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Kraken Kratom Shop: Red Vein Kratom

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OfflineDscid
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Registered: 03/27/08
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STB DMT final pull -> evap?
    #14063313 - 03/03/11 09:53 PM (12 years, 10 months ago)

This last pull has very little crystals stuck to the sides (all floaters)- can I just evap the 1/2 pint jar of Naptha/DMT?  At room temp , does the Naptha evap and leaves the crystals, or do they lose crystal form...and evap with it?


Edited by Dscid (03/03/11 10:43 PM)


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OfflineR2-D2
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Registered: 12/14/10
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Re: STB DMT final pull -> evap? [Re: Dscid]
    #14063696 - 03/03/11 10:55 PM (12 years, 10 months ago)

Yeah that should work just fine


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OfflineThat.X.Jester
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Registered: 02/04/11
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Re: STB DMT final pull -> evap? [Re: R2-D2]
    #14063739 - 03/03/11 11:06 PM (12 years, 10 months ago)

You may have to heat it up (safely) but make sure all the crystals are redesolved, and then let it evap.

All the small crystals should reform as a couple larger, very nice looking crystals.


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OfflineDscid
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Re: STB DMT final pull -> evap? [Re: That.X.Jester]
    #14064056 - 03/04/11 12:04 AM (12 years, 10 months ago)

Before I do -  I would like to understand what heating up the Naptha accomplishes, as opposed to just room temp.  Just for understanding :smile:

Thanks though, at least I have nothing to worry about :smile:


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OfflineDscid
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Re: STB DMT final pull -> evap? [Re: Dscid]
    #14065815 - 03/04/11 11:25 AM (12 years, 10 months ago)

So I evaporated overnight with two jars - one with 37.5ml and the other with 75ml. 

The smaller jar has finished, but it is COMPLETELY yellow crystal.

I am aware that each pull, the yield is less and more yellow, but the two pulls before it were as white as can be.  The smell...well, I don't really smell Naptha, as the tryptamine smell is -quite- strong...again, more so than the first/second pull.  So I assume it's pretty evaporated.

The 75ml jar is probably around half evaporated, and I almost wanted to freeze precipitate again, to see if it would be not so yellow...

Which brings to me these questions:

How do you know if you need a solvent wash?
How do you know if there was lye/water in your batch?

Is it normal for nice white crystals to turn reddish/purplish in the oil pipe?  Not entirely, as it crystallizes all around the bowl, but where it pools, it doesn't recrystallize. 

I don't taste anything wrong, it tastes like plastic.  I'm just afraid of chem burn.  I realize it can be harsh, but how do I know if it's...more harsh....? :P

So, anyone ever have a batch go completely white to completely yellow next pull?  Or is it due to evap that it is like this?


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OfflineR2-D2
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Re: STB DMT final pull -> evap? [Re: Dscid]
    #14067610 - 03/04/11 06:15 PM (12 years, 10 months ago)

If it's crystalline, at least that's a good sign


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OfflineJabbawaya

Registered: 07/10/05
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Re: STB DMT final pull -> evap? [Re: R2-D2]
    #14067953 - 03/04/11 07:35 PM (12 years, 10 months ago)

You could try a sodium carbonate wash with those yellow crystals, it might help remove impurities. Check the STB tek you're referencing.

Regarding evaporation at room temp versus heat: I do not recommend evaporating with heat because naphtha is ridiculously flammable and you want to keep all heating sources (especially fire!) away from it. Naphtha is a solvent, and like all aromatic hydrocarbons, evaporation will leave the solute behind crystallized.


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