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Offlinemicrodotty
Pro darts player!


Registered: 03/01/11 Happy 13th Shroomiversary!
Posts: 1,670
Loc: England Flag
Last seen: 6 years, 11 months
Re: Going to try to make my own LSD. [Re: 245willow19]
    #14164813 - 03/22/11 02:03 PM (12 years, 11 months ago)

why not...? any acid i make will be dynamite!

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Offlinewoutah
Royal A

Registered: 01/31/11
Posts: 159
Loc: Inside of a malnourished Flag
Last seen: 12 years, 7 months
Re: Going to try to make my own LSD. [Re: microdotty]
    #14164853 - 03/22/11 02:10 PM (12 years, 11 months ago)

Okay;


LSD-25 Synthesis from "Psychedelic Guide to the Preparation of the Eucharist":
Preparatory arrangements:
Starting material may be any lysergic acid derivative, from ergot on rye grain or from culture, or morning glory seeds or from synthetic sources.
Preparation #1 uses any amide, or lysergic acid as starting material. Preparations #2 and #3 must start with lysergic acid only, prepared from the amides as follows: 10 g of any lysergic acid amide from various natural sources dissolved in 200 ml of methanoic KOH solution and the methanol removed immediately in vacuo. The residue is treated with 200 ml of an 8% aqueous solution of KOH and the mixture heated on a steam bath for one hour. A stream of nitrogen gas is passed through the flask during heating and the evolved NH3 gas may be titrated is HCl
to follow the reaction. The alkaline solution is made neutral to congo red with tartaric acid, filtered,
cleaned by extraction with ether, the aqueous solution filtered and evaporated. Digest with MeOH to
remove some of the coloured material from the crystals of lysergic acid.
Arrange the lighting in the lab similarly to that of a dark room. Use photographic red and yellow safety lights, as lysergic acid derivatives are decomposed when light is present. Rubber gloves must be worn due to the highly poisonous nature of ergot alkaloids. A hair drier, or, better, a flash evaporator, is necessary to speed up steps where evaporation is necessary.
Preparation #1
Step I.
Use Yellow light Place one volume of powdered ergot alkaloid material in a tiny round bottom flask and add two
volumes of anhydrous hydrazine. An alternate procedure uses a sealed tube in which the reagents are
heated at 112 C. The mixture is refluxed (or heated) for 30 minutes. Add 1.5 volumes of H2O and boil
15 minutes. On cooling in the refrigerator, isolysergic acid hydrazide is crystallised.
Step II.
Use Red light Chill all reagents and have ice handy. Dissolve 2.82 g hydrazine rapidly in 100 ml 0.1 N ice-cold HCl using an ice bath to keep the reaction vessel at 0 C. 100 ml ice-cold 0.1 N NaNO2 is added and after 2 to 3 minutes vigorous stirring, 130 ml more HCl is added drop wise with vigorous stirring again in an ice bath. After 5 minutes, neutralise the solution with NaHCO3 saturated sol. and extract with ether. Remove the aqueous solution and try to dissolve the gummy substance in ether. Adjust the ether solution by adding 3 g diethylamide per 300 ml ether extract. Allow to stand in the dark, gradually warming up to 20 C over a period of 24 hours. Evaporate in vacuum and treat as indicated in the purification section for conversion of iso-lysergic amides to lysergic acid amide

Preparation #2
Step I.
Use Yellow light 5.36 g of d-lysergic acid are suspended in 125 ml of acetonitrile and the suspension cooled to about -20 C in a bath of acetone cooled with dry ice. To the suspension is added a cold (-20 C) solution of 8.82 g of trifluoroacetic anhydride in 75 ml of acetonitrile. The mixture is allowed to stand at -20 C for about 1.5 hours during which the suspended material dissolves, and the d-lysergic acid is
converted to the mixed anhydride of lysergic and trifluoroacetic acids. The mixed anhydride can be separated in the form of an oil by evaporating the solvent in vacuo at a temperature below 0 C, but this is not necessary. Everything must be kept anhydrous.
Step II.
Use Yellow light The solution of mixed anhydrides in acetonitrile from Step I is added to 150 ml of a second solution of acetonitrile containing 7.6 g of diethylamide. The mixture is held in the dark at room temperature for about 2 hours. The acetonitrile is evaporated in vacuo, leaving a residue of LSD-25 plus other impurities. The residue is dissolved in 150 ml of chloroform and 20 ml of ice water. The
chloroform layer is removed and the aqueous layer is extracted with several portions of chloroform. The chloroform portions are combined and in turn washed with four 50 ml portions of ice-cold water. The chloroform solution is then dried over anhydrous Na2SO4 and evaporated in vacuo.
Preparation #3
This procedure gives good yield and is very fast with little iso-lysergic acid being formed (its effect are mildly unpleasant). However, the stoichiometry must be exact or yields will drop.
Step I.
Use White light Sulphur trioxide is produced in anhydrous state by carefully decomposing anhydrous ferric sulphate at approximately 480 C. Store under anhydrous conditions.
Step II.
Use White light A carefully dried 22 litre RB flask fitted with an ice bath, condenser, dropping funnel and mechanical stirrer is charged with 10 to 11 litres of dimethylformamide (freshly distilled under reduced pressure). The condenser and dropping funnel are both protected against atmospheric moisture. 2 lb of sulphur trioxide (Sulfan B) are introduced drop wise, very cautiously stirring, during 4 to 5 hours. The
temperature is kept at 0-5 C throughout the addition. After the addition is complete, the mixture is stirred for 1-2 hours until some separated, crystalline sulphur trioxide-dimethylformamide complex has dissolved. The reagent is transferred to an air- tight automatic pipette for convenient dispensing, and
kept in the cold. Although the reagent, which is colourless, may change from yellow to red, its efficiency remains unimpaired for three to four months in cold storage. An aliquot is dissolved in water and titrated with standard NaOH to a phenolphthalein end point.

Step III.

Use Red light A solution of 7.15 g of d-lysergic acid mono hydrate (25 mmol) and 1.06 g of lithium hydroxide hydrate (25 mmol) in 200 ml of MeOH is prepared. The solvent is distilled on the steam bath under reduced pressure. the residue of glass-like lithium lysergate is dissolved in 400 ml of anhydrous dimethyl formamide. From this solution about 200 ml of the dimethyl formamide is distilled off at 15 ml pressure through a 12 inch helices packed column. the resulting anhydrous solution of lithium lysergate left behind is cooled to 0 C and, with stirring, treated rapidly with 500 ml of SO3-DMF solution (1.00 molar). The mixture is stirred in the cold for 10 minutes and then 9.14 g (125.0 mmol) of diethylamide is added. The stirring and cooling are continued for 10 minutes longer, when 400 ml of water is added to decompose the reaction complex. After mixing thoroughly, 200 ml of saturated aqueous saline solution is added. The amide product is isolated by repeated extraction with 500 ml portions of ethylene dichloride. the combined extract is dried and then concentrated to a syrup under reduced pressure. Do not heat up the syrup during concentration. the LSD may crystallise out, but the crystals and the mother liquor may be chromatographed according to the instructions on purification.
Purification of LSD-25
The material obtained by any of these three preparations may contain both lysergic acid and iso-lysergic acid amides. Preparation #1 contains mostly iso-lysergic diethylamide and must be converted prior to separation. For this material, go to Step II first.
Step I.
Use darkroom and follow with a long wave UV The material is dissolved in a 3:1 mixture of benzene and chloroform. Pack the chromatography column with a slurry of basic alumina in benzene so that a 1 inch column is six inches long. Drain the solvent to the top of the alumina column and carefully add an aliquot of the LSD-solvent solution
containing 50 ml of solvent and 1 g LSD. Run this through the column, following the fastest moving
fluorescent band. After it has been collected, strip the remaining material from the column by washing
with MeOH. Use the UV light sparingly to prevent excessive damage to the compounds. Evaporate the second fraction in vacuo and set aside for Step II. The fraction containing the pure LSD is concentrated in vacuo and the syrup will crystallise slowly. This material may be converted to the tartrate by tartaric acid and the LSD tartrate conveniently crystallised. MP 190-196 C.
Step II.
Use Red light Dissolve the residue derived from the methanol stripping of the column in a minimum amount of alcohol. Add twice that volume of 4 N alcoholic KOH solution and allow the mixture to stand at room temperature for several hours. Neutralise with dilute HCl, make slightly basic with NH4OH and extract with chloroform or ethylene dichloride as in preparations #1 or #2. Evaporate in vacuo and chromatograph as in the previous step

Note: Lysergic acid compounds are unstable to heat, light and oxygen. In any form it helps to add ascorbic acid as an anti-oxidant, keeping the container tightly closed, light-tight with aluminum foil, and in a refrigerator


GOOD LUCK


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Offlinemicrodotty
Pro darts player!


Registered: 03/01/11 Happy 13th Shroomiversary!
Posts: 1,670
Loc: England Flag
Last seen: 6 years, 11 months
Re: Going to try to make my own LSD. [Re: woutah]
    #14164895 - 03/22/11 02:18 PM (12 years, 11 months ago)

SIMPLES! :awecid2::lsdabc::slomo:

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Offline245willow19

Registered: 06/14/10
Posts: 4,861
Last seen: 8 years, 22 days
Re: Going to try to make my own LSD. [Re: microdotty]
    #14164955 - 03/22/11 02:30 PM (12 years, 11 months ago)

Quote:

microdotty said:
why not...? any acid i make will be dynamite!



well if its that good, then cook me some BROTHER:psychsplit:
but your little child Science set looks like a Bomb making Taliban Set from Dubai!!


--------------------
....

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Offlinemicrodotty
Pro darts player!


Registered: 03/01/11 Happy 13th Shroomiversary!
Posts: 1,670
Loc: England Flag
Last seen: 6 years, 11 months
Re: Going to try to make my own LSD. [Re: 245willow19]
    #14164975 - 03/22/11 02:34 PM (12 years, 11 months ago)

Here we go im all set up now... wish me luck guys!!


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Offline1tokeovrtheline
life=painfully beautiful
 User Gallery


Registered: 04/12/10
Posts: 866
Loc: innerverse&universe, surrealis...
Last seen: 2 years, 4 months
Re: Going to try to make my own LSD. [Re: microdotty]
    #14164978 - 03/22/11 02:35 PM (12 years, 11 months ago)

.

Edited by 1tokeovrtheline (03/22/11 03:10 PM)

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Offline1tokeovrtheline
life=painfully beautiful
 User Gallery


Registered: 04/12/10
Posts: 866
Loc: innerverse&universe, surrealis...
Last seen: 2 years, 4 months
Re: Going to try to make my own LSD. [Re: microdotty]
    #14164985 - 03/22/11 02:37 PM (12 years, 11 months ago)

Quote:

microdotty said:
Here we go im all set up now... wish me luck guys!!





:smirk:

odd how that looks EXACTLY like casey hardisons bedroom....lol

his lab was appraised at $50,000 btw


--------------------


Music, business as usual
Mi' spliff and Guiness as usual
Highgrade we puffin as usual
Fight down the system as usual
The system fight we down as usual
The cops dem a watch we as usual
And a we a watch the cops as usual

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Offline245willow19

Registered: 06/14/10
Posts: 4,861
Last seen: 8 years, 22 days
Re: Going to try to make my own LSD. [Re: microdotty]
    #14165029 - 03/22/11 02:45 PM (12 years, 11 months ago)

Quote:

microdotty said:
Here we go im all set up now... wish me luck guys!!






Perrrrrrrrrrty LAB!!!
but seriously it looks like a Bomb making Set!

British Soldiers LSD


--------------------
....

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Offlinemicrodotty
Pro darts player!


Registered: 03/01/11 Happy 13th Shroomiversary!
Posts: 1,670
Loc: England Flag
Last seen: 6 years, 11 months
Re: Going to try to make my own LSD. [Re: 1tokeovrtheline]
    #14165039 - 03/22/11 02:47 PM (12 years, 11 months ago)

Quote:

1tokeovrtheline said:
Quote:

microdotty said:
Here we go im all set up now... wish me luck guys!!





:smirk:

odd how that looks EXACTLY like casey hardisons bedroom....lol

his lab was appraised at $50,000 btw



who is casey hardison?

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InvisibleshLong
Male User Gallery


Registered: 03/04/10
Posts: 25,330
Loc: 'sconsin Flag
Re: Going to try to make my own LSD. [Re: microdotty]
    #14165154 - 03/22/11 03:08 PM (12 years, 11 months ago)

Quote:

microdotty said:

who is casey hardison?



http://www.brightoncity.com/martyrdom.html

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Offlinemicrodotty
Pro darts player!


Registered: 03/01/11 Happy 13th Shroomiversary!
Posts: 1,670
Loc: England Flag
Last seen: 6 years, 11 months
Re: Going to try to make my own LSD. [Re: shLong]
    #14165240 - 03/22/11 03:18 PM (12 years, 11 months ago)

Quote:

shLong said:
Quote:

microdotty said:

who is casey hardison?



http://www.brightoncity.com/martyrdom.html




Just read that link about him he is a fuckin legend!! Can't believe the harsh sentance he recieved for making LSD, yet it was a pretty dumb thing to do sending ecstasy through the mail...

Yet i praise the man!

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Offlinestarlight
Stranger

Registered: 03/22/11
Posts: 17
Last seen: 12 years, 10 months
Re: Going to try to make my own LSD. [Re: shLong]
    #14165274 - 03/22/11 03:22 PM (12 years, 11 months ago)

good luck on making it when u do pass it my way :smile::thumbup:

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Offline1tokeovrtheline
life=painfully beautiful
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Registered: 04/12/10
Posts: 866
Loc: innerverse&universe, surrealis...
Last seen: 2 years, 4 months
Re: Going to try to make my own LSD. [Re: microdotty]
    #14165290 - 03/22/11 03:25 PM (12 years, 11 months ago)

he didn't directly get caught because he sent it through the mail, the people he was sending it to in philly ratted him out.
he actually didn't get as harsh of a sentence as pickard either (pickard got a life sentence, in part thanks to neurosoup testifying against him for her own amnesty :mad2:)




--------------------


Music, business as usual
Mi' spliff and Guiness as usual
Highgrade we puffin as usual
Fight down the system as usual
The system fight we down as usual
The cops dem a watch we as usual
And a we a watch the cops as usual

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InvisibleNiffla
Male User Gallery

Registered: 06/09/08
Posts: 47,333
Loc: Texas
Re: Going to try to make my own LSD. [Re: microdotty]
    #14165292 - 03/22/11 03:26 PM (12 years, 11 months ago)

Quote:

microdotty said:
Here we go im all set up now... wish me luck guys!!






LMAO!


--------------------

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InvisibleNiffla
Male User Gallery

Registered: 06/09/08
Posts: 47,333
Loc: Texas
Re: Going to try to make my own LSD. [Re: Niffla]
    #14165304 - 03/22/11 03:29 PM (12 years, 11 months ago)

Yours looks a bit more intricate than mine, micro.



--------------------

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OfflineToltecatl
Psychonaut
Male

Registered: 07/29/10
Posts: 641
Loc: Tardis
Last seen: 10 years, 9 months
Re: Going to try to make my own LSD. [Re: 1tokeovrtheline]
    #14165305 - 03/22/11 03:29 PM (12 years, 11 months ago)

.


--------------------

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Offlinemicrodotty
Pro darts player!


Registered: 03/01/11 Happy 13th Shroomiversary!
Posts: 1,670
Loc: England Flag
Last seen: 6 years, 11 months
Re: Going to try to make my own LSD. [Re: 1tokeovrtheline]
    #14165414 - 03/22/11 03:57 PM (12 years, 11 months ago)

Quote:

1tokeovrtheline said:
he didn't directly get caught because he sent it through the mail, the people he was sending it to in philly ratted him out.
he actually didn't get as harsh of a sentence as pickard either (pickard got a life sentence, in part thanks to neurosoup testifying against him for her own amnesty :mad2:)







20 Years in UK is longer than most people who get sentanced for life do in the UK, you can get a life sentance in the UK and only do around 12-15 years!
Nerosoup testifyied against pickard?? first i knew.. she aint made any videos about that on youtube the bitch!

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Offline1tokeovrtheline
life=painfully beautiful
 User Gallery


Registered: 04/12/10
Posts: 866
Loc: innerverse&universe, surrealis...
Last seen: 2 years, 4 months
Re: Going to try to make my own LSD. [Re: microdotty]
    #14165475 - 03/22/11 04:10 PM (12 years, 11 months ago)

actually she did make a video about it and a book (two I think but idk if the other one is about the pickard bust), some interviews, etc. she even admitted that she left some parts out of her testimony that would've incriminated herself further


--------------------


Music, business as usual
Mi' spliff and Guiness as usual
Highgrade we puffin as usual
Fight down the system as usual
The system fight we down as usual
The cops dem a watch we as usual
And a we a watch the cops as usual

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Offlinesaxx
Stranger

Registered: 02/08/10
Posts: 3,351
Last seen: 9 years, 10 months
Re: Going to try to make my own LSD. [Re: 1tokeovrtheline]
    #14165545 - 03/22/11 04:24 PM (12 years, 11 months ago)

Shroomery moto : neurosoup is a hoe


--------------------
sucking dick for drink tickets
at the free bar at my cousin's bat mitzvah

zappateer said:
I'm not wasting time at school. I'm gaining hella knowledge and life experience, not trying to use my degree for financial gain.

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Offlinemicrodotty
Pro darts player!


Registered: 03/01/11 Happy 13th Shroomiversary!
Posts: 1,670
Loc: England Flag
Last seen: 6 years, 11 months
Re: Going to try to make my own LSD. [Re: 1tokeovrtheline]
    #14165675 - 03/22/11 04:45 PM (12 years, 11 months ago)

Quote:

1tokeovrtheline said:
actually she did make a video about it and a book (two I think but idk if the other one is about the pickard bust), some interviews, etc. she even admitted that she left some parts out of her testimony that would've incriminated herself further



I didn't even know she was his mate! What a bitch!... have you got a link to the video?

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