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Offlinehippi1287
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Registered: 05/03/11
Posts: 15
Last seen: 12 years, 5 months
Precipitation problems !!
    #14444361 - 05/13/11 08:56 AM (12 years, 8 months ago)

Someone has done a two pound spice extract and cannot get the spice to crystallize. Someone is panicking due to amoun of materials and money spent. Any help would be greatly appreciated!!


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Offlineabica
Intrepid Warlock's Apprentice
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Registered: 04/01/08
Posts: 443
Loc: The River City
Last seen: 11 years, 2 months
Re: Precipitation problems !! [Re: hippi1287]
    #14444387 - 05/13/11 09:05 AM (12 years, 8 months ago)

Evaporate some solvent (evap at least 25%), make sure freezer's max cold, and try again for 24hr.  Meanwhile, make sure aqueous solution is at proper ph 12.5-13 and give the next pull 2 days to soak with agitation every now and then.  Solvent "should" be piss yellow when pulled off.  Failing that, next pull, let extraction vessel sit in 100F water bath for a while in addition to above.


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My first poo tub




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OfflineHarryL
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Registered: 11/16/10
Posts: 8,070
Loc: Washington State
Last seen: 4 years, 8 months
Re: Precipitation problems !! [Re: abica]
    #14446429 - 05/13/11 04:28 PM (12 years, 8 months ago)

Ok... Let's get some more info

1) sounds like your doing a 1'kg extraction, right?
2) how much water and how much solvent are you using?
3) how big is your container?
4) are you doing acid-base extraction or just base?
5) how much of what chemical(s) are you using?
6) how long did the solvent sit on the root bark?
7) is the bark ground or not?

Let's problem solve!


--------------------
Mushroom hunting:  One bad mushroom can ruin your day! Know it or throw it.


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