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OfflineAn1cca
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Registered: 10/16/16
Posts: 2
Last seen: 1 year, 9 months
isolation of harmine, harmaline and THH from Syrian Rue the right way...
    #23741610 - 10/16/16 07:33 AM (7 years, 3 months ago)

Hey Guys,

I just ran into this piece of research: https://doi.org/10.5281/zenodo.154442

I thought it might be of interest to some people out here...

Safe journeys!

An1cca


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InvisibleAzuma
I'm a teapot


Registered: 03/10/17
Posts: 108
Re: isolation of harmine, harmaline and THH from Syrian Rue the right way... [Re: An1cca]
    #24173830 - 03/19/17 02:18 AM (6 years, 10 months ago)

Thanks for sharing this! I know this post is relatively old but I still hope you will read this someday. I really like the initiative of the writers. It seems to be a really easy and efficient method.

Have you tried it? I have some very good looking baby Peganum Harmala plants at the moment so this might be a nice thing to do when they start to yield seeds.

Btw, I love the pictures of the crystals!:heart:


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Invisiblesudly
Darwin's stagger


Registered: 01/05/15
Posts: 10,797
Re: isolation of harmine, harmaline and THH from Syrian Rue the right way... [Re: An1cca]
    #24231333 - 04/09/17 09:54 PM (6 years, 9 months ago)

Huehueuhe

Quote:

Results. Using pH-metry for the separation of harmine and harmaline proved rapid, effective and recovered 91% of alkaloids.





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I am whatever Darwin needs me to be.



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InvisibleAzuma
I'm a teapot


Registered: 03/10/17
Posts: 108
Re: isolation of harmine, harmaline and THH from Syrian Rue the right way... [Re: sudly]
    #24239460 - 04/13/17 06:49 AM (6 years, 9 months ago)

What am I looking at? You performed the extraction and separation?


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Invisiblesudly
Darwin's stagger


Registered: 01/05/15
Posts: 10,797
Re: isolation of harmine, harmaline and THH from Syrian Rue the right way... [Re: Azuma]
    #24239488 - 04/13/17 07:10 AM (6 years, 9 months ago)

Close enough, as long as it works ey, plus can be stored as dry pellet.


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I am whatever Darwin needs me to be.



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InvisibleAzuma
I'm a teapot


Registered: 03/10/17
Posts: 108
Re: isolation of harmine, harmaline and THH from Syrian Rue the right way... [Re: sudly]
    #24239497 - 04/13/17 07:18 AM (6 years, 9 months ago)

It looks amazing! :grin:


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OfflineMXDemon
don't worry... b. caapi!
Male


Registered: 04/15/17
Posts: 43
Loc: Florida, USA Flag
Last seen: 6 years, 8 months
Re: isolation of harmine, harmaline and THH from Syrian Rue the right way... [Re: Azuma]
    #24246784 - 04/15/17 03:29 PM (6 years, 9 months ago)

Thanks! I'm trying to learn more about basic chemistry theory and laboratory methodologies as I think its very useful information.


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- Demon


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Offlinedo it
Master of temporary solutions
Male

Registered: 06/01/15
Posts: 151
Loc: Korvatunturi
Last seen: 5 years, 10 months
Re: isolation of harmine, harmaline and THH from Syrian Rue the right way... [Re: MXDemon]
    #24264310 - 04/22/17 03:03 PM (6 years, 9 months ago)

I've seen threads and teks for this stuff on dmt nexus...
I'd say that unless its a microdose, extracting with manske and separating the alks is the way to go. Never tried that reduction since I don't know where to get pure zinc.


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OfflineConnoisseur
Registered: 05/13/11
Posts: 34,686
Last seen: 5 years, 2 months
Re: isolation of harmine, harmaline and THH from Syrian Rue the right way... [Re: An1cca]
    #24358047 - 05/29/17 03:08 AM (6 years, 7 months ago)

i successfully extracted my own harmalas only to find out that my kratom/opiate addiction makes them poisonous to me so i gave them to some friends


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