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OfflineHoosle
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DMT extraction for everybody
    #21511864 - 04/06/15 07:21 PM (8 years, 9 months ago)
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Hoosle's Method
*author’s own work

♥ a DIY approach to extraction & conversion of DMT ♥


Preface:

♥Greetings and welcome! If you are finding yourself in possession of this document, chances are that at some point, prior to the present moment, you heard about a compound that possessed properties so fascinating, so wildly unbelievable, that you felt a rush of excitement and wonder most people lose after childhood, never to experience again. This mysterious, fantastical, almost magical compound evoked in you a feeling reminiscent of a child’s exaggerated sense of wonder when those special occasions such as the Christmas holiday, the evening following the loss of a tooth, or anticipation of a special trip to a zoo, theme park, or a visit with grandma were in your imminent future. It is as if that deep, hidden desire for our world to be a magical place that we hide as we grow into adulthood might actually be worth entertaining as a reality on some level. DMT. A simple compound found in an incredible number of different species, both plants and the animals, the most remarkable of which happens to be our species; mankind. 


Ingredients:

♥ 1kg Mimosa Hostilis inner root bark powder
♥ ~4 gallons distilled water
♥ 1 container ~30% Muriatic Acid (Hydrochloric Acid)
♥ 1 can Lye Crystals (caustic soda, Roebic's)
♥ ~1 gallon VM P Naphtha
♥ ~1/2 liter Heptane (Bestine Rubber Cement Thinner)
♥ 1 liter Acetone
♥ ~10 grams Epsom Salts (Magnesium Sulphate)
♥ ~5 grams Fumaric Acid


Supplies:

♥ a couple gallon size milk jugs… HDPE containers, will have a “2” in the triangle of recycle arrows
♥ a few (5-6) 1/2 gallon Mason jars w/ lids & bands
♥ a few (3 or 4) 1 quart Mason jars w/ lids & bands
♥ 2 HDPE funnels ~500mL volume or greater (having more will reduce the time spent filtering)
♥ 2x 1,500mL wine bottles (non-opaque, preferably clear)
♥ 2x HDPE screw-on bottle sport-tops (the kind from a bottle of cleaner or water bottle)
♥ Epoxy quick-set adhesive (the kind found at hardware stores, w/ a heat limit around 300℉)
♥ 3/4" glass drill bit
♥ Power drill (a small cheap one will work)
♥ ~ 14" glass pipette (thin)
♥ 60mL HDPE bulb syringe (HDPE or glass turkey baster will do)
♥ glass eye dropper (found at pharmacy)
♥ 2 or more Borosilicate glass (Pyrex) baking dishes (~6 or more cups volume)
♥ 2 or more glass dishes (glad makes great little pyrex food storage containers)
♥ 2 or martini/wine glasses
♥ Pot for stovetop that can fit 4 quart mason jars or a 1 gallon milk jug
♥ HDPE or glass measuring cups ~ approximately 500mL (for measuring solvents)
♥ Measuring spoons (for measuring lye)
♥ 1 package of 100% cotton 'rounds' (found in cosmetics section of grocery/drug store)
♥ regular toilet paper
♥ pH test strips (both acidic & alkaline)
♥ Paper towels for cleanup and evaporation
♥ Glad wrap
♥ Digital scale (measuring grams to the thousandth place, i.e. mg)
♥ protective equipment, i.e. eyewear, gloves, painter's mask
♥ Stove and oven
♥ Refrigerator/freezer
♥ Portable fan as an evaporation/ventilation aid

I suggest using no more than 500mg root bark powder per extraction… I find that is the largest amount I can relatively easily work with using my materials. Beyond that it gets hectic.

I use the glass drill to drill a hole in the base of a 1500mL glass wine bottle and affix a pull-top HDPE spout to the mouth of the bottle by placing the pull-top in boiling water for several seconds and after applying epoxy adhesive around the mouth of the bottle, i shove it onto the mouth of the bottle as evenly as possible while holding it in place for 5 minutes, then letting the epoxy set for at least an hour or per the instructions provided with the epoxy. This is a cheap way to have yourself a 1500 mL separatory funnel for about $15 instead of spending a couple to several hundred dollars on a “real” one.

(Put a pot of water on the stove and set your stovetop burner to a Low setting… you want your H2O to heat up to around 120-150 degrees  Fahrenheit, or hot enough to leave your finger in about 2 seconds before it burns you.)
1.Firstly, fill 3-4 quart-sized Mason jars with 800mL of distilled water.
2.Wearing proper eye and hand protective gear, carefully use a small dropper to add 5 drops Muriatic acid to each jar of distilled H2O.
***NEVER ADD WATER TO ACID***
Slowly stir with your longer glass pipette and cover.
3.Next evenly distribute the root bark powder amongst 3 1/2 gallon jars… filling the jars with root bark powder to the 300mL marker is usually a perfect ratio of solid to acidic solution.
4.Carefully pour your jars of 800mL acidic solution into the 1/2 gallon jars. Make sure to completely saturate the bark material… Repeat the process in steps 1 & 2. as needed to fill the jars with powder to the top mL line. (You will want to leave space for shaking the heck outta these suckers once the lids are secured)
5.Shake the heck outta each 1/2 gallon jar and place in the pot on the stove for a few minutes until the particulates have settled.
***MAKE SURE THERE IS A TOWEL OR METAL TRAY IN THE POT ON THE STOVE***
(your jars WILL crack and burst if put directly onto to the bottom of the pot.)
6. Using cotton rounds or a “charmin filter” made out of a few squares of any toilet paper by folding the squares onto themselves, then in half, in half again, and finally roll starting at one end into a tight plug that can be inserted into the narrow spout of your funnels. Make as many filters as you have HDPE funnels and gallon milk jugs, insert them into the funnels, and place the funnels over the opening of the jugs or jars you will be using to collect filtered solution.
7. Using a 60mL bulb syringe or turkey baster, pipette the liquid from the 1/2 gal jars into the funnels. Replenish the 1/2 gallon jars of powder with another 5 drops acid/800mL of distilled water acidic solution as needed and shake the heck outta the powder jars and set them in the hot water bath on the stove again to settle.
8. Repeat steps 4-7 two or three more times until the color of the acidic solution becomes a pale pink.

Now you should have at least a couple gallons of acidic solution filtering.

You will want to change filters as needed to expedite the filtering process (which I consider a crucial part of the extraction if you want as high quality and pure end-product as possible.
I set up a row of 4 filters/jugs or mason jars… the first 2 are fitted with somewhat lightly packed cotton rounds… the second 2 filters are tightly wound “charmin filters”
7. Once the filtering has completed place the jugs of filtered acidic solution (now saturated with alkaloid HCl salts in the refrigerator overnight. This will cause the solution to decant and in the morning you will find that your jugs have a layer of sediment that settled on the bottom. Pour off the acidic solution and rinse out the sediment.

At this point I ditch the milk jugs a use the 1/2 gallon glass Mason jars. This way you can see clearly into the solution. It should be the color of dark red Kool-Aid and completely see-through, i.e. no visible cloudiness or particulates in the acidic solution.
It is preferable to simmer down the volume of acidic solution using a stainless steel pot or opening the lids of the mason jars and letting the acidic solution reduce on Low heat until you have about 1200mL per 1/2 gallon mason jar. I usually end up with three 1/2 gal jars of acidic solution at this point.

Optional with MHRB ~ add  VM P Naphtha (15% of the volume of the acidic solution) to each jar of red liquid and gently turn end over end to get a good distribution of solvent around the solution and then set the jar down until the contents separate completely. Using your separatory funnel, pour the contents of the jar(s) into the upside down wine bottle making sure the pull-top is closed, wait for the liquids to separate and open the pull-top to empty the acidic solution on the bottom back into the mason jars, close the stopper before any solvent comes out and dispose of this solvent. This is called defatting the solution which takes out oils and plant matter, while not visible, will cause a  hinderance to crystal formation later and purity later on. I always do this step, although I have read it is an unnecessary step when using MHRB, as there is little oily/cellulose material compared to some of the acacia grasses. I do this step 2-3 times after a thorough filtering/decanting/reducing job first and I have yet to run into elf-spice that is as pure, with perfectly clear petal-like crystal formations as mine… purity is a must if you plan on converting the freebase spice to the salt form DMT fumarate at any point.

8. Mix approximately 1 Tablespoon (3 teaspoons or approximately 15mL of lye caustic soda crystals to 800mL of distilled water in a quart Mason jar.

***USE CAUTION… LYE WILL BURN ANYTHING IT TOUCHES IN YOUR HOME ***SAVE GLASS… AS YOU STIR THE LYE INTO THE H2O YOU WILL NOTICE
***THE LYE SOLUTION HEAT UP SLIGHTLY***

9. Using your 60mL HDPE bulb syringe or GLASS pipette (no turkey baster for lye solution) slowly add the lye solution drop-wise to the 1/2 gal mason jars of acidic solution… you will notice an immediate reaction as the basic lye solution hits the acidic solution… keep stirring and adding lye solution drop-wise into the acidic solution until it turns a milky color… look closely at the solution as you stir and you can actually see the elf-spice fall out… it looks like tiny glitter in the milky solution.
Keep adding lye solution drop-wise while stirring and you will eventually notice the milky solution in the 1/2 gal jars turn brown and then quickly black like coffee. This takes approximately 250mL of lye solution per 1200mL of acidic solution. Add approximately 50mL more lye solution to each 1/2 gal jar and stir.

10. Use a pH tester or strip to make sure your solution (which should look like black coffee) is at a pH of 13. (BASIC ENOUGH TO MELT YOUR SKIN OFF)
11. Now prepare VM P Naphtha by heating a 10% of the total volume of basic solution (now around 1500mL, so about 150 mL Naphtha) per jar of basic solution in the hot water bath on the stove and add each ~150mL warm solvent to the 1/2 gallon jars of basic solution.
12. Close the lids securely and tip the jars end over end and roll them over and back to mix up the solvent and aqueous solution as much as possible while avoiding shaking the jars as this will cause a frothy emulsion that may take some time to clear.
13. Set the jars in the hot water bath to settle. Once settled use your separatory funnel as before, but this time after emptying the black basic solution back into the mason jars, close the stopper and empty the solvent into a clean quart sized jar.
14. Repeat steps 11-13 2 more times.
15. Prepare one VM P Naphtha 15%/vol of solution and briefly warm in the hot water bath on the stove. Add to the basic solution as before, agitate as before, let settle and separate as before, except this time you can discard the black basic solution, keeping the Naphtha in a clean mason jar or two.
16. There may be some small amounts of basic (dark) solution at the bottom of your solvent… you do not want this at all… carefully pour the solvent from the jar(s) into a clean Pyrex baking dish leaving any dark solution behind to discard.
17. Cover the Pyrex dish with plastic wrap and let the solvent cool to room temp. Once cooled, place the dish inside your refrigerator for 4-5 hours, then transfer to your freezer (set it colder than usual) and don’t disturb for at least 48 hours… by then you will have a nice coating of elf spice on the bottom of the Pyrex dish.
18. Pour off Naphtha quickly as possible without draining any loose crystals… you can turn the dish upside down to drip dry for a few minutes before covering with a paper towel to keep out dust and let evaporate until no solvent can be smelled.

♥Re-crystalize/clean up

1. Once the Naphtha has completely evaporated, use a razor blade to scrape up the elf spice in the bottom of the Pyrex dish and place no more than 1 gram into each martini glass.
2. Heat up the Heptane in the hot water bath and using a glass pipette add warmed Heptane slowly to the elf spice in the martini glass(es) until it is mostly dissolved. At this point stir the Heptane and agitate any undissolved particulates. Add Heptane drop-wise as needed until no more particulates are visible…

***MARTINI GLASS SHOULD IDEALLY BE IN A HOT WATER BATH… YOU WILL NOTICE THAT THE DISSOLVED SPICE WILL SEPARATE AND A YELLOW OILY SUBSTANCE WILL SETTLE ON THE BOTTOM, MAINTAINING THE HEAT OF THE HEPTANE WILL HELP THIS SEPARATION OF THE 5-METHOXY-DMT AND THE FREEBASE DMT CONSIDERABLY***

3. Pipette off the heptane that is clean into a clean glass dish leaving behind the yellow oily 5-MeO.

4. At this point let the solvent cool to room temp, transfer to the refrigerator for maybe 30-60 minutes, by 60 minutes you should see crystal formation beginning, at the very least the clear heptane will have turned cloudy. Transfer to the freezer and leave undisturbed overnight at least.
5. Pour off the heptane and evaporate as before.

***REPEAT RE-CRYSTALIZE/CLEAN UP AT LEAST ONCE MORE THIS TIME USING STAINLESS STEEL TWEEZERS TO AGITATE AND PICK OUT ANY VISIBLE PARTICULATES OR DUST THAT APPEAR***



Finally, remember to let the solvent evaporate completely… there should only be the strong smell of indole when you sniff the martini glass. Scrape your high quality elf spice off the sides of the glass then go forth and be a righteous person.
Opinions?
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"Worry is preposterous, we don't know enough to worry." ~ Wei Po-yang


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OfflineTripoTrick
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Registered: 05/19/14
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Loc: melbourne
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Re: DMT extraction for everybody [Re: Hoosle]
    #21582870 - 04/23/15 03:43 AM (8 years, 9 months ago)

Awesome read.:thumbup:
How much yield did you get out?
Regards


--------------------
"Life isn't as serious as the mind makes it out to be"



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Offlinedjskipmode
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Registered: 05/01/13
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Re: DMT extraction for everybody [Re: TripoTrick]
    #21621401 - 05/01/15 10:08 AM (8 years, 8 months ago)

People the government is trying to take are mushroom spore syringes away . So fight and start making friend so you can start to store them so that if they do get taken away there will be enough people out there with spores that we can fight and make it so that if anyone that would want these for medicinal reason to healthcare self they can get them from people like use. If u would like to.be friends PM me and we can talk.    Also if you got any seeds that you would like me to try out and grow please get at me to


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InvisibleLate2theparty
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Re: DMT extraction for everybody [Re: Hoosle]
    #21632750 - 05/03/15 11:58 PM (8 years, 8 months ago)

Fantastic method, I like it.

How effective are simply using some of the intermediate steps on their own, in terms of marginally increasing concentration of DMT? Are there steps any in here which can be performed on their own to create usable DMT?


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OfflineHoosle
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Re: DMT extraction for everybody [Re: TripoTrick]
    #21645348 - 05/06/15 06:29 PM (8 years, 8 months ago)

Yield from 500mg root bark is around 10-14 grams of Elfspice... taking out the 5-MethOxy will take away a significant portion of this yield.. possibly up to 40-50%... but purified spice is a must for salting, so it depends on your goals and intentions


--------------------
"Worry is preposterous, we don't know enough to worry." ~ Wei Po-yang


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OfflineTripoTrick
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Re: DMT extraction for everybody [Re: Hoosle]
    #21700929 - 05/20/15 01:49 AM (8 years, 8 months ago)

Quote:

Hoosle said:
Yield from 500mg root bark is around 10-14 grams of Elfspice... taking out the 5-MethOxy will take away a significant portion of this yield.. possibly up to 40-50%... but purified spice is a must for salting, so it depends on your goals and intentions




500gr or 500mg?

Kind regards


--------------------
"Life isn't as serious as the mind makes it out to be"



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Offlinekakashi68
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Re: DMT extraction for everybody [Re: TripoTrick]
    #21741622 - 05/30/15 03:58 PM (8 years, 7 months ago)

This isnt for everybody... this is for americans who have these legal ingredients

Always american... always arrogant


--------------------
You know, just sometimes in between the first cigarette with coffee in the morning to that 400th glass of cornershop piss at 3am--you do sometimes look at yourself and think--this is fantastic. I'm in heaven.
-Bernard Black



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Offlinejonneturke
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Registered: 05/16/15
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Re: DMT extraction for everybody [Re: kakashi68]
    #21759308 - 06/03/15 09:26 PM (8 years, 7 months ago)

Quote:

kakashi68 said:
This isnt for everybody... this is for americans who have these legal ingredients

Always american... always arrogant




Which of these ingredients are illegal in Au?


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Offlinekakashi68
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Re: DMT extraction for everybody [Re: jonneturke]
    #21759893 - 06/04/15 12:12 AM (8 years, 7 months ago)

Mimosa Hostilis


--------------------
You know, just sometimes in between the first cigarette with coffee in the morning to that 400th glass of cornershop piss at 3am--you do sometimes look at yourself and think--this is fantastic. I'm in heaven.
-Bernard Black



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OfflineKenneth
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Registered: 06/07/15
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Re: DMT extraction for everybody [Re: Hoosle]
    #22183864 - 09/03/15 05:06 PM (8 years, 4 months ago)

how much dmt would this give you?


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OfflineCraterBait
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Re: DMT extraction for everybody [Re: Hoosle]
    #22352809 - 10/09/15 12:28 AM (8 years, 3 months ago)

Completely unacceptable, and bad chemistry.

Never use muriatic acid, only pure HCL. Citric acid found in the canning section of walmart performs exceptionally well for the purpose of this extraction. Most of you have pressure cookers anyway, just PC it in jar in acidic solution Ph3.


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OfflineBig Worm
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Re: DMT extraction for everybody [Re: djskipmode]
    #22352859 - 10/09/15 12:42 AM (8 years, 3 months ago)

Quote:

djskipmode said:
People the government is trying to take are mushroom spore syringes away . So fight and start making friend so you can start to store them so that if they do get taken away there will be enough people out there with spores that we can fight and make it so that if anyone that would want these for medicinal reason to healthcare self they can get them from people like use. If u would like to.be friends PM me and we can talk.    Also if you got any seeds that you would like me to try out and grow please get at me to







lol nice try.


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OfflinefirstTIMER420
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Re: DMT extraction for everybody [Re: djskipmode] * 1
    #22456238 - 10/31/15 12:30 AM (8 years, 2 months ago)

Quote:

djskipmode said:
People the government is trying to take are mushroom spore syringes away . So fight and start making friend so you can start to store them so that if they do get taken away there will be enough people out there with spores that we can fight and make it so that if anyone that would want these for medicinal reason to healthcare self they can get them from people like use. If u would like to.be friends PM me and we can talk.    Also if you got any seeds that you would like me to try out and grow please get at me to





:cop: Got my eyes on you, son.


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OfflineHoosle
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Re: DMT extraction for everybody [Re: TripoTrick]
    #22818808 - 01/24/16 12:15 PM (8 years, 5 days ago)

Hey there, my apologies, that was grams... i'm a space cadet.


--------------------
"Worry is preposterous, we don't know enough to worry." ~ Wei Po-yang


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OfflineHoosle
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Re: DMT extraction for everybody [Re: TripoTrick]
    #22818831 - 01/24/16 12:18 PM (8 years, 5 days ago)

just under 15 grams, but  when it removed the 5meo it had just over 9 grams.


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"Worry is preposterous, we don't know enough to worry." ~ Wei Po-yang


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InvisibleBacchus
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Re: DMT extraction for everybody [Re: CraterBait]
    #22959846 - 02/29/16 08:15 PM (7 years, 10 months ago)

Quote:

CraterBait said:
Completely unacceptable, and bad chemistry.

Never use muriatic acid, only pure HCL. Citric acid found in the canning section of walmart performs exceptionally well for the purpose of this extraction. Most of you have pressure cookers anyway, just PC it in jar in acidic solution Ph3.




To be clear, don't use HCL in an aluminum vessel. Use citric acid, for example, if aluminum will be around. Even though the aluminum chloride that you produce will probably react completely with your sodium hydroxide (and therefore not be in your final product), it's smart to avoid producing neurotoxins in your kitchen :smile:


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Offlinegekkogecko
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Re: DMT extraction for everybody [Re: Bacchus]
    #22982305 - 03/07/16 11:27 AM (7 years, 10 months ago)

Just out of curiosity, anyone have a ballpark of what the cost of the supplies add up to?


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Invisiblemicro
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Re: DMT extraction for everybody [Re: Bacchus]
    #22986290 - 03/08/16 04:39 PM (7 years, 10 months ago)

Quote:

Bacchus said:
To be clear, don't use HCL in an aluminum vessel. Use citric acid, for example, if aluminum will be around. Even though the aluminum chloride that you produce will probably react completely with your sodium hydroxide (and therefore not be in your final product), it's smart to avoid producing neurotoxins in your kitchen :smile:




Aluminum oxide, or table salt o.O?

Quote:

gekkogecko said:
Just out of curiosity, anyone have a ballpark of what the cost of the supplies add up to?




Cheap? You can do it for under $100 depending on how thrifty you are.

Much less if you have things like Pyrex dishware.


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(Avatar is Maxxy, a character by Mizzyam, RIP)


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InvisibleBacchus
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Re: DMT extraction for everybody [Re: micro]
    #22987380 - 03/08/16 10:11 PM (7 years, 10 months ago)

Aluminum Chloride. It's a single displacement reaction between the HCl and Al.


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Living on a no-Flash diet is way easier than you think. Give it a shot.


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InvisibleKelazam
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Re: DMT extraction for everybody [Re: Hoosle]
    #24357191 - 05/28/17 06:44 PM (6 years, 7 months ago)

No


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