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Offlinemico-padawan
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Any additions to this DMT tek friends? Fluffy White Fun Fest!
    #19191432 - 11/26/13 11:07 AM (10 years, 2 months ago)

Are there any flaws with this tek?

Tek lists MHRB as what was used. But I will be extracting from Hawaiian Acacia Confusa. Will this still work?

Tek 2: The Fluffy White Funfest > Pulled info from Q2121"s tek

About Naptha

Naptha petroleum is a non-polar solvent and the only non-food-safe ingredient, though it's toxicity is quite benign. Assuming it is always used with ample ventilation and isn't spilled all over you.
The LD50 (amount needed to consume for 50% of subjects to die) for naptha is stated as 8000-20000mg/Kg while the LD50 for DMT is 60-110mg/Kg. Heck the LD50 for Vitamin A is 1510-2570mg/Kg and Vitamin B is 560mg/Kg.

Plus 2 things:
1. It evaporates cleanly without a trace in a couple hours
2. When burned it produces only WATER and CARBON DIOXIDE, that is why using it as a lighter fuel is safe.

Anyway, it is simply lighter fluid which many houses have around already, but you need one that doesn't have any nasty additives.

If you are in the US then VM+P Naptha is your choice.
If you are in Canada then Ronsonol Lighter Fluid or Escort Camp Fuel are your choices.
If you can't find either then buy some lighter fluid and test it:
1.Pour a little on a surface (I use blank CDs)
2.Wait an hour or two for it to evaporate. If it smells or looks like anything other than a blank and clean/dry surface then the lighter fluid SHOULDN'T be used.


(what your product will look like If you follow the tek)
whitejn.th.jpg


Materials required:

IMPORTANT: The lime, the vinegar, the naptha and MHRB MUST MUST MUST be correct and suitable for use in this tek. The vast majority or problems or complete failures in this tek and others as well are simply due to questionable or incorrect materials. This tek is very easy and I tell people who ask about it "It is just as easy as it sounds. If your materials are good then your end product will be VERY GOOD"


Two Containers that fit one in another (HDPE plastic, glass, metal, something naptha won't dissolve/degrade)
one Electric Kettle or Stove w/ pot (kettle is best)
one or more baking pans/wide mouth containers for freezer precipitation
one freezer
30g or more Mimosa Hostilis root bark (MHRB)
50ml or more 5% White Vinegar (CH3COOH)
Some Lime Ca(OH)2
100ml or more Naptha
one or more chopsticks or wooden spoons(to stir the gooey bark)

Useful tools
a few Playing cards
one or more razor blades/scrapers
Some coffee filters
one blender (unless you buy, pre-powdered bark)

Preparation:

sany0106d.th.jpg
Step 0: If your MHRB isn't powdered, use a blender to cut it into powder/fibers as small as possible

Note:Household blenders tend to blend bark to fibres rather than powders bark so the the consistency may be different than the descriptions.

Step 1: Prepare your supplies

Chopsticks/Spoon: Chopsticks work best for 100g or less MHRB while a spoon works better for more than 100g.

Your container, it can be a glass or HDPE2 sealed container for shaking/rolling to mix or on open container for stirring. (The fact that the sealed container works is recently discovered so the tek may say stir when someone using a sealed container would shake/roll)

Have nearby: vinegar, hot/boiling water, lime.

Lastly have everything else needed for the tek available and have the tek open an a computer for quick reference.

[gradient:#FF0808,#]Caution[/gradient]: Using plastic containers or any plastic in the extraction creates risk either small plastic residues in the product or even a completely messed up end product (This is not an exaggeration, read these posts #1, #2, #3) HDPE2 (Most dense non-clear plastics, labeled as such on the bottom) should be safe to use but but glass would be the safest choice.

Acidification:

acidv.th.jpg
This step utilizes the vinegar (acetic acid) to change the DMT-tannate molecules contained in the MHRB into DMT-acetate and in the process dissolve them into the surrounding vinegar. The PH of the dilute vinegar is ~2.5 so the mix will probably be around that but checking the PH shouldn't be necessary


Note 1:this step does not need to be too "exact"

Step 1: Take 30g-500g powdered MHRB and place in your container.

Step 2: Add vinegar to the bark and stir until the bark starts forming clumps. Add enough so most of the bark is wet, red and clumpy.

Step 3: Then slowly and while stirring add near-boiling tap water. Add and stir until it is wet enough to flow when you tip the container to one side or the other. (Approximately: 100ml vinegar and 100ml near-boiling water for 100g MHRB)

Step 4: Stir several times as the bark is let to sit for 20-40 minutes. (Longer won't hurt though) YOU DO NOT NEED TO STIR CONSTANTLY, ONLY PERIODICALLY


Note 2: If you were to choose not the acidification step, thus doing a STB lime tek, it would work... but would take periodic stirring over a minimum of 2 days before a significant yield will be achieve and several days more for the rest

The vinegar step is essential for the swiftness of the tek to be utilized.


Basification:

sany0015.th.jpg
This step utilizes the alkalinity of the lime to convert the polar DMT-acetate in the vinegar-water (a polar solvent) into non-polar DMT freebase which is soluble in limonene/xylene (non-polar solvents) and not soluble in water. Since lime can raise the PH to 12-12.5 the PH of the "mush" should be close to that though once again PH testing shouldn't be necessary

MAKE SURE YOUR LIME IS Calcium Hydroxide OR ELSE THE TEK WILL NOT WORK!

Step 1: Add to the mix at least 3g of lime for every 4g of MHRB used. (IE: 150g lime for 200g MHRB)
(More lime will not hurt.)

Adding it bit-by-bit and mixing will be easier to mix, but you can dump it all in if you want.
(For those of you without scales: 1 cup of lime is 130-150g)


Step 2: Stir it very thoroughly until all the pure-white lime is mix and there is no more red. Add very small amounts of water if needed to achieve a moist and consistent mixture.

Note 1: The mix tends to form a "dark top" when you stop mixing that is fine. It is completely normal.

Step 3: Create the right consistency.
The ideal consistency is not super exact. There are 2 main options for consistency. Consistency 1 will work 100% as well as Consistency 2, it may absorb more solvent than Consistency 2.

There will be inevitable solvent loss regardless but my estimate is anywhere from 25%-40% reduction in solvent loss using Consistency 2 which in a 100g MHRB extraction might be 50-80ml less solvent lost. If solvent supplies are plentiful then there should be no problem using Consistency 1 or Consistency 2, remember that they can be RE-USED many times.


Consistency 1: Add water (if needed) to make the mix look like anywhere from thick oatmeal too kinda like thick pea-soup. Both will work fine. If it is like tomato soup that's too soupy!
Step 3a: if it is too dry add some tap water a TINY TINY splash at a time, stir well and repeat adding and stirring until it is JUST moistened throughout

Step 3b: if it is too wet add more lime a little bit at a time, stir well and repeat adding and stirring until it thickens and dries to the right consistency

Consistency 2: Either let the mix dry until crumbly (Like the top of an apple crisp) or dry it in the oven (in an oven-safe container!) at 95C or the lowest setting until crumbly.
You don't want it bone-dry because it will absorb more solvent than Consistency 1, if it does get bone-dry then just add some water to make it crumbly.

Non-Polar Wash:

naptha.th.jpg
Each time this step is done it is called "a pull" and the step uses naptha to dissolve the DMT freebase from the bark-mush. This separation is is essential if a pure product is to be extracted


[gradient:#FF0000,#]CAUTION[/gradient]: Naptha fumes are toxic and it evaporates very quickly, so do this in a ventilated area (window open and/or a fan) Also if it is left for a several hours the naptha will all be gone

Note 1: The tek is designed to do each step directly after another without any waiting periods except those that are steps.

The first pull if done immediately after getting the lime-bark to one of the consistencies shouldould yield anywhere from 10%-35% (in my experience.) If the first pull is done after 6-8 hours however it will likely yield 25%-60%.
2 pulls done around 24 hours and 48 hours (or later) should be enough to get 80%-90% of the DMT (In my experience).
Pulls after that tend to be rather small but I highly recommend doing pulls at 1 week and another at 2 or 3 weeks to get all the DMT possible.


Step 1: Put the top/smaller bowl into the bottom/larger bowl and add enough boiling water to the BOTTOM bowl to match the level of the bark in the top bowl, either that or just until the top bowl floats. This is very simply to warm the naptha indirectly and safely.

Step 2: Add enough naptha so you can see it on the sides. It should be 1ml naptha per 1g of bark or more (100ml naptha or more for 100g MHRB) The naptha should stay completely separate from the bark and remain transparent.

*The naptha does NOT need to be hot, only warm (feel the bowl, not the naptha)*

Step 3: Stir the bark around with the naptha thoroughly and periodically until it is warmed from the water underneath. Once warm 5-10 minutes is all that is needed. YOU DO NOT NEED TO STIR CONSTANTLY, ONLY PERIODICALLY


I like to think of using the non-polar solvent like using water to dissolve some salt. Though the salt will not instantaneously become saturated with salt, it will in a few minutes. Same with the solvent, it is the bark and lime that works for hours, not the solvent.

Step 4: Pour off the naptha from the bark-goo and into *your precipitation container* to get naptha out pour off as much as you can by tilting the bowl, this will get at least 90% of the naptha out and there is no need to get 100% of it.
*make sure to wipe the bottom of the container dry before pouring or else water will drip into your naptha*

If after this step the naptha still looks clear and colorless, don't worry.
The naptha will be either colorless or slightly slightly yellow unlike the deep-yellows and sometimes browns you may see in STB teks.

*your precipitation container*
I find it easiest to work with a small glass baking tray since a razor blade scraper can be used to get 99% of the crystals.
You can use any naptha-safe container though.

Recrystallization:

spices.th.jpg
This step works on the principal that naptha can dissolve DMT-freebase quite well when warm/hot but can barely dissolve any when it is freezing. When the naptha with DMT-freebase dissolved in it is cooled the DMT precipitates out slowly as crystals.


Step 1: Just pop the naptha straight into the freezer.
You can do a recrystallization later for larger crystals, but for the initial step it is best to just put the naptha in the freezer right away.

Note: You can cover the container with saran-wrap or a lid, but expect your freezer to smell like naptha for a day or two whether you do or not. I usually to leave it uncovered.

It will always require several pulls to get all the DMT-freebase. There are 2 ways you can approach the multiple pulls
Step 2a: While the first batch of naptha is in the freezer you can add new naptha and do another "pull", repeating the non-polar wash.

Step 2b: Wait until the mix has precipitated all the crystals and re-use only the single batch of naptha.

In either case it will require 2-3 pulls to get about 90% of the DMT, likely over 5 pulls to get over 98%.

Step 3: Keep the naptha in the freezer for a couple hours and you should start seeing crystals forming.
If the naptha is still foggy that means that there are microscopic DMT-freebase molecules trying to find a crystal to attach to. Once it is clear then it is getting close to being done. It's best to leave it overnight or at least 8-12 hours though.

Step 4: Once you are satisfied with the "snow-globe" take it out and pour off the naptha. Make sure to pour it off slowly so none of the crystals spill out, then find a (preferably outdoors, fumes) place to lean the container against, the excess naptha will drip off and evaporate in a couple hours.
Sometimes the crystals are floating all over, usually just SLOWLY pouring the naptha off works, you may need to pour it through a coffee filter to get all the crystals though.


Note 1: If the first 2 pulls don't cloud or precipitate crystals after 8-12 hours then check something in the extraction did not work correctly. Check Common issues/Troubleshooting because that should not happen.

Note 2:there may be a small film underneath the crystals. The film is soluble in vinegar and I am pretty sure it is either DMT-n-oxide or Jungle DMT

Once it no longer smells like naptha the DMT-freebase is ready.


Storage:

You can either scrape the DMT up and store in a mini-ziplock bag or any other small sealable container as is.
A playing card folded with a crease down the middle works very well for moving the crystals around.

The other option is to dissolve it in vinegar as a tincture.
(Most will probably keep it as is, but the tincture method is worth mentioning)

I personally prefer the tincture because it is easier to measure, keep, transport, smoke and it can be filtered for the utmost purity.
If a tincture is to be made then all you need to do is dissolve everything in the precipitation container in a minimal amount of vinegar, the liquid will need to be evaporated down until it starts getting deep-yellow.
There is a lot more information on tinctures in Tek 1


--------------------
Take me again to the place my body wanders and my mind is free. Let me venture into the spirit realm, to the place where all life starts and all life returns.


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Offlinemico-padawan
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Registered: 09/11/10
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Re: Any additions to this DMT tek friends? Fluffy White Fun Fest! [Re: mico-padawan]
    #19193953 - 11/26/13 08:13 PM (10 years, 2 months ago)

Bump!

So this is all good I am assuming. I realize this is a long post. But, I really need a expert overview here community.

No additions or subtractions guys, I should just run with this tek as is?


--------------------
Take me again to the place my body wanders and my mind is free. Let me venture into the spirit realm, to the place where all life starts and all life returns.


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Offline46N2
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Registered: 11/18/14
Posts: 12
Last seen: 8 years, 2 months
Re: Any additions to this DMT tek friends? Fluffy White Fun Fest! [Re: mico-padawan]
    #21043613 - 12/30/14 11:45 AM (9 years, 1 month ago)

any current reviews on this tek?


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InvisibleGuardian187
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Registered: 11/29/14
Posts: 716
Loc: Center of the Universe
Re: Any additions to this DMT tek friends? Fluffy White Fun Fest! [Re: 46N2]
    #21044292 - 12/30/14 02:29 PM (9 years, 1 month ago)

Try Cybs' hybrid ATB tek. It is beginner friendly and been thoroughly vetted.


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OfflineLogicaL ChaosM
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Re: Any additions to this DMT tek friends? Fluffy White Fun Fest! [Re: mico-padawan]
    #21046329 - 12/30/14 09:44 PM (9 years, 1 month ago)

I cant believe Hawaiian Acacia Confusa has DMT!

I used to live in Hawaii, and there are lots of these HUGE trees. Really cool looking too.


Nooooo! I could have made DMT in Hawaii! Why cant i time-travel back :thumbdown::mad2:


--------------------
"What you must understand is that your physical dimension affects everyone in the higher dimensions as well. All things are interconnected. All things are One. Therefore, if one dimension is broken or out of balance, then all other dimensions will experience repercussions." - Pleiadian Prophecy 2020 The New Golden Age by James Carwin

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InvisibleGuardian187
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Registered: 11/29/14
Posts: 716
Loc: Center of the Universe
Re: Any additions to this DMT tek friends? Fluffy White Fun Fest! [Re: LogicaL Chaos]
    #21046936 - 12/31/14 12:01 AM (9 years, 1 month ago)

Quote:

LogicaL Chaos said:
I cant believe Hawaiian Acacia Confusa has DMT!

I used to live in Hawaii, and there are lots of these HUGE trees. Really cool looking too.


Nooooo! I could have made DMT in Hawaii! Why cant i time-travel back :thumbdown::mad2:




Ahh sad haha


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