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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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1.06 KG Whatcha's Tek (picture updates)
#14011349 - 02/23/11 12:50 AM (12 years, 11 months ago) |
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1 kilo of high quality MHRB powder. Performing Whatcha's tek for the first time. Will update with pictures and all along the way.

Currently freeze precipitating two pulls after a sodium carbonate wash.
 Ran out of naptha and felt like checking how it does. I'll be picking up some xylene when I get my next gallon of naptha. Freezing till friday evening. as of 11PM Wednesday.
Ah shoot...all my dmt was floating and I wasn't paying much attention. Guess I'll need to get them stored in my next freeze percip. Hey on the bright side i'll have a huge yield on my second go around..


**UPDATE 3/1**
Quote:
erikksonb said: Very, very neat. Pan is maybe? 12"x12" it's a square I think. Right now it's stashed away, my bad with no size referances. What is in the pan had no Washes/Re-x done to it. Straight pulls -> Freeze percip for 30hrs. What is in my signature had a sodium carb. wash.

4.54g^

4.54g^
So much more to be pulled..will need to eventually store this in naptha I'm guessing. Anyone have the shelf life before deterioration and so on?
-------------------- Imagine a world of Peace.

Edited by erikksonb (03/05/11 10:49 PM)
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Dosile Kouki
derp

Registered: 03/08/10
Posts: 14,963
Loc: Paradise
Last seen: 11 years, 6 months
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Re: 1.06 KG Whatcha's Tek [Re: erikksonb]
#14011814 - 02/23/11 02:47 AM (12 years, 11 months ago) |
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i just smoked some in the forrest the other day. only a tiny bit, didnt go to deep, but it was still fun.
What are you using as source material, if you dont mind me asking?
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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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Spot on, I've actually never ventured away from my couch and bed in my room, as I have lately always been CEV tranced almost and I feel most comfortable here. Lucy or any other psychedelic almost i'm always out and about venturing. How is dmt in the forest? Have you ever done a hefty dose outside? Now i'm eager...3-4 days so stoked
I'm using ground MHRB powder, most recent harvest around. Coming from mexico. This guy has been reputable for great yield percentages.
-------------------- Imagine a world of Peace.

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Dosile Kouki
derp

Registered: 03/08/10
Posts: 14,963
Loc: Paradise
Last seen: 11 years, 6 months
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Re: 1.06 KG Whatcha's Tek [Re: erikksonb]
#14011851 - 02/23/11 03:03 AM (12 years, 11 months ago) |
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its great, i was mostly focusing on cev's too after i saw the grid. I am the same though mostly just smoking in my bedroom, but as of late ive been venturing out into the forrest and stuff.
It's pretty cool in the forrest , in a nice secluded place with an epic view where you wont be disturbed.
I think thats where its meant to be taken, somewhere where you dont feel enclosed and trapped in by walls and things.
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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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I can see where that can be a big positive, i'll make sure to give that scenario a few runs soon.
-------------------- Imagine a world of Peace.

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Dosile Kouki
derp

Registered: 03/08/10
Posts: 14,963
Loc: Paradise
Last seen: 11 years, 6 months
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Re: 1.06 KG Whatcha's Tek [Re: erikksonb]
#14011887 - 02/23/11 03:24 AM (12 years, 11 months ago) |
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thing is though its tough to vape crystal outside in the wind, because vaping usually requires 100% no wind at all, unless its one of those vaping machines which does everything for you.
so it's best to make some changa to smoke in the forrest, becaues this can be smoked through traditional methods like bongs joints pipes etc with no trouble out in the wind.
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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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This will be fun.
-------------------- Imagine a world of Peace.

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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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Re: 1.06 KG Whatcha's Tek [Re: erikksonb]
#14014862 - 02/23/11 04:35 PM (12 years, 11 months ago) |
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Two pulls in.

Now waiting for my PH Plus in the mail still... package has been stuck in Illinois for 4 days now.
-------------------- Imagine a world of Peace.

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DimensionWithin
Chemist


Registered: 08/23/10
Posts: 220
Last seen: 11 years, 1 month
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Re: 1.06 KG Whatcha's Tek [Re: erikksonb]
#14016617 - 02/23/11 09:33 PM (12 years, 11 months ago) |
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Can't wait to see your yields. I just bought 10lbs of bark myself. I should be set for life...
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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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Ahahah yeah that's quite a score. Are you going for an A/B or STB extraction?
-------------------- Imagine a world of Peace.

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DimensionWithin
Chemist


Registered: 08/23/10
Posts: 220
Last seen: 11 years, 1 month
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Re: 1.06 KG Whatcha's Tek [Re: erikksonb]
#14016740 - 02/23/11 09:52 PM (12 years, 11 months ago) |
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I'm going to do an alcohol cake. It really seems like the only way to handle such a large batch. http://wiki.dmt-nexus.com/The_MHRB_CAKE_METHOD
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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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Never seen that done before, good luck man. Doing all 10lbs at once wow. should you store most in some naptha then? Don't want to have it going bad on you.
-------------------- Imagine a world of Peace.

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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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Re: 1.06 KG Whatcha's Tek [Re: erikksonb]
#14016798 - 02/23/11 10:02 PM (12 years, 11 months ago) |
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Screw it, I'm anxious I'm putting these two pulls in the freezer tonight, will do 2-3 more pulls and will decide if I want to wash it. I want too but i'll see how this batch comes out. Planning on redissolving if I need to.
-------------------- Imagine a world of Peace.

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DimensionWithin
Chemist


Registered: 08/23/10
Posts: 220
Last seen: 11 years, 1 month
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Re: 1.06 KG Whatcha's Tek [Re: erikksonb]
#14016810 - 02/23/11 10:05 PM (12 years, 11 months ago) |
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I think that I will probably only do a pound or two at a time. But you're right. I think as long as you don't purify the "cake" the dmt won't oxidize. So I'll probably keep it as that, and when I run out, just cut another piece of the cake off to extract.
Edit: Just do a sodium carbonate wash. Sodium Bicarbonate (baking soda) decomposes into sodium carbonate at 50ºC (112ºF).
Edited by DimensionWithin (02/23/11 10:07 PM)
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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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Sodium carbonate wash went through well, only spilled a few drops. In the freezer now. Also this is my first extraction over 100g, does the amount of naptha ML (not the concentration of dmt/naptha) affect how long the freeze should be conducted? Either way I'm going to leave it in for 36-40 hours till friday evening.
-------------------- Imagine a world of Peace.

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argg
Stranger


Registered: 07/20/09
Posts: 4,848
Loc: Nigeria
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Re: 1.06 KG Whatcha's Tek [Re: erikksonb]
#14017366 - 02/23/11 11:44 PM (12 years, 11 months ago) |
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no need for a "cake" with that much. A cake works well if you have buckets of stuff. A five gallon busket can handle that in a one pot shot.
edit:10 lbs of bark would be about 5 buskets.Might be able to go down to 3 but 5 will leave a nice headspace. I read cake and thought OP was gunna cake a kilo. A xylene pull at the end of each run in a hot water bath to collect it all plus mix in all the yellow goop from re-x with some acid will get you ready for a zinc wash. Stir it with some Zn for a few days and the yellow goes milky white and then your garbage will be cleaner then the first pull stb stuff. When you have that much a 3 dollar bottle of Zn is your friend.
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Edited by argg (02/23/11 11:51 PM)
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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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Re: 1.06 KG Whatcha's Tek [Re: argg]
#14024672 - 02/25/11 10:11 AM (12 years, 11 months ago) |
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I would pour the naptha out and all my dmt was floating..should have paid more attention.
Screwed. I'll get all them next pulls I guess


All that dmt...is now back in my two gallons and jar..any tips for pouring it out after my next freeze percip? I was rolling it and it helped but shot I dunno, haven't had this slight inconvenience before.
-------------------- Imagine a world of Peace.

Edited by erikksonb (02/25/11 10:15 AM)
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erikksonb
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Registered: 12/22/10
Posts: 344
Loc: Trees of the PNW
Last seen: 9 years, 6 months
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Re: 1.06 KG Whatcha's Tek [Re: erikksonb]
#14025667 - 02/25/11 02:06 PM (12 years, 11 months ago) |
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how much do you think this weighs out to?

First pull. I watched about 3/4 of the dmt float back into my MHRB sludge jars. My .001 scale is still in transit from hong kong
-------------------- Imagine a world of Peace.

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d-LSD-25
Stranger
Registered: 12/26/10
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Last seen: 12 years, 6 months
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Re: 1.06 KG Whatcha's Tek [Re: erikksonb]
#14025918 - 02/25/11 02:55 PM (12 years, 11 months ago) |
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There's no way to tell, but that looks like a gram to me...
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Cakk


Registered: 01/30/10 
Posts: 1,362
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Re: 1.06 KG Whatcha's Tek [Re: d-LSD-25]
#14025925 - 02/25/11 02:59 PM (12 years, 11 months ago) |
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Quote:
d-LSD-25 said: There's no way to tell, but that looks like a gram to me...
That's what I was thinking he should get around 10g total from 1 kilo
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