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OfflineEywa_devotee
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Registered: 10/04/10
Posts: 1,088
Loc: State of Confusion, Arkan... Flag
Last seen: 3 years, 7 months
Eywa's Efficient Psilocin Psilocybin Mushroom Extraction Tek
    #19128254 - 11/12/13 07:29 PM (10 years, 2 months ago)

Eywa's Efficient Psilocin Psilocybin Mushroom Extraction Tek- Use to covert mushrooms to purified alkaloids

Equipment needed:
Cofee grinder
Mason Jars or any other glass jar.
Glass measuring cup
Pyrex cooking pan or dish.
Small tubing to build a gas generator with.
Freezer
Funnel
Hotplate
Fan to blow ammonia fumes away!

Materials needed:
Magic mushrooms
Malic, Fumaric, or Tartaric acid
Dry acetone
Dry Isopropyl alcohol
Dry Methanol
Filter paper
Concentrated Ammonia solution.
Lye crystals

Finely powder the magic mushrooms. Make a 80/20 mixture of DRY isopropanol/methanol. Use Enough to cover the shrooms up to 1/3 of their volume and add ammonia GAS generated from concentrated ammonia solution dripped on lye crystals. (make a meth lab style gasser bottle) Do this slowly as the lye crystals will get very hot! This will freebase the mushrooms with ammonia when the solution stops absorbing ammonia. Ethanol will work, but is hard to make absolutely dry. Put the lid on the jar and allow the mix to sit at room temperature for 3 days than decant the alcohol and wring the mushrooms dry of alcohol saving the alcohol solution.

Gently heat the solution in a pyrex pan until the ammonia smell is gone and set aside. NO OPEN FLAMES!!! Dissolve an organic acid like malic, fumaric, or tartaric acid in methanol and add this acid to the the alcohol mixture at a ratio of a gram for expected gram of psilo. Stir thouroughly and then add about 20-30% dry acetone to the mixture. NOTE: It must be dry or you will NOT get crystals!

Put into the freezer and let sit a day or two. The crystals of psilocin and psilocybin in a salt form will precipitate out. While still ice cold filter this out; a clever trick is to pour the alcohol slowly and keep the crystal mass in the jar. Leave the jar at a slight angle in the freezer and allow the rest of the alcohol to seep from the crystals in about an hour or so.

Pour this off and let it set tightly closed to warm to room temperature and remove the remaining alcohol by drying with a stream of absolute dry air. You can recrystallize from dry methanol if you like. Scrape the crystals out and put in a jar sealed under butane or argon gas to prevent oxidation.

Measure the amount you want, and dissolve in neutral saline solution and place in a nebulizer to inhale, gel cap, or dissolve and shoot it (for the brave).


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"Love one another." "To Love is to know me." "Love is the Law, Love under Will." "In Compassion, all sorrows end." Regardless of the Master, the message is the same- Choose love and you shall live, Choose Fear and you shall die. Help bring peace to this Earth: Love one another, and serve others before yourself.


Edited by Eywa_devotee (11/12/13 07:51 PM)


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OfflineSugar Of Saturn
Student

Registered: 11/03/13
Posts: 37
Last seen: 9 years, 11 months
Re: Eywa's Efficient Psilocin Psilocybin Mushroom Extraction Tek [Re: Eywa_devotee]
    #19128365 - 11/12/13 07:55 PM (10 years, 2 months ago)

Hmm, this is very interesting. Ive wasted ounces of mushrooms and litres of solvent trying to get a clean extract. the only thing that works for me is http://www.erowid.org/archive/rhodium/chemistry/psilocin.extraction.html
or the alcohol tek. but i think those crystals are not pure.

have you tried it? Did you get clean crystals with no organic residue? post pics.


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InvisibleStygianKnight
A Mushroom

Registered: 03/12/12
Posts: 2,717
Re: Eywa's Efficient Psilocin Psilocybin Mushroom Extraction Tek [Re: Sugar Of Saturn]
    #19129049 - 11/12/13 10:40 PM (10 years, 2 months ago)

Have you personally tried these crystals for activity?

Note: Careful evaporating flamable liquids in a normal freezer as this can blow the door off if ignited.


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