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Offlineirreligiosity
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Registered: 11/20/13
Posts: 7
Last seen: 10 years, 2 months
Muscimol purification
    #19168382 - 11/21/13 01:29 AM (10 years, 2 months ago)

I've looked through the forum for this, and see the question come up, but it always seems to end short of the answer. I know of Ott's work, and how much effort it took him to make a completely pure product. I don't need a product pure enough to sell to pharmaceutical companies. Working under the premise that I have access to a laboratory has anyone toyed around with purification?

I took ~30lbs of Amanita mushrooms, chopped them all up and placed them in hot water for a couple hours. I then strained that liquid removing the meat of the mushrooms. I then evaporated all of the water off with low heat. I am hoping the fact that it was constantly hot from the time of hitting the water to the end product it has fully decarboxylated the ibonetic acid. While evaporating the water off a layer of film manifested so half way through evaporating I refiltered to remove the film. Once evaporated I had a dark sludge (the same consistency of BHO reclaim if you're familiar with that).

I have yet to weigh the sludge because I have another tray evaporating, but based on my first yields I'm going to going to guess I have about an oz of that sludge. Obviously this is far from a pure substance because Ott used 100kg+ to make a couple grams.

I'm fine with running a couple tests in some test tubes on the material because it is more than I will ever take, and I have no interest in selling substances.

Would a simple alkaloid A/B extraction work? Dissolve the goo in water, then acidify, then pass chloroform through and discard. Then alkaline it and use chloroform to pull the alkaloids out?


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InvisibleWillSolvem
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Folding@home Statistics
Registered: 04/24/12
Posts: 1,519
Loc: Chapter 26 Flag
Re: Muscimol purification [Re: irreligiosity]
    #19226089 - 12/04/13 10:51 AM (10 years, 1 month ago)

:popcorn:


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AMU Q&A Thread because questions deserve answers.


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OfflineDark76


Registered: 07/14/13
Posts: 121
Last seen: 5 years, 8 months
Re: Muscimol purification [Re: WillSolvem]
    #19226124 - 12/04/13 11:02 AM (10 years, 1 month ago)

And what does this have to do with Mycology?

Your post seems to describe a chemical extraction.

If only there were a Chemistry and Pharmacology forum or something...

:hmm:


Edited by Dark76 (12/04/13 11:02 AM)


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InvisibleWillSolvem
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Registered: 04/24/12
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Re: Muscimol purification [Re: Dark76]
    #19226600 - 12/04/13 12:59 PM (10 years, 1 month ago)

Kind of got a point there


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AMU Q&A Thread because questions deserve answers.


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