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pnus
Stranger


Registered: 06/03/10
Posts: 23
Last seen: 11 years, 10 months
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FML SPILLED NAPTHA!!!! Help Me Please
#14501032 - 05/23/11 08:19 PM (12 years, 8 months ago) |
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OMFG!!!!
right before i put the naptha into the freezer i dropped it and spilled on the floor...
I squeegeed some of it up with a paper towl and now their is only like 5% left...
Can i add more naptha to the sludge for another pull?
how much did i just lose on that first pull??
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erikksonb
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Registered: 12/22/10
Posts: 344
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: pnus]
#14501126 - 05/23/11 08:38 PM (12 years, 8 months ago) |
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Relax, smoke some bud. maybe rinse the paper towel with fresh naptha and save that and throw it back into the sludge jar.
We can't predict how much you lost, you lack important details. Also it doesn't really get lost, only transferred say to that paper towel. So getting it out of there is worth a shot by saturating/rinsing the towel with new naptha.
-------------------- Imagine a world of Peace.

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muistrue
Inspired by the mystery


Registered: 03/20/05
Posts: 12,899
Loc: Behind the Redwoods
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: pnus]
#14501160 - 05/23/11 08:42 PM (12 years, 8 months ago) |
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Let it dry then scrape the crystals off your floor.
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pnus
Stranger


Registered: 06/03/10
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: pnus]
#14501177 - 05/23/11 08:45 PM (12 years, 8 months ago) |
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yea i just squeezed some of the naptha back into the jar, and put it into the freezer.
added some more naptha to the 240gram MHRB sludge
hopefully i see some crystals on the floor, my floors kinda dirty tho.. LOL
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shadowman-x
Useless hippy.



Registered: 02/15/11
Posts: 1,840
Loc: PNW
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: pnus]
#14501255 - 05/23/11 08:56 PM (12 years, 8 months ago) |
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Rinse the towel with fresh naptha. Scrape up the DMT that will be where the naptha evaporated if your floor is wood or laminate. Chill.
-------------------- knock me down i'll just come back runnin' knock you down it won't be long now
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PorcupinesRevenge
Porcupine


Registered: 05/14/10
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: pnus]
#14501263 - 05/23/11 08:58 PM (12 years, 8 months ago) |
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meh, you'll just loose one pull. put in some new naphtha. how much bark are you using? if its between 50-100 grams, you probably lost a few hundred mgs, nothing to worry about cause the second pulls usually just as good as the first (for me at least)
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pnus
Stranger


Registered: 06/03/10
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Last seen: 11 years, 10 months
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Quote:
PorcupinesRevenge said: meh, you'll just loose one pull. put in some new naphtha. how much bark are you using? if its between 50-100 grams, you probably lost a few hundred mgs, nothing to worry about cause the second pulls usually just as good as the first (for me at least)
nice i used half pound, about 248 grams (they sent me a little extra)
i think i might have lost around a gram probably less
Quote:
shadowman-x said: Rinse the towel with fresh naptha. Scrape up the DMT that will be where the naptha evaporated if your floor is wood or laminate. Chill.
thanks i almost threw it out, i will let use it on the next pull
How long do you guys wait until you pull the naptha from the sludge? Marsofold's tek says 4 hours i believe.
Edited by pnus (05/23/11 09:07 PM)
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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: pnus]
#14501356 - 05/23/11 09:10 PM (12 years, 8 months ago) |
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Wait longer. I do 24 hours or more. As unnecessary as it might be, I believe it is beneficial. Also warm up the container before you pull. Always be patient when extracting dmt, it will pay off
But that is just from my experience after pulling 13+g from a kilo.
-------------------- Imagine a world of Peace.

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muistrue
Inspired by the mystery


Registered: 03/20/05
Posts: 12,899
Loc: Behind the Redwoods
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: pnus]
#14501396 - 05/23/11 09:16 PM (12 years, 8 months ago) |
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Quote:
pnus said: How long do you guys wait until you pull the naptha from the sludge? Marsofold's tek says 4 hours i believe.
As long as it takes the layers to separate completely which shouldn't be more than a few minutes. Letting it sit any longer is unnecessary.
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pnus
Stranger


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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: muistrue]
#14501428 - 05/23/11 09:19 PM (12 years, 8 months ago) |
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Quote:
FractalDust said:
Quote:
pnus said: How long do you guys wait until you pull the naptha from the sludge? Marsofold's tek says 4 hours i believe.
As long as it takes the layers to separate completely which shouldn't be more than a few minutes. Letting it sit any longer is unnecessary.
Dont you see more yellow if i swish it around and leave it in for a longer period? im new to this so i wouldnt know lol
Quote:
erikksonb said: Wait longer. I do 24 hours or more. As unnecessary as it might be, I believe it is beneficial. Also warm up the container before you pull. Always be patient when extracting dmt, it will pay off
But that is just from my experience after pulling 13+g from a kilo.
wow thats allot LOL
maybe i didnt lose that much, my first pull i only waited 4 hours.
I guess i will wait till tomorrow for the next one?
I was hoping to go into hyperspace tomorrow =/
Hopefully their will be some crystals in the little amount that i was able the salvage...
At least i have some shroomies colonizing, and MHRB is pretty cheap
Edited by pnus (05/23/11 09:22 PM)
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muistrue
Inspired by the mystery


Registered: 03/20/05
Posts: 12,899
Loc: Behind the Redwoods
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: pnus]
#14501477 - 05/23/11 09:24 PM (12 years, 8 months ago) |
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Quote:
pnus said: I see more yellowish if i swish it around and leave it in for a longer period. im new to this so i wouldnt know lol
The DMT migrates into the non polar when the basic solution is mixing with the solvent. Once they separate the DMT is pulled along with the solvent into the top layer and at that point you can pull it and add more solvent for the next pull. No more DMT will migrate into the non polar layer once they have separated, that's impossible so it's unnecessary to wait any longer once they've separated.
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erikksonb
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Registered: 12/22/10
Posts: 344
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Last seen: 9 years, 6 months
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: muistrue]
#14501490 - 05/23/11 09:25 PM (12 years, 8 months ago) |
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I try to swirl and heat multiple times before pulling.
-------------------- Imagine a world of Peace.

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muistrue
Inspired by the mystery


Registered: 03/20/05
Posts: 12,899
Loc: Behind the Redwoods
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: erikksonb]
#14501508 - 05/23/11 09:28 PM (12 years, 8 months ago) |
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Quote:
erikksonb said: I try to swirl and heat multiple times before pulling.
That won't hurt but it's unnecessary and time consuming. You can do 4-5 pulls within an hour and get all the DMT so why waste time heating and swirling multiple times over the period of days?
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pnus
Stranger


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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: muistrue]
#14501534 - 05/23/11 09:34 PM (12 years, 8 months ago) |
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Quote:
FractalDust said:
Quote:
pnus said: I see more yellowish if i swish it around and leave it in for a longer period. im new to this so i wouldnt know lol
The DMT migrates into the non polar when the basic solution is mixing with the solvent. Once they separate the DMT is pulled along with the solvent into the top layer and at that point you can pull it and add more solvent for the next pull. No more DMT will migrate into the non polar layer once they have separated, that's impossible so it's unnecessary to wait any longer once they've separated.
thanks allot, i just have a limited amount of jar space and solvent. good to know i can refill the stupid jar again ASAP =) and not wait till tomorrow
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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: muistrue]
#14501540 - 05/23/11 09:35 PM (12 years, 8 months ago) |
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Quote:
FractalDust said:
Quote:
erikksonb said: I try to swirl and heat multiple times before pulling.
That won't hurt but it's unnecessary and time consuming. You can do 4-5 pulls within an hour and get all the DMT so why waste time heating and swirling multiple times over the period of days?
days, hah well i've been working on this same kilo for 3 months now hah. doing a pull once every week or two.
I would have to agree with your logic though. Just comes down to me being lazy and having an excess amount of crystal.
-------------------- Imagine a world of Peace.

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pnus
Stranger


Registered: 06/03/10
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: muistrue]
#14501602 - 05/23/11 09:46 PM (12 years, 8 months ago) |
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Quote:
FractalDust said:
Quote:
erikksonb said: I try to swirl and heat multiple times before pulling.
That won't hurt but it's unnecessary and time consuming. You can do 4-5 pulls within an hour and get all the DMT so why waste time heating and swirling multiple times over the period of days?
Could i use the same naptha i froze and withdrew crystals from?
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bholzer
quasi-scientist



Registered: 03/22/11
Posts: 2,409
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: pnus]
#14501633 - 05/23/11 09:51 PM (12 years, 8 months ago) |
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Quote:
pnus said:
Quote:
FractalDust said:
Quote:
erikksonb said: I try to swirl and heat multiple times before pulling.
That won't hurt but it's unnecessary and time consuming. You can do 4-5 pulls within an hour and get all the DMT so why waste time heating and swirling multiple times over the period of days?
Could i use the same naptha i froze and withdrew crystals from?
You could, but it would take a while because you'd have to let all your crystals precip out before you could do another pull. A waste of time really.
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Use these substances wisely, they have the ability to cause life altering realizations.
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muistrue
Inspired by the mystery


Registered: 03/20/05
Posts: 12,899
Loc: Behind the Redwoods
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: pnus]
#14501634 - 05/23/11 09:51 PM (12 years, 8 months ago) |
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Quote:
pnus said: Could i use the same naptha i froze and withdrew crystals from?
Absolutely.
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pnus
Stranger


Registered: 06/03/10
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: muistrue]
#14501665 - 05/23/11 09:56 PM (12 years, 8 months ago) |
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Quote:
FractalDust said:
Quote:
pnus said: Could i use the same naptha i froze and withdrew crystals from?
Absolutely. 
thanks again ^^
How long would you guys think my fridge would take to freeze/make crystals on max settings?
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muistrue
Inspired by the mystery


Registered: 03/20/05
Posts: 12,899
Loc: Behind the Redwoods
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Re: FML SPILLED NAPTHA!!!! Help Me Please [Re: pnus]
#14501686 - 05/23/11 10:00 PM (12 years, 8 months ago) |
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Quote:
pnus said: How long would you guys think my fridge would take to freeze/make crystals on max settings?
It's really easy to know when they're ready. When you put the jar in it will be clear or with a yellowish tint. As the temperature drops the crystals will begin precipitating and the solution will get foggy and you will see crystals begin to form. Once the solution goes clear again with the crystals formed you know it's done, shouldn't take more than 3-4 hours.
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