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Master Roshi
Stranger
Registered: 09/04/15
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What DMT extraction procedure is right for me? (Chemist)
#22190414 - 09/04/15 09:34 PM (8 years, 4 months ago) |
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Swim is a chemist/lab technician. Swim has access to any chemical you can think of and any acid or base. swim owns some of his own glass including separatory funnels.
Swim been having a lot of trouble choosing a procedure and have been putting off ordering bark because of it. Please swim is begging one of you to belp him out here and lead him to a good operating procedure. PLEASE
Swim doesnt need to substitute chemicals but also doesnt want unnecessary steps.
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impatientguy
Ganjalf a very mighty lab wizard



Registered: 11/26/14
Posts: 5,054
Loc: USA
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: Master Roshi]
#22190496 - 09/04/15 09:49 PM (8 years, 4 months ago) |
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Just do a normal lye acid base extraction.
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Mescalitoe
Psychonaut



Registered: 05/14/14
Posts: 584
Loc: California!
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: Master Roshi]
#22190503 - 09/04/15 09:50 PM (8 years, 4 months ago) |
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Head over to the nexus and read up.
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LogicaL Chaos
Ascension Energy & Alien UFOs




Registered: 05/12/07
Posts: 69,360
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: Mescalitoe]
#22190770 - 09/04/15 10:38 PM (8 years, 4 months ago) |
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Quote:
Mescalitoe said: SWIM over to the nexus and read up.
*Fixed.
-------------------- "What you must understand is that your physical dimension affects everyone in the higher dimensions as well. All things are interconnected. All things are One. Therefore, if one dimension is broken or out of balance, then all other dimensions will experience repercussions." - Pleiadian Prophecy 2020 The New Golden Age by James Carwin PROJECT BLUE BOOK ANALYSIS! (312 pages!) | Psychedelics & UFOs | Ready to Contact UFOs? | The Source on Mushrooms | Trippy Gematrix | Dj TeknoLogical | Fentanyl Test Kits R.I.P. Big Worm || The Start of the Ascension Process was 2020. Welcome to the Next Great Era of Earth 🌎🌍🌏
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thewanderer25
Special Karma



Registered: 08/11/13
Posts: 1,642
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: LogicaL Chaos]
#22190873 - 09/04/15 11:12 PM (8 years, 4 months ago) |
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Hey man this is what I do for the premo stuff and if you've got access to hexane it should be easy. Get some acacia confusa root bark powder and freeze it then thaw it 3 times next soak it in a sulfuric acid and distilled water solution make sure the PH is no lower than 1 and no higher than 2 you dont want it super concentrated this will make the alkaloids very soluble in the water but not in NP solvents so add some naptha and then heat it a little bit with a hot plate and a magnetic stir bar this will make some plant fats and other nastiness go into the naptha but since the DMT is so acidic it will stay in the water so get rid of the naphtha layer, just dump it or recycle it via distillation it contains nothing good. Now you can filter the root bark out but make sure the water has had time to absorb everything from the root bark otherwise you will lose product I suggest heating the water, bark, and acid before filtering just to make sure you've got it all out.
Now you have DMT in an acidic solution so slowly add sea salt till the PH is up to about 4 or 5 on the scale make sure to do it slow as you dont want to cause a reaction. Now slowly add sodium hydroxide till it is up to about 13 PH it will then convert the DMT into freebase and you can use naphtha or petroleum ether to get the DMT from the water solution to the petroleum ether solution. Now dry it completely and then add hot hexane till it dissolves completely but use as little hexane as possible then dry it out again this will cause the DMT to join the DMT and the impurities to join the impurities so once it has dried you can add more hexan (not to hot this time) and filter through a filter paper then dry the hexane till its super saturated and freeze it. You should be left with the impurities filtered out or left behind you will get 99% pure DMT crystals it is the best method to use and is easy to do if you've got the gear.
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thewanderer25
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Registered: 08/11/13
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: thewanderer25]
#22190895 - 09/04/15 11:19 PM (8 years, 4 months ago) |
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Also you can use a separatory funnel to get all the naphtha out or use a turky baster but you will find its a lot harder to get the last bit out than a sepratory funnal and here is why you whant to dry it two times
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LogicaL Chaos
Ascension Energy & Alien UFOs




Registered: 05/12/07
Posts: 69,360
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: thewanderer25]
#22190923 - 09/04/15 11:26 PM (8 years, 4 months ago) |
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if u really are a chemist OP, get peterolum ether. Its like naptha, but better and more pure.
Also get reagent grade lye.
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Bugler Boy
Cultivar


Registered: 09/19/11
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: thewanderer25]
#22191820 - 09/05/15 09:01 AM (8 years, 4 months ago) |
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Quote:
thewanderer25 said: Hey man this is what I do for the premo stuff
Weren't you just posting about lye contaminated dmt? ...premo.... 
-------------------- The mushroom speaks: '"I am old, older than thought in your species, which is itself fifty times older than your history. Though I have been on earth for ages I am from the stars. My home is no one planet, for many worlds scattered through the shining disc of the galaxy have conditions which allow my spores an opportunity for life... How the hypercommunication mode operates is a secret which will not be lightly given to man. But the means should be obvious: it is the occurrence of psilocybin and psilocin in the biosynthetic pathways of my living body that opens for me and my symbiots the vision screens to many worlds"
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LogicaL Chaos
Ascension Energy & Alien UFOs




Registered: 05/12/07
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: Bugler Boy]
#22192062 - 09/05/15 10:15 AM (8 years, 4 months ago) |
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I thewanderer half-assed his own extraction method
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thewanderer25
Special Karma



Registered: 08/11/13
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: LogicaL Chaos]
#22192131 - 09/05/15 10:44 AM (8 years, 4 months ago) |
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It was a STB I fucked up on and I was drunk during the pulling faze ive got a bad hangover this morning though and just woke up but just dont drink and make DMT. Im becoming an alcoholic though but its all good.
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impatientguy
Ganjalf a very mighty lab wizard



Registered: 11/26/14
Posts: 5,054
Loc: USA
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: thewanderer25]
#22192486 - 09/05/15 12:35 PM (8 years, 4 months ago) |
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Quote:
thewanderer25 said: Im becoming an alcoholic though but its all good.
Naah don't do that
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LogicaL Chaos
Ascension Energy & Alien UFOs




Registered: 05/12/07
Posts: 69,360
Loc: The Inexpressible...
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: impatientguy]
#22192521 - 09/05/15 12:42 PM (8 years, 4 months ago) |
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Yeah, extractuons should only be done while sober.
Come on wanderer. U should know better When working with dangerous chemicals.
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thewanderer25
Special Karma



Registered: 08/11/13
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: LogicaL Chaos]
#22192549 - 09/05/15 12:48 PM (8 years, 4 months ago) |
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Quote:
LogicaL Chaos said: Yeah, extractuons should only be done while sober.
Come on wanderer. U should know better When working with dangerous chemicals.
Sober me knows that but drunk me just doesn't care. The issue is no matter how much I drink I can still do things im a high functioning drunk I dont do things well though.
But ya I probably should have not drank and extracted. Drinking while extracting increases the risk of accidents 23.2 times over unimpaired extracting. Fixed it was drinking and driving but I think it still counts here
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impatientguy
Ganjalf a very mighty lab wizard



Registered: 11/26/14
Posts: 5,054
Loc: USA
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: thewanderer25]
#22192588 - 09/05/15 01:01 PM (8 years, 4 months ago) |
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Haha yup prolly. I extracted mescaline while on mescaline (a small dose) but it was somthing I won't be doing again.
Lol you get such confidence. It's like crystal alcohol.
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natedawgnow
Rocky mountain hood rat



Registered: 02/09/15
Posts: 8,939
Loc: ation
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: thewanderer25]
#22193728 - 09/05/15 05:35 PM (8 years, 4 months ago) |
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Quote:
thewanderer25 said:
Quote:
LogicaL Chaos said: Yeah, extractuons should only be done while sober.
Come on wanderer. U should know better When working with dangerous chemicals.
Sober me knows that but drunk me just doesn't care. The issue is no matter how much I drink I can still do things im a high functioning drunk I dont do things well though.
But ya I probably should have not drank and extracted. Drinking while extracting increases the risk of accidents 23.2 times over unimpaired extracting. Fixed it was drinking and driving but I think it still counts here 
Aren't you under 21? I don't know how you can be a true alcoholic if you can't even buy booze for yourself.
And ditto on the extraction advice from this guy  Not smoking contaminated product is clandestine chemistry 101 style shit.
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thewanderer25
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: natedawgnow]
#22195126 - 09/05/15 11:31 PM (8 years, 4 months ago) |
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My stuff aint contaminated man my STB was but I was drunk as shit like I am now. I have guys who work at ABC so they sell me whatever I need I buy my own shit and ya im not 21 and never will be at this rate.
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ShroomyBudz
지혜



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Re: What DMT extraction procedure is right for me? (Chemist) [Re: thewanderer25]
#22195221 - 09/06/15 12:01 AM (8 years, 4 months ago) |
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Anyone else think OP might be "swim"?
-------------------- . Explore the unknown! Love forever & always..
me if you ever need anything! I try to check them daily!
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natedawgnow
Rocky mountain hood rat



Registered: 02/09/15
Posts: 8,939
Loc: ation
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: thewanderer25]
#22196869 - 09/06/15 11:46 AM (8 years, 4 months ago) |
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Quote:
thewanderer25 said: My stuff aint contaminated man my STB was but I was drunk as shit like I am now. I have guys who work at ABC so they sell me whatever I need I buy my own shit and ya im not 21 and never will be at this rate.
STB is the easiest extraction tek, so fucking up on that says a lot about your skill level, and smoking the end product of said "fuck up" says even more about your judgement.
Being drunk is a terrible excuse. I have done a lot of extractions while drinking and still don't smoke lye when i know for a fact it's there. Just sayin, man.
Grains of salt and shit.
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openmind
curious


Registered: 08/03/07
Posts: 13,866
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: Master Roshi]
#22197811 - 09/06/15 03:40 PM (8 years, 4 months ago) |
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Quote:
Master Roshi said: Swim is a chemist/lab technician......
.....but you're having difficulty choosing a route for a simple extraction ?
I would have never thought that someone who went to school for chemistry and works as a lab tech would have such problems.
-OM
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ShroomyBudz
지혜



Registered: 05/23/12
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: openmind]
#22198152 - 09/06/15 04:35 PM (8 years, 4 months ago) |
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Quote:
openmind said:
Quote:
Master Roshi said: Swim is a chemist/lab technician......
.....but you're having difficulty choosing a route for a simple extraction ?
I would have never thought that someone who went to school for chemistry and works as a lab tech would have such problems.
-OM
.
-------------------- . Explore the unknown! Love forever & always..
me if you ever need anything! I try to check them daily!
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thewanderer25
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: ShroomyBudz]
#22199540 - 09/06/15 09:08 PM (8 years, 4 months ago) |
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Maybe he is trying to figure our method out. Anyways this is the real way mr.officer
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Master Roshi
Stranger
Registered: 09/04/15
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: thewanderer25]
#22215870 - 09/10/15 08:09 AM (8 years, 4 months ago) |
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Honesty im just not satisfied with the procedures ive seen. I feel like a lot of them are simplified nd use substitute chemicals and lab equiptment. I want to make it easy on swim and find a procedure utilizing the best solvents and lab instruments.
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impatientguy
Ganjalf a very mighty lab wizard



Registered: 11/26/14
Posts: 5,054
Loc: USA
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: Master Roshi]
#22215917 - 09/10/15 08:22 AM (8 years, 4 months ago) |
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Like we all said lye straight to base is how you do it.Quote:
Master Roshi said: Honesty im just not satisfied with the procedures ive seen. I feel like a lot of them are simplified nd use substitute chemicals and lab equiptment. I want to make it easy on swim and find a procedure utilizing the best solvents and lab instruments.
Then make your own procedure because this has worked to get clean crystals for everyone else. Good yeild too if you have a good starting material.
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ONE OZ SLUG
-



Registered: 05/22/13
Posts: 17,839
Loc: TX
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: Master Roshi]
#22215954 - 09/10/15 08:37 AM (8 years, 4 months ago) |
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If you want to get into the really advanced stuff, DMT nexus has a lot of information on that.
A lot of the extraction methods are very simple, only because DMT is illegal and production is mostly clandestine as a result. Not many advances has been made in DMT production because of that. It is up to people like us to experiment and find what's effective and what isn't.
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Master Roshi
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Re: What DMT extraction procedure is right for me? (Chemist) [Re: ONE OZ SLUG]
#22218236 - 09/10/15 06:58 PM (8 years, 4 months ago) |
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Tf is nexus
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