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InvisibleSjaman
Registered: 10/02/13
Posts: 19
Loc: Amsterdam
Syrian rue extraction - help needed *DELETED*
    #18919771 - 10/02/13 07:04 AM (10 years, 3 months ago)

Post deleted by Sjaman

Reason for deletion: solved



Edited by Sjaman (10/02/13 08:58 AM)


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OfflineHarryL
Squnä'am
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Registered: 11/16/10
Posts: 8,070
Loc: Washington State
Last seen: 4 years, 8 months
Re: Syrian rue extraction - help needed [Re: Sjaman]
    #18920004 - 10/02/13 08:47 AM (10 years, 3 months ago)

The SWiM crap is really getting old...
Stop please... Everyone knows it you... Not needed on here

For some reason, I can't open the link you put in your post

Can you fix that so we can see what you did?


--------------------
Mushroom hunting:  One bad mushroom can ruin your day! Know it or throw it.


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InvisibleSjaman
Registered: 10/02/13
Posts: 19
Loc: Amsterdam
Re: Syrian rue extraction - help needed *DELETED* [Re: HarryL]
    #18920040 - 10/02/13 09:00 AM (10 years, 3 months ago)

Post deleted by Sjaman

Reason for deletion: solved



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OfflineHarryL
Squnä'am
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Registered: 11/16/10
Posts: 8,070
Loc: Washington State
Last seen: 4 years, 8 months
Re: Syrian rue extraction - help needed [Re: Sjaman]
    #18920181 - 10/02/13 09:49 AM (10 years, 3 months ago)

Hey... No worries.... Not trying to bust your balls but....

Very simple tek really... Don't improvise on your first run through on a tek... Just my advice.

Did you use rock salt or table salt?  Sounds a bit like you have iodine in your crystals, giving you the brown color... Won't hurt ya in small amounts... Neither will dirt though..

Methanol and a less fine filter were called for in the tek... Not IPA and 150 um filter
The filter doesn't matter if you dissolved the crystals in the alcohol but I am not sure how important the specific alcohol is to this simple tek.... Might not matter at all

You are not changing the pH so you can't have a base. Sort of leaves a salt or possibly an acetate if you used vinegar. Would have to look closer at what you are doing...

Peace


--------------------
Mushroom hunting:  One bad mushroom can ruin your day! Know it or throw it.


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InvisibleSjaman
Registered: 10/02/13
Posts: 19
Loc: Amsterdam
Re: Syrian rue extraction - help needed *DELETED* [Re: HarryL]
    #18920337 - 10/02/13 10:33 AM (10 years, 3 months ago)

Post deleted by Sjaman

Reason for deletion: solved



Edited by Sjaman (10/02/13 10:42 AM)


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OfflineHarryL
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Registered: 11/16/10
Posts: 8,070
Loc: Washington State
Last seen: 4 years, 8 months
Re: Syrian rue extraction - help needed [Re: Sjaman]
    #18920446 - 10/02/13 10:56 AM (10 years, 3 months ago)

That is a lot if vinegar if you ask me
Normally, I just add a teaspoon of vinegar not 5%... Though, it does boil off in the process

IPA might make a difference but don't know for sure...it's might change the solubility but not the chemical form
Like I said... Filter probably didn't make a difference but 150 um is pretty small

Honestly... I would give it a try...


--------------------
Mushroom hunting:  One bad mushroom can ruin your day! Know it or throw it.


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InvisibleSjaman
Registered: 10/02/13
Posts: 19
Loc: Amsterdam
Re: Syrian rue extraction - help needed *DELETED* [Re: HarryL]
    #18920529 - 10/02/13 11:16 AM (10 years, 3 months ago)

Post deleted by Sjaman

Reason for deletion: solved



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InvisibleSjaman
Registered: 10/02/13
Posts: 19
Loc: Amsterdam
Re: Syrian rue extraction - help needed *DELETED* [Re: Sjaman]
    #18921119 - 10/02/13 01:14 PM (10 years, 3 months ago)

Post deleted by Sjaman

Reason for deletion: solved



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OfflineHarryL
Squnä'am
Male User Gallery


Registered: 11/16/10
Posts: 8,070
Loc: Washington State
Last seen: 4 years, 8 months
Re: Syrian rue extraction - help needed [Re: Sjaman]
    #18922042 - 10/02/13 03:45 PM (10 years, 3 months ago)

I would test it out myself
You haven't don't anything to make it bad that I can see

Might want to try it again though... See what you get the second time


--------------------
Mushroom hunting:  One bad mushroom can ruin your day! Know it or throw it.


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