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uisim881988
Stranger


Registered: 05/07/11
Posts: 10
Last seen: 12 years, 8 months
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In need of help with my extraction of mhrb
#14437424 - 05/11/11 10:08 PM (12 years, 8 months ago) |
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Here we go....I will post the Tek at the end.
I followed this tek step by step but still ran into problems. When I pull the solvent out of the freezer I can see a yellow substance stuck to the bottom and a bunch of whiteish crystal particles floating all over. After A moment they settle at the bottom but then melt as I am trying to syphon off the remaining solvent. I know this is DMT because It has been tested. The first time I scraped these when still wet and most of it ended up melting into a honey like goo. Now however, they melt before I can do anything. I even let this solvent do its work for 6-10 hours before I syphon it so I know there is DMT somewhere in there. These are the conclusion I came to so let me know what you think.
1) the temperature change is too drastic; my freezer is VERY VERY cold, (the bowl burns to the touch from the cold). I read that taking it from the freezer and putting it into the refrigerator and then to a room that is 65f might help. Someone posted that they ruined many batches because the DMT melts when it goes from -30 (or however cold it is in there) to room temp. Also I was going to pour the solvent thru a filter while it is still very cold. Hoping to trap crystals
2) too much solvent; for my second pull I let about 1/4th evap(the substance was getting foggy), then stuck it in my freezer. I also turned down the temp because I read cooling down too fast may not allow something to separate from the Naptha ?
Also I found a third pull from another batch sitting in my room( I forgot about it) It has this yellow guey liquid with slightly orange things settled at the bottom. After sticking in the freezer it looked like it was solidifying. is this DMT , will anything form? here is a pic of what my pull looked like after a few days I have one more batch of 100grams MHRB left that is sitting in distilled water and Lye and I plan to use this TEK,
powder RB best u can, put in Bigass jar
mix eight TBSP lye into vessel with 750-1000ml water...mix well (it'll get warm)
carefully pour basified water right onto bark...use all of it...
mix well, it will look like motor-oil and smell like, im not sure what...fish?
add 250ml Naptha to solution...mix and mix (dont recommend shaking STB as there's no filtering or defatting and it may never fucking separate)
sit in hot water bath, mixing every 15 min or so until it gets 'color'..like hangover pee...
now u can do first pull...siphon Naptha with turkey baster into glass dish
SWIM uses fan evap at room temp...
re-cover w/Naptha repeat x3
now, add second pull to whatever is in tray- this 'seeds' tray with crystals and makes em big and scary...(do same with pull 3)
any help can be appreciated
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ephrem
Stranger

Registered: 04/29/11
Posts: 35
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Re: In need of help with my extraction of mhrb [Re: uisim881988]
#14438320 - 05/12/11 01:42 AM (12 years, 8 months ago) |
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Allright, i've had good result with this:
100 gr MHRB 1 liter water 500 mg lye 500 ml solvent
Mix water and lye and add mhrb. Don't know if it matter, but add mhrb to the water/lye mix, not the other way 'round.
Wait till water cools, add mhrb. Let it sit for 24 hours and shake now and again. Mix solvent with soup, shake it and let it separate. Repeat this for an hour. Then pull.
Put pull in very cold freezer for 24 hours. You should have lovely crystals.
So more lye, less solvent.
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uisim881988
Stranger


Registered: 05/07/11
Posts: 10
Last seen: 12 years, 8 months
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Re: In need of help with my extraction of mhrb [Re: ephrem]
#14440921 - 05/12/11 04:35 PM (12 years, 8 months ago) |
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now this happend, I just syphoned my solvent from the jar and noticed after a bit it turned light brown/yellow (when I look close it seems to kinda look like a normal extraction????? what is this??? what do I do?
I used this technique http://forums.mycotopia.net/botanica...ree-stb-2.html (HASSLE-FREE STB)
maybe I stirred too much and it needs time to settle? if so can I throw it back into the jar and run it thru again?
I do see yellow residue forming so it has dmt.......... I know NO base water got in cause I syphoned it whith a samll tube so the flow was little. I cut it off wen it got too low and I saw base water flowing through the tube
powder RB best u can, put in Bigass jar
mix eight TBSP lye into vessel with 750-1000ml water...mix well (it'll get warm)
carefully pour basified water right onto bark...use all of it...
mix well, it will look like motor-oil and smell like, im not sure what...fish?
add 250ml Naptha to solution...mix and mix (dont recommend shaking STB as there's no filtering or defatting and it may never fucking separate)
sit in hot water bath, mixing every 15 min or so until it gets 'color'..like hangover pee...
now u can do first pull...siphon Naptha with turkey baster into glass dish
SWIM uses fan evap at room temp...
I dont know how to upload a pic to the thread so u can view wat happened in my folder or wherever the hell they send them
Edited by uisim881988 (05/12/11 10:16 PM)
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ephrem
Stranger

Registered: 04/29/11
Posts: 35
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Re: In need of help with my extraction of mhrb [Re: uisim881988]
#14441428 - 05/12/11 06:29 PM (12 years, 8 months ago) |
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Keep it simple.
Don't know what else to say.
Good luck!
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bholzer
quasi-scientist



Registered: 03/22/11
Posts: 2,409
Last seen: 11 years, 7 months
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Re: In need of help with my extraction of mhrb [Re: ephrem]
#14441562 - 05/12/11 06:50 PM (12 years, 8 months ago) |
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This is how my first extraction went. It was extremely frustrating. Do move it from the freezer to the fridge, then to room temperature. When there isn't any spice on the sides of the jar, your best bet is to evap using a fan. When you do, you'll be left with either a yellow-orange goo, or white crystals, which are preferred. My first time, I had some yellow goo. I took some oregano and scrubbed my dish with it. When I smoked that oregano, I had a near breakthrough, so don't think that the yellow goo isn't good.
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Use these substances wisely, they have the ability to cause life altering realizations.
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uisim881988
Stranger


Registered: 05/07/11
Posts: 10
Last seen: 12 years, 8 months
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Re: In need of help with my extraction of mhrb [Re: bholzer]
#14442635 - 05/12/11 10:17 PM (12 years, 8 months ago) |
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what about that brown stuff? is it just too saturated
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