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Offlinejagarjt
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What are the steps after freezing Naphtha for 24 hrs?
    #22351887 - 10/08/15 08:36 PM (8 years, 3 months ago)

After my first freeze I immediately poured the liquor threw a coffee filter. The coffee filter had yellow goo that won't come out even after being at room temp for hrs. What should I do after freezing naphtha do I let it evap at room temp? Please help :/


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OnlineLogicaL ChaosM
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Re: What are the steps after freezing Naphtha for 24 hrs? [Re: jagarjt]
    #22351931 - 10/08/15 08:44 PM (8 years, 3 months ago)

I never liked the coffee filter technique. seems like a mess and more trouble than necessary.

Its better to freeze then pour into a flat glass pan, and let evaporate in open air outside.

You could try wash the coffee filter with naptha, keep the naptha, then evaporate that in a glass pan :shrug:


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OfflineSupachopped719
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Re: What are the steps after freezing Naphtha for 24 hrs? [Re: LogicaL Chaos]
    #22352047 - 10/08/15 09:09 PM (8 years, 3 months ago)

If you have goo stuck to your coffee filter run warm naphtha through it again but flip the filter so the naphtha goes through from the opposite direction. Evaporate what come through.


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OfflineIcon
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Re: What are the steps after freezing Naphtha for 24 hrs? [Re: Supachopped719]
    #22352098 - 10/08/15 09:22 PM (8 years, 3 months ago)

If you can eliminate vibration and other disruptions during the freezing stage the crystals will be stuck to the glass and you won't need a coffee filter to catch them. Also helps to let the solution crystallize over 2 days, just 24 hours is a little quick. If you're getting goo instead of crystals then there's improvements to be made before the freezing step.

Once you have the crystals stuck to the glass I pour off the naphtha and prop the container upside down in the freezer to drip dry for 10 minutes. Any drops of naphtha touching the crystals when you bring the dish out to room temperature will redissolve your crystals into a goo. Quickly take the dish out of the freezer and prop it upside down in front of a fan. Naphtha will drip away from the crystals and be evaporated. After a couple hours you can set the dish right-side up and let it continue to dry under the fan for at least 12 hours until the naphtha smell is gone.

If you do have to catch crystals with a coffee filter, try to do it in the freezer. Pour your crystal laden naphtha into a funnel with the filter, setup over a jar, and let that filter through while in the freezer. Once it's completely filtered, quickly take the filter out like you would the dish and pin it in front of the fan. Doing any of these steps at room temperature with naphtha in contact with crystals is gonna result in a gooey mess.


Edited by Icon (10/08/15 09:28 PM)


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Offlinejagarjt
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Re: What are the steps after freezing Naphtha for 24 hrs? [Re: Icon]
    #22352134 - 10/08/15 09:28 PM (8 years, 3 months ago)

You guys are awesome man thanks (:


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Offlinejagarjt
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Re: What are the steps after freezing Naphtha for 24 hrs? [Re: jagarjt]
    #22352807 - 10/09/15 12:28 AM (8 years, 3 months ago)

So what's it mean when there's a bunch of white flakes in the naphtha. That it needs frozen longer? That it's going to be a good yield? That it's precipitated as much as it can?


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OfflineBig Worm
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Re: What are the steps after freezing Naphtha for 24 hrs? [Re: jagarjt]
    #22352851 - 10/09/15 12:41 AM (8 years, 3 months ago)

Quote:

jagarjt said:
So what's it mean when there's a bunch of white flakes in the naphtha. That it needs frozen longer? That it's going to be a good yield? That it's precipitated as much as it can?






IME not all crystals will stick to the bottom of the pan during the freeze.

I always have floaters.

But as I pour the naptha off I just wear a glove and put my finger over the corner that i'm pouring to keep them from falling out of the pan.


But it's fairly minimal regardless.  maybe 10-20mg.


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Offlinejagarjt
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Re: What are the steps after freezing Naphtha for 24 hrs? [Re: Big Worm]
    #22371717 - 10/13/15 02:54 AM (8 years, 3 months ago)

After 3 days in freezer and 2 days drying my pan looks greesy on the bottom with see-threw clusters of soft piles of idk what. What did I do wrong? Not enough bark used?


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OnlineLogicaL ChaosM
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Re: What are the steps after freezing Naphtha for 24 hrs? [Re: jagarjt]
    #22373244 - 10/13/15 12:56 PM (8 years, 3 months ago)

Be patient.

It needs more time to evaporate.


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