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Invisiblehobowizard
beginner
Registered: 04/10/15
Posts: 192
DMT extraction of phalaris
    #21533657 - 04/11/15 02:50 PM (9 years, 1 month ago)

Has anyone tried extracting DMT from phalaris?

The plant grows p. much everywhere like a weed. http://en.wikipedia.org/wiki/Phalaris_%28plant%29

Anyway, here's how you do it:

  EXTRACTION -

        1.  Pulverize the grass cuttings as much as you can.  You must
            do this to rupture the cellular structure the plant.  A good
            way is to put the plant material in the freezer overnight,
            remove the next day, thaw it, put it in the freezer again, and
            then remove and thaw it again.  After two or three such cycles
            it will usually be mushy and easily minced in a blender.  Place
            the phalaris in the blender when it is frozed and the blender
            will chop it easier.
        2.  Next add enough water to the much to make a pourable soup.
        3.  Now you must add an acid.  Just enough to bring the PH down to
            about 5.  You can use white vinegar, lemon juice, or acetic acid.
            Check the PH with PH paper, it is usually sold at most drug
            stores.  The acid reacts with the alkaloids in the plant
            material and converts them into a salt.  A good way to
            facilitate this reaction is to simmer the acidified soup in a
            slow cooker overnight; leave the lid on, as we don't want any
            liquid to evaporate.
        4.  Strain the plant matter through cheesecloth, then through a
            paper coffee filter.  The bulk roughage may now be discarded
            because the alkaloids we seek have migrated into the aqueous
            solution.
        5.  Add a small percentage of a defatting solvent such as methylene
            chloride, ether, chloroform, or naphtha.  Naptha is easily
            available in the form of Coleman fuel or lighter fluid.  The
            reason we do this procedure is to remove the oils and fats
            which are in the solution - they will migrate into the solvent.
            Shake up the mixture and put it aside long enough to seperate
            into two layers, one aqueous, the other solvent.  If you've ever
            made vinegar and oil salad dressing then you've seen this done.
        6.  A separatory funnel is useful for this next operation.  This is
            a simple lab tool consisting of a tapered glass container
            with a tap at the bottom and a stoppered opening at the top.
            The two liquids are poured in the top (the bottom faucet is
            closed, of course);  The container is corked and shaken about
            to mix its contents.  It is then set aside until the fluids
            seperate into 2 layers.  Then a tap is opened to allow the lower
            stratum to drain into a container.  Just before the descending
            upper fraction reaches the faucet, it is closed off.  You can
            also do the above separation procedure with a turkey baster :smile:
            Discard the solvent (along with the unwanted oils and fats) and
            now the remaining aqueous solution contains the alkaloids.
        7. The next step is to add a base to our solution.  One often used
            in extraction formulas is ammonium hydroxide, a liquid.  If this
            is unobtainable you can substitute regular lye crystals.  This
            is sold as drain cleaner and is also called sodium hydroxide.
            Dissolve this is water to a high concentration.  This fluid is
            added in small increments to the aqueous solution, shaking the
            mixture each time, then testing it until eventually the pH
            reaches 9 or 10.  Be patient.  It usually takes a while to
            get it just right.  Now you have 'unhooked' the salt and
            transformed the alkaloids into their freebase form.  They are
            now no longer a salt, and hence no longer soluble in water...
            So now the are accessable to extraction by one of the organic
            solvents mentioned above.  Using coleman starting fuel is best
            and easy to obtain.
        8. A ratio of 10 percent of the aqueous solution should be enough
            solvent for each extraction.  The easiest way to estimate this
            is to visualize where the 10% line is on your container of
            aqueous solution, then add that amount of solvent to the whole,
            increasing the volume to 110% (A super accurate measurement is
            not necessary)  The container must be kept closed tightly so
            that the solvent won't evaporate from the solution.
        9. Four extractions are made to make SURE that all of the alkaloids
            are removed.  These are done at one 24-hour, and then at three
            weekly intervals.  The solvent layer will soon take on a darker
            tint, usually yellowish or reddish-brown.  This indicates the
            presence of alkaloids as they slowly move out of the aqueous
            solution.  It will take almost a month to get most of them, and
            the mixture should be shaken at least twice a day to ensure
            that all of the alkaloid molecules come into contact with the
            solvent.  At each weekly extraction carefully separate this from
            the aqeous solution be either of the methods mentioned above.
            Save these solvent fractions and combine them in one container.
            each time add fresh solvent to the aqeous solution until the
            extraction series is complete.
        10. The last step is to pour the combined solvent fractions into a
            shallow baking dish or pan and allow it all to evaporate in an
            open space free from flame or sparks.  The residue remaining
            after the evaporation contains the alkaloids, and may be put
            into gelatin capsules.  If it is unduly gummy, one may add
            small amounts of ordinary flour to the gum until it thickens.

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Invisiblemindbodysoul
the fertile


Registered: 03/10/14
Posts: 912
Re: DMT extraction of phalaris [Re: hobowizard]
    #21534711 - 04/11/15 07:47 PM (9 years, 1 month ago)

holy molly brother..thanks... but can u post the ingredients


--------------------

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Invisiblehobowizard
beginner
Registered: 04/10/15
Posts: 192
Re: DMT extraction of phalaris [Re: mindbodysoul]
    #21535873 - 04/12/15 04:28 AM (9 years, 1 month ago)


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