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OfflineDaoysterking
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DMT extraction * 1
    #26086040 - 07/02/19 11:48 AM (4 years, 10 months ago)

Hey guys, dont know if this is in the right section but here we go, was planning on using a Roto vapor that i just got, has anyone used a roto  vapor to evaporate the solvents and if so what temperature did you use to not oxidize the dmt, looking forward to saving some time instead of freeze precipt.


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OfflineVP123
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Re: DMT extraction [Re: Daoysterking] * 1
    #26086094 - 07/02/19 12:15 PM (4 years, 10 months ago)

I don't know about the stability of DMT. However,  rotovaps usually have the option to purge the system with an inert gas such as N2 or Ar. It won't be cheap but neither are rotovaps. For amines, you want to avoid also their reaction with CO2.

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OfflineBoomerBud
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Re: DMT extraction [Re: VP123]
    #26086286 - 07/02/19 01:43 PM (4 years, 10 months ago)

Not sure what a rotovap is but if you just put your nps in a large dish slightly tilted with a fan blowing over it it will evap pretty quick. Check every so often to tilt the dish slightly more. Evapped down to about 1/5 in an hour last night from about 450 ml solvent.

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InvisibleLizardWizard
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Re: DMT extraction [Re: BoomerBud]
    #26172212 - 09/06/19 09:55 AM (4 years, 8 months ago)

I'm also pretty sure freeze precip is still a chemically more sound way to go since you're not concentrating whatever impurities are left in your NP solvent. But you go and smonk dem heavy metal deemsters boi!


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OfflineLogicaL ChaosM
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Re: DMT extraction [Re: Daoysterking]
    #26191813 - 09/16/19 01:22 PM (4 years, 7 months ago)

That's pretty badass. Only issue is how do you get the DMT out of the flask? Or do you just evap the solvent down to a low level then freeze it?

Not sure the temp but I think DMT burns around 250F.

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Offlinechibiabos
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Re: DMT extraction [Re: BoomerBud]
    #26206952 - 09/24/19 04:01 PM (4 years, 7 months ago)

Quote:

BoomerBud said:
Not sure what a rotovap is but if you just put your nps in a large dish slightly tilted with a fan blowing over it it will evap pretty quick. Check every so often to tilt the dish slightly more. Evapped down to about 1/5 in an hour last night from about 450 ml solvent.



It's basically a machine that helps control evaporation.

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Offlinechibiabos
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Re: DMT extraction [Re: LizardWizard]
    #26207000 - 09/24/19 04:26 PM (4 years, 7 months ago)

Quote:

LizardWizard said:
I'm also pretty sure freeze precip is still a chemically more sound way to go since you're not concentrating whatever impurities are left in your NP solvent. But you go and smonk dem heavy metal deemsters boi!



How do you figure that?  The entire point of either method is to reduce the number of molecules that the solution can hold.  :justdontknow:

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InvisibleLizardWizard
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Re: DMT extraction [Re: chibiabos] * 1
    #26207257 - 09/24/19 06:51 PM (4 years, 7 months ago)

Yes, and both theoretically use lab grade solvents, where as we use construction store grade solvents, so any and all impurities that don't evaporate readily are being concentrated into your final product. That's how I figure. Not Rocket Science. Also, evaporation usually leads to brown wet gunk, where as freeze precip leads to high purity crystals. IIRC there's waxes present in the extract solution as well, which is likely a cause for the brown gunk. People use that stuff to make changa though :shrug:


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