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Offline403Forbidden
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Registered: 01/17/11
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Receiving Different Crystals from Evap and Freeze
    #14232189 - 04/03/11 05:18 PM (12 years, 10 months ago)

So I was evaporating my solution down to super-saturation, when I fell asleep for a few hours. When I awoke, I checked my solution, and there were these beautiful crystals forming. They were clear, very crystalline, and I guess looked like a porcupine with plates rather than spikes.

However, I thought that this wasn't good, and that I can't go to the freeze precipitation with a solution like this, so I added more naphtha, evaporated down to super-saturation, before crystals formed, and then froze it.

I just took it out of the freezer, after almost 4 days, and the product isn't as appealing. There's a shit ton of small white particles. I've had this appear the last time I did an extraction, but I'm wondering if they are as good as the crystals I got during the evaporation.

Essentially, I'm wondering: based on these results, would you say that I should evaporate my next batch, rather than freeze it?

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OfflineSomeGuy
I feel better now :)
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Registered: 04/18/10
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Re: Receiving Different Crystals from Evap and Freeze [Re: 403Forbidden]
    #14232223 - 04/03/11 05:24 PM (12 years, 10 months ago)

the prob. with freezing it is you will never get it all out, so unless you plan to continually extract, you will always have dmt in solution. Evap. is the only way to get it all out anyway

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