for roughly 1.5hours each boil (Once I almost run out of water when boiling, I think here is my problem). Then added 50g NaOH mixed with 100ml H2O, then xylene, did 3 pull, with fresh xylene each time. Then added 20% HCL (couldn't get cc.HCL, this might be a problem as well?) Then separated the acid-water to a dish and evapped. Lye I used was drain cleaner 
I was thinking my lye was not the best, I used too much vinegar maybe, and not concentrated HCL. These all added up so I got goo. I have to mention I have lab experience I just did it home so not the perfect environment for this. Also have to add while evapping I felt vinegar smell so maybe I used not enough lye? I was unable to check pH, another big mistake... Anything salvageable here? I kept everything, I mean I got the crumbled cacti material as well as the basic solution too in case I fuck up - But I think in basic water it already decomposed.
I know it's not the proper way to do these things, I just really wanted to try myself.
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SpacedX
Stranger

Registered: 07/08/20
Posts: 203
Last seen: 4 months, 14 days
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Re: First mescaline extract [Re: Revemu]
#26969193 - 10/04/20 02:16 PM (3 years, 3 months ago) |
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I have some knowladge of the d-limonene extraction so can offer advice. I don't know the tek you are following so won't comment on that.
The end product when using vinegar as the acid is a brown waxy amber. If fully dried you will see crystals. If not fully dried it will be a sludge much like cannabis oil.
You will need more of this than you expect. One cap (not packed) I weighed at .18g One cap was a very mild trip, almost not noticeable although it was a very pleasant microdose. The end product isn't 100% active so I am guessing that I need five caps to get to the 800mg recommended dose for a decent trip.
If you are starting with Pyote I think you should just eat it. It's rare, precious and much more active than san pedro. Save your extraction teks for san pedro.
If you have an end product then the only way to test it is to eat a little bit and see what happens.
Keep persisting. Mescaline, once separated from the nausea that comes with cactus juice, is lovely. Small doses are also very pleasant.
I would just use the d-limonene tek. It's food safe and simple.
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