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desiretoheal
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How do I wash DMT crystals?
#11795607 - 01/09/10 11:27 AM (14 years, 1 month ago) |
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Somebody here used the STB tek and can certainly smell the naphtha on the crystals. The crystals themselves have a consistent yellowish tint. I heard people talking about a solvent wash but never could find a detailed explanation on how to perform this. It would be great to have pure crystals, as I would imagine.
Any help would be great!
-------------------- If there were no rewards to reap,No loving embrace to see me through This tedious path I've chosen here,I certainly would've walked away by now. Gonna wait it out. If there were no desire to heal The damaged and broken met along This tedious path I've chosen hereI certainly would've walked away by now. And I still may ... (sigh) ... I still may.Be patient. I must keep reminding myself of this.
Edited by desiretoheal (01/09/10 11:33 AM)
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tyler_0_durden
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The naphtha didn't completely evaporate?
Just do D.I. water washes in a saucepan a few times until all the naphtha is evaporated.
-------------------- "As a man who has devoted his whole life to the most clear headed science, to the study of matter, I can tell you as a result of my research about atoms this much: There is no matter as such. All matter originates and exists only by virtue of a force which brings the particle of an atom to vibration and holds this most minute solar system of the atom together. We must assume behind this force the existence of a conscious and intelligent mind. This mind is the matrix of all matter." --Max Planck
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desiretoheal
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Was the naphtha supposed to evap completely? the deemsters were left to dry for a good hour, but the smell never left.
What do you mean by D.I ??
-------------------- If there were no rewards to reap,No loving embrace to see me through This tedious path I've chosen here,I certainly would've walked away by now. Gonna wait it out. If there were no desire to heal The damaged and broken met along This tedious path I've chosen hereI certainly would've walked away by now. And I still may ... (sigh) ... I still may.Be patient. I must keep reminding myself of this.
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tyler_0_durden
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deionized water. you can also use natural spring water from the store.
-------------------- "As a man who has devoted his whole life to the most clear headed science, to the study of matter, I can tell you as a result of my research about atoms this much: There is no matter as such. All matter originates and exists only by virtue of a force which brings the particle of an atom to vibration and holds this most minute solar system of the atom together. We must assume behind this force the existence of a conscious and intelligent mind. This mind is the matrix of all matter." --Max Planck
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killuminati420
Swimmin in Cyans soon



Registered: 09/20/09
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i never have problems with the naphtha not evaporating with freeze precip...when i let it sit out to dry for about an hour, i notice the smell of naphtha will slowly go away, leaving a certain smell of fresh DMT and the DMT should be crisp when scraped and not wet....when the DMT is dry, when you go to smell the jar, it should smell almost like a new pair of leather shoes...for real
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desiretoheal
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would it be a good idea to let the crystals "air out" by a fan for an hour?
-------------------- If there were no rewards to reap,No loving embrace to see me through This tedious path I've chosen here,I certainly would've walked away by now. Gonna wait it out. If there were no desire to heal The damaged and broken met along This tedious path I've chosen hereI certainly would've walked away by now. And I still may ... (sigh) ... I still may.Be patient. I must keep reminding myself of this.
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MCSteveyC
lib lover



Registered: 08/23/09
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what the fucks DMT?
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killuminati420
Swimmin in Cyans soon



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you could use a fan if you think it is wet but dont aim it directly on it...set it up where there is air just blowing through the inside of the jar gently...watch often(every 10 mins) because a fan will dry it out FAST in my opinion...you dont want to keep a fan on for a really long time because when too much oxygen gets exposed to the DMT, it will lose potency i hear and might go into n-oxide DMT....that is when WAY too much oxygen gets exposed and it turns the crystals to a yellow goo i hear....but this is with a long time of a fan blowing. Just dont leave the fan on it for like the whole day and you will be fine. DMT should be stored in a airtight container in a dark freezer.
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Humility
Working on it



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sansa

Registered: 11/17/09
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I did a couple sodium carbonate washes using this tek and finally got white crystals:
http://www.drugs-forum.com/forum/showpost.php?p=449459&postcount=13
Quote:
put SWIYs nonpolar solution that contains spice freebase into a seperatory funnel or whatever other home made equivalent your are using. simply pour your sodium carbonate solution pH (about 10 just add a bit of sodium carbonate to water if you have pH papers it will suffice dont worry if your pH is a bit higher or lower then 10. lower then 9 is too low) into non polar solvent. mix brielfy let phases separate and collect your non polar solvent discard water. repeat maybe one or two times if necessary.
there are two reasons this works better then washing the crystals themselves. one is that crystals can actually form around solvent and impurities and in a way hide them inside so that when you wash you only wash the outside. when in solution everything is mixed and phases can separate better. also if you wash the crystals themselves you run the risk of dropping or squirting them away.
I made the sodium carbonate by getting a $0.42 box of baking soda (not baking powder) and cooking it in a jar in the oven at 350F for 3 hours.
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Zander
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Re: How do I wash DMT crystals? [Re: sansa]
#11796202 - 01/09/10 01:30 PM (14 years, 1 month ago) |
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hmm
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Zander
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Re: How do I wash DMT crystals? [Re: sansa]
#11796203 - 01/09/10 01:30 PM (14 years, 1 month ago) |
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hmm
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Nature Boy
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If its re-crystallization you want, then see:
http://www.shroomery.org/forums/showflat.php/Number/11726174
I highly doubt there's naphtha in your spice. Yellow is powerful mojo. Vaporize it as-is. Get used to that smell. That's the smell of tryptamine, which is... 
N.B.
-------------------- All submitted posts under this user name are works of pure fiction or outright lies. Any information, statement, or assertion contained therein should be considered pure unadulterated bullshit. Note well: Sorry, but I do not answer PM's unless you are a long-time trusted friend. If you have a question, ask it in the appropriate thread.
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desiretoheal
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Re: How do I wash DMT crystals? [Re: Nature Boy]
#11796461 - 01/09/10 02:11 PM (14 years, 1 month ago) |
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I guess I fumbled a little because I didn't COMPLETELY dry it out. I poured off as much naphtha to the drop after I pulled out the freezer. When I scraped, it was pretty dry but not 100%. Like I mentioned, it is sitting in a vial now, which I am not around at the moment. I guess I will just let it sit out at room temp for a few hours, uncovered. Should I expect the scent to change?..or better yet, will it be safe enough to smoke without killing my lungs?
I DO most certainly appreciate the help fellow shroomerites
-------------------- If there were no rewards to reap,No loving embrace to see me through This tedious path I've chosen here,I certainly would've walked away by now. Gonna wait it out. If there were no desire to heal The damaged and broken met along This tedious path I've chosen hereI certainly would've walked away by now. And I still may ... (sigh) ... I still may.Be patient. I must keep reminding myself of this.
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desiretoheal
Seeker


Registered: 08/16/09
Posts: 1,286
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Re: How do I wash DMT crystals? [Re: Nature Boy]
#11796472 - 01/09/10 02:13 PM (14 years, 1 month ago) |
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and thank you again NB for the ever so simple STB tek
-------------------- If there were no rewards to reap,No loving embrace to see me through This tedious path I've chosen here,I certainly would've walked away by now. Gonna wait it out. If there were no desire to heal The damaged and broken met along This tedious path I've chosen hereI certainly would've walked away by now. And I still may ... (sigh) ... I still may.Be patient. I must keep reminding myself of this.
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Nature Boy
Stranger than most



Registered: 07/09/07
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Believe me, its not my tek...just passed on the tutorial. Nonetheless, your kind words are greatly appreciated.
Again, if your spice is powdery, then there's no naphtha present. Give it two solid hits and report back!
N.B.
-------------------- All submitted posts under this user name are works of pure fiction or outright lies. Any information, statement, or assertion contained therein should be considered pure unadulterated bullshit. Note well: Sorry, but I do not answer PM's unless you are a long-time trusted friend. If you have a question, ask it in the appropriate thread.
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mongo lloyd
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Re: How do I wash DMT crystals? [Re: Nature Boy]
#11797268 - 01/09/10 04:31 PM (14 years, 1 month ago) |
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Soap and hot water.
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