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InvisibleButtFace
Registered: 08/06/08
Posts: 1,559
Re: How to make LSD *DELETED* [Re: Cyclohexylamine]
    #14093158 - 03/09/11 03:27 PM (13 years, 13 days ago)

Post deleted by TieACable2aTree

Reason for deletion: f


Edited by ButtFace (03/09/11 03:35 PM)

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OfflineMr E Guest
partly animal
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Registered: 05/11/07
Posts: 635
Loc: 404: not found Flag
Last seen: 8 years, 2 months
Re: How to make LSD [Re: ButtFace]
    #14094045 - 03/09/11 06:09 PM (13 years, 13 days ago)

Quote:

TieACable2aTree said:
[...]at a minuimum proofread and spell check it before it is released[...]



:wink::thumbup:


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Be joyful. This could be the only chance you get.

All of the above posts are the fevered imaginings of a deluded mind, itself entirely the fictional creation of a somewhat peculiar author with a bizarre sense of humour.

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InvisibleButtFace
Registered: 08/06/08
Posts: 1,559
Re: How to make LSD *DELETED* [Re: Mr E Guest]
    #14096462 - 03/10/11 06:01 AM (13 years, 12 days ago)

Post deleted by TieACable2aTree

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OfflineMr E Guest
partly animal
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Re: How to make LSD [Re: ButtFace]
    #14096558 - 03/10/11 07:19 AM (13 years, 12 days ago)

I agree with you. Badly written drug synth books are a nightmare to read. Typo's and bad paragraphing are far too distracting. I'm a good proofreader, by the way... Feel like such a nerd for finding your typo amusing! :shrug: Context-based humour?


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Be joyful. This could be the only chance you get.

All of the above posts are the fevered imaginings of a deluded mind, itself entirely the fictional creation of a somewhat peculiar author with a bizarre sense of humour.

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Offline1tokeovrtheline
life=painfully beautiful
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Registered: 04/12/10
Posts: 866
Loc: innerverse&universe, surrealis...
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Re: How to make LSD [Re: Mr E Guest]
    #14096814 - 03/10/11 09:17 AM (13 years, 12 days ago)

haha I hear you. No worries though, I've already spent quite a bit of time spellchecking. It could be a little off here and there maybe (mostly in the historical and neurochemical action sections where I don't have as much knowledge), but I think the spelling should be fine.

And just to be clear the book won't be done for several months, but a shorter version (about 9,000 words) should be out later today


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Music, business as usual
Mi' spliff and Guiness as usual
Highgrade we puffin as usual
Fight down the system as usual
The system fight we down as usual
The cops dem a watch we as usual
And a we a watch the cops as usual

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Offline1tokeovrtheline
life=painfully beautiful
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Registered: 04/12/10
Posts: 866
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Re: How to make LSD [Re: 1tokeovrtheline]
    #14097255 - 03/10/11 11:25 AM (13 years, 12 days ago)

k, its up, let me know what you think, and enjoi!
http://www.shroomery.org/forums/showflat.php/Number/14097244


--------------------


Music, business as usual
Mi' spliff and Guiness as usual
Highgrade we puffin as usual
Fight down the system as usual
The system fight we down as usual
The cops dem a watch we as usual
And a we a watch the cops as usual

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Offlinehighasfak
Stranger
Registered: 07/08/13
Posts: 1
Last seen: 10 years, 8 months
Re: How to make LSD [Re: illxyz]
    #18529141 - 07/08/13 10:23 AM (10 years, 8 months ago)

#26 LSD-25
ACID; LYSERGIDE; D-LYSERGIC ACID DIETHYLAMIDE; METH-LAD; D-LYSERGAMIDE, N,N-DIETHYL; N,N-DIETHYL-D-LYSERGAMIDE; 9,10-DIDEHYDRO-N,N-DIETHYL-6-METHYLERGOLINE-8b-CARBOXAMIDE

SYNTHESIS : A solution of 6.7 g KOH in 100 mL H2O, under an inert atmosphere and magnetically stirred, was brought to 75 °C, and 10 g ergotamine tartrate (ET) added. The reaction mixture turned yellow as the ergotamine went into solution over the course of 1 h. The stirring was continued for an additional 3 h. The reaction mixture was cooled to about 10 °C with an external ice bath, and acidified to a pH of about 3.0 by the dropwise addition of 2.5 N H2SO4. White solids started to appear early in the neutralization; approximately 60 mL of sulfuric acid was required. The reaction mixture was cooled overnight, the solids removed by filtration, and the filter cake washed with 10 mL Et2O. The dry solids were transferred to a beaker, suspended in 50 mL 15 % ammonia in anhydrous ethanol, stirred for 1 h, and separated by decantation. This extraction was repeated, and the original decantation and the second extract combined and filtered to remove a few hundred milligrams of unwanted solids. The clear filtrate was stripped of solvent under vacuum, the residual solids dissolved in 50 mL of 1% aqueous ammonia, and this solution was acidified as before with 2.5 N H2SO4. The precipitated solids were removed by filtration and washed with Et2O until free of color. After drying under vacuum to a constant weight, there was obtained 3.5 g of d-lysergic acid hydrate, which should be stored in a dark, sealed container.

A suspension of 3.15 g d-lysergic acid hydrate and 7.1 g of diethylamine in 150 mL CHCl3 was brought to reflux with stirring. With the external heating removed, there was added 3.4 g POCl3 over the course of 2 min, at a rate sufficient to maintain refluxing conditions. The mixture was held at reflux for an additional 5 min, at which point everything had gone into solution. After returning to room temperature, the solution was added to 200 mL of 1 N NH4OH. The phases were separated, the organic phase dried over anhydrous MgSO4, filtered, and the solvent removed under vacuum. The residue was chromatographed over alumina with elution employing a 3:1 C6H6/CHCl3 mixture, and the collected fraction stripped of solvent under hard vacuum to a constant weight. This free-base solid can be recrystallized from benzene to give white crystals with a melting point of 87-92 °C. IR (in cm-1): 750, 776, 850, 937 and 996, with the carbonyl at 1631. The mass spectrum of the free base has a strong parent peak at mass 323, with sizable fragments at masses of 181, 196, 207 and 221.

This base was dissolved in warm, dry MeOH, using 4 mL per g of product. There was then added dry d-tartaric acid (0.232 g per g of LSD base), and the clear warm solution treated with Et2O dropwise until the cloudiness did not dispel on continued stirring. This opaqueness set to a fine crystalline suspension (this is achieved more quickly with seeding) and the solution allowed to crystallize overnight in the refrigerator. Ambient light should be severely restricted during these procedures. The product was removed by filtration, washed sparingly with cold methanol, with a cold 1:1 MeOH/Et2O mixture, and then dried to constant weight. The white crystalline product was lysergic acid diethylamide tartrate with two molecules of methanol of crystallization, with a mp of about 200 °C with decomposition, and weighed 3.11 g (66%). Repeated recrystallizations from methanol produced a product that became progressively less soluble, and eventually virtually insoluble, as the purity increased. A totally pure salt, when dry and when shaken in the dark, will emit small flashes of white light.
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