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Offlinepepe the frog
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WHOA! I CRYSTALLIZED A TREE!!! * 1
    #26447526 - 01/23/20 02:11 AM (4 years, 6 days ago)


Closeup on one



Edit:forgot other pics


also the bunch crystals look exactly like the acacia flowers!!!!




Or do the flowers look like the bunch crystals? my guess is the flowers formed as a expression of the DMT within. But this is just speculation. I do know my crystal tree looks like a acacia tree and not the other way around......or do I?



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The English biologist, Dawkins , invented the word MEME. Do you all know what a MEME is? It's the smallest unit of an idea. It's like what a gene is to biology, a MEME is to ideology. Our task is to create MEMES.....Shadilay frens


Edited by pepe the frog (01/23/20 04:17 AM)


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OfflinePandemoon
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: pepe the frog]
    #26447846 - 01/23/20 09:20 AM (4 years, 6 days ago)

That "tree" is cool!  :laugh:

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OfflineKorean Jesus
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: Pandemoon]
    #26447859 - 01/23/20 09:30 AM (4 years, 6 days ago)

Those look awesome! Good job.


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:rastamon::getstoned::rastamon:


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OfflineSFS96
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: Korean Jesus]
    #26448028 - 01/23/20 11:34 AM (4 years, 6 days ago)

That’s badass :rockon: what Tek do u use?


--------------------
How I make and preserve tea


Consuming consumes a man That was never a purpose of life To only crave for material joys Is believing the lie - Mellow Mood


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Offlinepepe the frog
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: SFS96]
    #26448384 - 01/23/20 02:49 PM (4 years, 6 days ago)

my own, which I am currently awaiting a sample of bark from a kind soul, of which I will make sure to photo document the steps but the written tek is as follows:

MATERIALS REQD:
-250G ACRB (powdered, or finely shredded)
-Magnetic Stirrer & Stir bar to handle min. of 1L liquid (amazon)
-Distilled H2O
-2 Large pots
-coffee grinder/blender(grinding ACRB)
-Naphtha
-5% acetic acid (distilled white vinegar)
-pyrex pipette (graduated) with hand wheel(IMPORTANT)
-pyrex measuring cup
-1L Pyrex media bottle with gl45 cap (https://www.amazon.com/Pyrex-1399-1000CNEa-M-Bottle-Corning-1000ML/dp/B00QU9BYD2/ref=sr_1_5?keywords=pyrex+1000ml+gl45&qid=1579293743&sr=8-5)
-75G 100% Sodium Hydroxide (lye)
-50G NON IODINIZED SALT (optional)
-Chemical resistant goggles
-chemical resistant gloves
-NIOSH VOC respirator (to protect when gasifying as LYE-->H2O does make caustic fumes
-.001/gram scale (MG)
-Heptane A (bestine) (for re-extractions, if unavailable naphtha will suffice) just use clean naphtha to re-X
-Glad Press N SEAL
-2 pyrex shallow dishes (for crystallization)


TOTAL TIME REQD:
Roughly 24 hours from start to finished, pure smokable spice

PREP
250g acrb
Grind up bark as best you can using blender or coffee grinder (careful of dust explosions I turned my grinder into a hand grenade before)

ACID BOIL
Put bark into large pot (pot A)
Measure 900ml distilled H2O add 100ml 5% acetic acid
add to pot A, the acid solution (1000ml)
Bring pot A (with lid!) to a good steady boil for 1hr 15min, stirring a few times throughout
Be sure to check and make sure it’s not too much heat and you end up boiling all the liquid away!
Strain pot a, into pot b (same size, no lid)
Your 1000ml of acid water should be a deep red color and now roughly 250ml now, this doesn’t have to be exact(just not too little!) 
as you add another 1000ml of acidified, distilled h20 to pot a with your bark you strained simmer pot B to reduce further (but not to quick you don’t want to go to add your next boil only to find you reduced pot b to nothing!!)
Straining and adding as In the previous step until you have 4x1000ml(4000ml) acid boils reduced to a total of 1000ml when combined (250mlx4)
Take the combined boils and further boil until you have roughly 750ml-800ml of DEEP red strongly aromatic liquor

DEFAT
At this point while the acidic solution is hot I do a single defat with 50-75ml naptha removing and discarding this naphtha as it just contains plant oils waxes and fats. If you are in a hurry to finish the acid boils and move on to basing and pulling you can opt to skip the defat, although you will not get as much crystallization on your room temp precipitation, and you will likely end up doing a retraction to clean up the oils and fats at the end anyways. Defatting only takes 5-10 mins and makes it so your first crystals are pure enough to just leave as is (no Rex)

Place this into a 1L Pyrex Jar and place into the freezer(don’t forget about it) or fridge to let the acidic  solution cool completely before proceeding to the next step!


BASIFY
WARNING! Caustic soda(sodium hydroxide) is incredibly dangerous to work with unless proper safety protocols are followed(PPE)?meaning chem resistant gloves AND eye protection. A single drop off base solution in your eye will make you blind!! DONT RISK IT, IT ISNT WORTH IT!

◦ Begin by placing a large stir bar(made to handle 1L liquid at all speeds without spinning out
◦ Place this acidified solution onto your magnetic stirrer, mix on med high before proceeding any further
◦ Once the cooled acidic solution has a good vortex going, weigh out 25g NAOH and begin adding it over 2 minutes direct to the red acid liquor
◦ Repeat the previous step 2 more times, the solution will go grey as dmt will be seen beginning to precipitate as the solution turns black( similar to MHRB just more red-black than purple-black
◦ Go directly to the next section do not take a break!

PULLING/CRYSTALLIZATION

◦ Warm 100ml naptha in a mason jar
◦ With the now basified black-red solution still mixing strongly add the warm naptha slowly 10ml at a time
◦ Turn the mag stir to the highest speed possible before spinning out for 1 hr.
◦ Place the thoroughly mixed naptha base solution in a hot h20 bath to separate
◦ Likely the heavy mixing caused a emulsion(this is Okay!) we want this! Yes I said it! The mag stirrer is your best weapon and when utilized properly can break up any emulsion we can form here during this extraction!
◦ Place based solution back on mag stirrer on low; no vortex should be seen forming on the top layer of naphtha but the lower base fraction should be seen slightly with a vortex but moreso you want it to be rotating at roughly 1 rotation/second.
◦ Once your emulsion is no more ( usually about 45minutes to 1hr depending on how emulsified it was) bump the mixing speed back to max again for 2-3 hours this time.
◦ Repeat like before to break up any emulsion that forms from long and heavy mixings
◦ for the next couple mixings I mixed mine much longer than the first 2 mix/sep the third i mixed on max for 5 hours and the fourth an final mix I did for 7 hours these last two long mixes made large emulsion but the magstir makes easy work of it
◦ Heat a pot of h20 to 75c and pull it off the stove top you had it on (cause ur not using gas right!!??)
◦ Place the thoroughly mixed naptha and aqueous solution/emulsion in the hot water bath from previous step!  Wait 10 minutes and check if you can’t see a clearly naptha or aq base layer (emulsion) but it’s close then put the heat back on the mixer on low low no vortex at all just slight circulation of the aq base!
◦ Now after you have mixed/separated a few times for long intervals 2-3hours mixing and you have your nice clear naphtha layer it’s time to precipitate!
◦ This tek uses josh isoms method for this step because it’s unlike any other method I’ve seen and boy George does it work!!
◦ Get a Pyrex baking dish to be the first crystallization pan that’s right we are going to first pull the naphtha off the top with our glass pipette (10ml with hand wheel) being careful to not suck up any black layer!
◦ Next using some press n seal (I prefer this to cellophane befause it’s made of plant cellulose and is bio degradable, as well as makes a much stronger seal than cellophane.) it also holds up better in the freezer!
◦ Now place this dish away from light and any foot traffic for 12 hours. When you return some big ol honking crystals should await! But we aren’t finished!
◦ Next decant your naphtha from around your beautiful crystals, and transfer into a new clean mason jar or dish. Cover with press n seal and place in freezer for 18 hrs you should come back to a gram or so each pull maybe a little more the first few but I didn’t get much maybe 500mg the first few but I don't think I mixed/settled enough on the first pull.

I can’t stress the mag stirrer enough they are only 40$ but they are soooo useful!!
◦ Now repeat pulling until you get nothing in the first room temp precipitation and nothing in the freeze!
◦ Remember to let your spice dry for ~24 hours under a fan near ventilation and away from open flame!!!
◦ Enjoy! I find I don’t need to do a rextraction on anything I room temp crystallize I do it on the freeze stuff cause it’s mostly powder/small crystals and usually I don’t see a need with this method it is 10000x better than any mhrb method! Plus the spice smells and tastes pleasant unlike the plastic bag/shoe smell of mhrb spice!
◦ Enjoy and be tucking careful DMT can pose severe drug interactions! Opiates or Benzos mixed with dmt can result in a blackout and easily lead to vomiting while unconcious! followed by asphyxiation. (I know I had this happen to my best friend while I was trip sitting him, had I not been there to keep him upright he would not be with us today.) If Under the influence of either of these, please, for your or others safety do not dmt period, until you have at least 48-72 hours since last use, it isn’t worth it. Again I’d like to thank josh isom for the inspiration, as well as anyone whos posted something informational or helpful, I am nothing without all of you!
You will end up with more NMT in the freezer stuff. This is okay since NMT is very active and is a wonderful accent to NN DMT!!!

Will be certain to provide corresponding images to each step tomorrow after the goodies arrive. for reference I based this off of Josh ISOMS ACRB tek from the nexus! I basically just adapted it to 1/4 scale since this was my first acrb extract and didn't want to screw something up and all my bark to be gone, when in reality 250g of acrb yielded me 5.5g of pretty pure stuff, some of which made anything I've made using mhrb look filthy with oils and fats, seee these:


--------------------
The English biologist, Dawkins , invented the word MEME. Do you all know what a MEME is? It's the smallest unit of an idea. It's like what a gene is to biology, a MEME is to ideology. Our task is to create MEMES.....Shadilay frens


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OfflinePandemoon
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: pepe the frog]
    #26448621 - 01/23/20 05:12 PM (4 years, 6 days ago)

Your yields seem very good and clean! But that reads like so much work compared to mhrb. :crazy:

With mhrb I get like 1.5% of pure white, or up to 2% of yellow crystals:
https://www.shroomery.org/forums/showflat.php/Number/26442581#26442581

Water, lye, naphtha, salt. And bark of course. Nothing more.
No defat, no boil, no acid. Just soak, stirr, heat up, suck off np, freeze.
Maybe an hour of work, spread over a couple of days for multiple pulls.. :shrug:

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InvisibleBph
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: Pandemoon]
    #26448711 - 01/23/20 05:51 PM (4 years, 6 days ago)

Damn bro. That's some purty crystals you got there.


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OfflineThekd95
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: Bph]
    #26448727 - 01/23/20 05:59 PM (4 years, 6 days ago)

Nice


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Offlinepepe the frog
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: Pandemoon]
    #26448736 - 01/23/20 06:05 PM (4 years, 6 days ago)

Dude my defat if I do I takes 15 min, you get nmt with your normal nn yield. Sure the acid boil is a bit tedious I will give you that but it’s not bad and you are able to do a initial room temp precip that yields the most pure,crystal clear shards much more so than anything I’ve pulled out of MHRB. I understand your initial hesitation but please try it and you will see! Mag stirrer can’t function properly with all the slag mhrb In your reaction vessel


--------------------
The English biologist, Dawkins , invented the word MEME. Do you all know what a MEME is? It's the smallest unit of an idea. It's like what a gene is to biology, a MEME is to ideology. Our task is to create MEMES.....Shadilay frens


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OfflinePandemoon
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: pepe the frog]
    #26448751 - 01/23/20 06:12 PM (4 years, 6 days ago)

I actually have 500g of acrb on hand, for more than a year already. Might give it a try someday.
As I said, your yield looks nice! :thumbup:

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OfflineNature Boy
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: pepe the frog]
    #26448757 - 01/23/20 06:14 PM (4 years, 6 days ago)

Check THESE out from 8 plus years ago.  The last pix is spectacular.  I contributed a pix (on page 3 or 4) but in a fit of paranoia after some buddies got busted, I deleted it.

https://www.shroomery.org/forums/showflat.php/Number/14837230#14837230


--------------------
All submitted posts under this user name are works of pure fiction or outright lies.  Any information, statement, or assertion contained therein should be considered pure unadulterated bullshit.  Note well:  Sorry, but I do not answer PM's unless you are a long-time trusted friend.  If you have a question, ask it in the appropriate thread.

                                                                               


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OfflinePandemoon
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: Nature Boy]
    #26448786 - 01/23/20 06:26 PM (4 years, 6 days ago)

:shocked:

http://www.imagebam.com/image/c13862115577246
http://www.imagebam.com/image/028455115577277


:shockedpussy:


Quote:

From the linked nexus -thread:

We need a new "Diamond Tek". Seriously, this is remarkable information.





Thanks NB. Now I have some threads to read.. :thumbup:

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Offlinepepe the frog
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: Pandemoon]
    #26449030 - 01/23/20 09:27 PM (4 years, 6 days ago)

You just double the portions of materials and add about 30 mins to each acid boil due to increasing the volume. I can’t recommend the magnetic stirrer enough just get a good variety of stir bars I prefer the triangle shape to the standard pill oblong shaped ones. The best part about this tek is the yield from the initial 12hr room temp precipitation then after you decant the naphtha do so into a clean crystallization dish and put into freezer for 18 hours you want to reuse this naphtha for your next pull so you hyper saturate your solvent this builds up over the pulls and eventually you get out the stuff that always seems like you yielded it but you can’t ever seem to get it to not come with the naphtha


--------------------
The English biologist, Dawkins , invented the word MEME. Do you all know what a MEME is? It's the smallest unit of an idea. It's like what a gene is to biology, a MEME is to ideology. Our task is to create MEMES.....Shadilay frens


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OfflineSFS96
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: Nature Boy]
    #26449127 - 01/23/20 10:44 PM (4 years, 5 days ago)

Quote:

Nature Boy said:
Check THESE out from 8 plus years ago.  The last pix is spectacular.  I contributed a pix (on page 3 or 4) but in a fit of paranoia after some buddies got busted, I deleted it.

https://www.shroomery.org/forums/showflat.php/Number/14837230#14837230




That’s kickass. I need to make some I have a kilo of MHRB I bought a while back. One of my buddies made a batch with 100gs of bark but the yield was shit so I think I’ll give it a shot myself next time, I’m not sure I’f he really knows what he’s doing.


--------------------
How I make and preserve tea


Consuming consumes a man That was never a purpose of life To only crave for material joys Is believing the lie - Mellow Mood


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OfflineCosmic Eye
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: SFS96]
    #26450603 - 01/24/20 07:13 PM (4 years, 5 days ago)

It looks fantastic. Its all in the prep!


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Offlineowerfull
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: Cosmic Eye]
    #26452089 - 01/25/20 03:16 PM (4 years, 4 days ago)

Amazing crystals man :heart: Definitely top notch quality.


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Offlinepepe the frog
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Re: WHOA! I CRYSTALLIZED A TREE!!! [Re: owerfull]
    #26470802 - 02/05/20 05:46 PM (3 years, 11 months ago)

Thanks for the complements everyone!!! I think I need to get a clean gallon of naphtha though as my latest 250g extracts aren't yielding crystals like the first few extracts I did (I reused all my NPS its all quite yellow now)


--------------------
The English biologist, Dawkins , invented the word MEME. Do you all know what a MEME is? It's the smallest unit of an idea. It's like what a gene is to biology, a MEME is to ideology. Our task is to create MEMES.....Shadilay frens


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