Home | Community | Message Board

MushroomCube.com
This site includes paid links. Please support our sponsors.


Welcome to the Shroomery Message Board! You are experiencing a small sample of what the site has to offer. Please login or register to post messages and view our exclusive members-only content. You'll gain access to additional forums, file attachments, board customizations, encrypted private messages, and much more!

Shop: PhytoExtractum Kratom Powder for Sale, Maeng Da Thai Kratom Leaf Powder   Bridgetown Botanicals CBD Concentrates   Kraken Kratom Red Vein Kratom

Jump to first unread post Pages: 1 | 2 | Next >  [ show all ]
Some of these posts are very old and might contain outdated information. You may wish to search for newer posts instead.
Offlinetotal
Post Office Tyvek Advocator
Male User Gallery


Folding@home Statistics
Registered: 10/03/04
Posts: 11,405
Last seen: 6 months, 24 days
DMT Extraction of MHRB ?'s
    #14579188 - 06/08/11 10:59 AM (12 years, 7 months ago)

So following 13shroom's STB Tek(or his copypasta from a source i cant remember (and im too lazy to look)), i froze my naptha overnight and poured it off and placed a fan ontop of it to dry the remaining naptha off the crystals...
Now im left with a orange/yellow sludge.. :shrug:
Does this look normal to you guys?
There are some white crystals around the top edge, but for the most part, its very yellow/orange..



Extras: Filter Print Post Top
OfflineDave Bowman
Albert Hoffmans Apprentice
Male User Gallery


Folding@home Statistics
Registered: 08/30/07
Posts: 2,104
Loc: Your Imagination
Last seen: 3 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: total]
    #14579202 - 06/08/11 11:02 AM (12 years, 7 months ago)

How much MHRB did you start with?  The crystals around the edge is what you want.


Extras: Filter Print Post Top
Offlinetotal
Post Office Tyvek Advocator
Male User Gallery


Folding@home Statistics
Registered: 10/03/04
Posts: 11,405
Last seen: 6 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: Dave Bowman]
    #14579203 - 06/08/11 11:03 AM (12 years, 7 months ago)

100g
I was very careful not to get any of the basified sludge from the bottom layer...
The naptha was very piss colored...


Edited by total (06/08/11 11:03 AM)


Extras: Filter Print Post Top
OfflineDave Bowman
Albert Hoffmans Apprentice
Male User Gallery


Folding@home Statistics
Registered: 08/30/07
Posts: 2,104
Loc: Your Imagination
Last seen: 3 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: total]
    #14579427 - 06/08/11 11:58 AM (12 years, 7 months ago)

Quote:

total said:
100g
I was very careful not to get any of the basified sludge from the bottom layer...
The naptha was very piss colored...




What kind of Naptha did you use?  Just some from the hardware store?

This is quite possibly just impurities leftover from solvent.

Did you test you solvent first by pouring a little amount in your crystallization vessel [in this case it looks like you are using either a jar or petri dish] and letting it evaporate completely overnight?  And then seeing what is left?

You should always test your solvent for purity before actually using.  All the yellow shit could just be impurities from the solvent but you'll never know unless you test first.

You could always do that now, pour some fresh solvent in a glass dish and let it evaporate 100%.  if you are left with the same yellow shit that means your solvent is much to dirty to use.

EDIT:  One time I used Coleman's fuel as the solvent and was left with very pink crystals but nothing that looks like your pics, like the yellow sludge in the middle. 

I fixed my product by re-crystallizing and was left with very pure, white crystals.

Your actual crystals look crystal white so I think that just may be dirty solvent.

Try the solvent test first.


Edited by Dave Bowman (06/08/11 11:59 AM)


Extras: Filter Print Post Top
OfflineDave Bowman
Albert Hoffmans Apprentice
Male User Gallery


Folding@home Statistics
Registered: 08/30/07
Posts: 2,104
Loc: Your Imagination
Last seen: 3 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: Dave Bowman]
    #14579446 - 06/08/11 12:03 PM (12 years, 7 months ago)

Also if you could find Toluene as your solvent, you may have better luck.  Only evaporate the toluene in a WELL ventilated area or in a garage / shed though.  It's carcinogenic. 

Also, you'll increase your yield a bit using toluene because only toluene pulls "jungle spice" out of MHRB, it's not soluble in Naptha.

Read around DMT-Nexus about Jungle Spice.


Extras: Filter Print Post Top
Offlinetotal
Post Office Tyvek Advocator
Male User Gallery


Folding@home Statistics
Registered: 10/03/04
Posts: 11,405
Last seen: 6 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: Dave Bowman]
    #14579555 - 06/08/11 12:30 PM (12 years, 7 months ago)

The naptha was just bought at home depot... :shrug:
It was very clear, until mixed with the basified sludge, then it turned piss yellow...
Its the VM&P type...
Ill do a evap test tonight to see...
In the meantime, do i need to heat the naptha to get the crystals to redissolve?


Edited by total (06/08/11 12:31 PM)


Extras: Filter Print Post Top
OfflineDave Bowman
Albert Hoffmans Apprentice
Male User Gallery


Folding@home Statistics
Registered: 08/30/07
Posts: 2,104
Loc: Your Imagination
Last seen: 3 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: total]
    #14579692 - 06/08/11 12:58 PM (12 years, 7 months ago)

Quote:

total said:
The naptha was just bought at home depot... :shrug:
It was very clear, until mixed with the basified sludge, then it turned piss yellow...
Its the VM&P type...
Ill do a evap test tonight to see...
In the meantime, do i need to heat the naptha to get the crystals to redissolve?




Hmmmm so the only time the Naptha turned colored was once in contact with your basified MHRB solution?  It sounds like you just pulled some extra garbage with your DMT.  A simple Re-crystallization should take care of this, most likely.

Also I would still do the evaporation test on your solvent, just to make sure you didn't get an extra-dirty batch of Naptha, for whatever reason.

It depends on ambient temps where you are at.  If its warm enough ambient temperature, your Xtals should dissolve fine in the Naptha.

But if you are looking to re-crystallize anyways, you're going to have to heat your Naptha for that regardless.

Hope this helps and good luck!


Extras: Filter Print Post Top
Offlinetotal
Post Office Tyvek Advocator
Male User Gallery


Folding@home Statistics
Registered: 10/03/04
Posts: 11,405
Last seen: 6 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: Dave Bowman]
    #14579778 - 06/08/11 01:18 PM (12 years, 7 months ago)

Can you point me to a good recrystalization tek?


Extras: Filter Print Post Top
Offlinetotal
Post Office Tyvek Advocator
Male User Gallery


Folding@home Statistics
Registered: 10/03/04
Posts: 11,405
Last seen: 6 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: total]
    #14579807 - 06/08/11 01:25 PM (12 years, 7 months ago)

Nm...
In the Tek i found, they are doing it with dry finished product...
Think heating naptha and adding it to the sludge is ok?


Extras: Filter Print Post Top
Offlinetotal
Post Office Tyvek Advocator
Male User Gallery


Folding@home Statistics
Registered: 10/03/04
Posts: 11,405
Last seen: 6 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: total]
    #14579955 - 06/08/11 01:59 PM (12 years, 7 months ago)

So I heated up some naptha, and then swirled it around for a few mins...
I was left with 2 layers...

Bottom layer was the nasty sludge...


And then a nice piss colored Top layer of Naptha


Throwing it in the freezer and hoping all goes well! :super:


Extras: Filter Print Post Top
Invisiblejohn6886
Stranger
Female

Registered: 08/04/10
Posts: 320
Re: DMT Extraction of MHRB ?'s *DELETED* [Re: total]
    #14579996 - 06/08/11 02:09 PM (12 years, 7 months ago)

Post deleted by john6886

Reason for deletion: asd



Extras: Filter Print Post Top
Offlinetotal
Post Office Tyvek Advocator
Male User Gallery


Folding@home Statistics
Registered: 10/03/04
Posts: 11,405
Last seen: 6 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: john6886]
    #14580012 - 06/08/11 02:15 PM (12 years, 7 months ago)

Yes i did...
I never thought of adding a larger bottom water layer for the impurities to fall to...
If this freeze doesnt handle it, ill give that a go...

Should i bring the ph of the water up to 13?


Extras: Filter Print Post Top
Invisiblejohn6886
Stranger
Female

Registered: 08/04/10
Posts: 320
Re: DMT Extraction of MHRB ?'s *DELETED* [Re: total]
    #14580081 - 06/08/11 02:27 PM (12 years, 7 months ago)

Post deleted by john6886

Reason for deletion: asd



Extras: Filter Print Post Top
Offlinetotal
Post Office Tyvek Advocator
Male User Gallery


Folding@home Statistics
Registered: 10/03/04
Posts: 11,405
Last seen: 6 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: john6886]
    #14580098 - 06/08/11 02:29 PM (12 years, 7 months ago)

Thats the tek i was following...

When you say...
Quote:

john6886 said:
I took my entire solution and added another 800 ML's of water and this seemed to fix my woes.



Do you mean you dumped your naptha back in with the root bark and added more water?
Or just added water to the naptha?


Extras: Filter Print Post Top
Invisiblejohn6886
Stranger
Female

Registered: 08/04/10
Posts: 320
Re: DMT Extraction of MHRB ?'s *DELETED* [Re: total]
    #14580118 - 06/08/11 02:34 PM (12 years, 7 months ago)

Post deleted by john6886

Reason for deletion: asd



Extras: Filter Print Post Top
Offlinetotal
Post Office Tyvek Advocator
Male User Gallery


Folding@home Statistics
Registered: 10/03/04
Posts: 11,405
Last seen: 6 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: john6886]
    #14580144 - 06/08/11 02:39 PM (12 years, 7 months ago)

Ill double the water/lye solution on my next batch...
Im just to far ahead atm to start back over...
I've been told recrystalization can clean it :shrug:
So i might as well try that...

I think maybe next time 2x water, 2x lye, and 1.5x mhrb


Extras: Filter Print Post Top
Offlinetotal
Post Office Tyvek Advocator
Male User Gallery


Folding@home Statistics
Registered: 10/03/04
Posts: 11,405
Last seen: 6 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: total]
    #14580148 - 06/08/11 02:40 PM (12 years, 7 months ago)

Oh John...
What was your avg yield with this STB tek off 100g bark?


Extras: Filter Print Post Top
Invisiblejohn6886
Stranger
Female

Registered: 08/04/10
Posts: 320
Re: DMT Extraction of MHRB ?'s *DELETED* [Re: total]
    #14580169 - 06/08/11 02:44 PM (12 years, 7 months ago)

Post deleted by john6886

Reason for deletion: asd



Extras: Filter Print Post Top
Offlinetotal
Post Office Tyvek Advocator
Male User Gallery


Folding@home Statistics
Registered: 10/03/04
Posts: 11,405
Last seen: 6 months, 24 days
Re: DMT Extraction of MHRB ?'s [Re: john6886]
    #14580289 - 06/08/11 03:04 PM (12 years, 7 months ago)

So after the freeze, the crystals came out much less Orange/yellow...
Def Cleaner stuff! :super:
Im gonna let this completely dry and then try another recrystalization with as little naptha as possible!


Extras: Filter Print Post Top
Offlineheratogwea
 User Gallery


Registered: 05/05/11
Posts: 607
Last seen: 3 years, 8 months
Re: DMT Extraction of MHRB ?'s [Re: total]
    #14584452 - 06/09/11 09:33 AM (12 years, 7 months ago)

Quote:

total said:
So after the freeze, the crystals came out much less Orange/yellow...
Def Cleaner stuff! :super:
Im gonna let this completely dry and then try another recrystalization with as little naptha as possible!




from the picture it looks kinda goopy.looks like you got some moisture in your jar.


Extras: Filter Print Post Top
Jump to top Pages: 1 | 2 | Next >  [ show all ]

Shop: PhytoExtractum Kratom Powder for Sale, Maeng Da Thai Kratom Leaf Powder   Bridgetown Botanicals CBD Concentrates   Kraken Kratom Red Vein Kratom


Similar ThreadsPosterViewsRepliesLast post
* Best DMT extraction guide? Plok 115,590 14 09/19/10 10:27 PM
by greystealth
* Whats easier...a mescaline extraction or a DMT extraction?
( 1 2 all )
PsillyNilly 23,535 23 03/23/11 04:39 PM
by fung
* DMT extraction time skullfarmer1979 3,264 5 09/17/04 06:48 AM
by skullfarmer1979
* DMT extraction experimental yields (not theoretical) ShroomyTunes 2,985 5 10/14/05 11:09 PM
by Koala Koolio
* Help with DMT extraction Tangerines 3,115 14 10/22/05 10:36 AM
by djred
* DMT Extraction -- quick question! Plok 1,941 4 09/03/05 09:39 PM
by CandyLand
* Performing a Legal DMT extraction PoopShooter 9,761 8 03/13/05 05:04 PM
by rdnp2035
* DMT Extractions EvilGir 4,324 4 02/13/03 05:09 PM
by psychopsilocyber

Extra information
You cannot start new topics / You cannot reply to topics
HTML is disabled / BBCode is enabled
Moderator: psilocybinjunkie, Rose, mushboy, LogicaL Chaos, Northerner, bodhisatta
3,088 topic views. 2 members, 37 guests and 15 web crawlers are browsing this forum.
[ Show Images Only | Sort by Score | Print Topic ]
Search this thread:

Copyright 1997-2024 Mind Media. Some rights reserved.

Generated in 0.029 seconds spending 0.006 seconds on 16 queries.