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OfflineShroom_dancer
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Final DMT Extraction Question(Still Need HELP)
    #10682985 - 07/15/09 04:17 PM (14 years, 8 months ago)

Alright I'm doing the Lazy Man's Tek now and I have the top layer of naphtha that i've been swirling around for like 20 minutes.

It's still pretty clear, should I swirl a little harder and faster for it to start turning yellow?

Once I start evaporating I think I'm going to let it evap for a few hours then put half in a mason jar to freeze while the other half just evaps so I can utilize both methods for future extractions.

But as long as it's yellow and not too dark it will yield 100% safe DMT right?

I'm worried that some lye would end up in the final product and then kill off anyone who tries it =-O

Can someone debunk that if it isn't true^^

Just want to be careful... lye is strong stuff

Edited by Shroom_dancer (07/15/09 05:32 PM)

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OfflineFisherman
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683004 - 07/15/09 04:21 PM (14 years, 8 months ago)

Yeah don't worry, yellowish crystals are just fine, and if you do want them cleaner, do an ammmonia wash :>


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OfflineShroom_dancer
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Re: Final DMT Extraction Question [Re: Fisherman]
    #10683013 - 07/15/09 04:22 PM (14 years, 8 months ago)

I'm asking if the color of the naphtha is yellow but kind of dark, and some NaOH did end up in the final product and I didn't do a wash, what would happen

Would I end up dying from smoking lye?

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OfflineShroom_dancer
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683049 - 07/15/09 04:29 PM (14 years, 8 months ago)

My naphtha is still clear 30 min later :-\

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OfflineFisherman
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683090 - 07/15/09 04:37 PM (14 years, 8 months ago)

No, I am absolutly sure one wouldn't die, but it wouldn't be pleasant or healthy.

Chillness


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OfflineShroom_dancer
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Re: Final DMT Extraction Question [Re: Fisherman]
    #10683124 - 07/15/09 04:42 PM (14 years, 8 months ago)

Alright thank you.

Glad to know my product won't kill people :laugh:

Should I swirl it around for another 30 minutes? It's still quite clear and I know the naphtha should be a yellowish color once it has DMT in it.

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OfflineFisherman
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683180 - 07/15/09 04:55 PM (14 years, 8 months ago)

hmmm.. stirr more, maybe heat it up abit, like above a radiator or something


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OfflineShroom_dancer
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683198 - 07/15/09 04:58 PM (14 years, 8 months ago)

I don't have anything to heat it and the last time I stirred it, my naphtha ended up becoming brown because I'm using Mimosa Powder, so some dust particles were trapped in the naphtha and it was unusable.

I'm just swirling the bowl around gently now.

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OfflineFisherman
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683211 - 07/15/09 05:01 PM (14 years, 8 months ago)

Ah yes, you have to be carefull not to stir/twirl it too hard, thatll cause emulsion :p

But I really suggest you try finding something to heat it up, else stop twirling it around and leave it for some time, i'm sure it'll turn out fine.


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Edited by Fisherman (07/15/09 05:01 PM)

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OfflineShroom_dancer
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683223 - 07/15/09 05:04 PM (14 years, 8 months ago)

How would letting it sit allow the DMT to migrate into the naphtha?

I just want some DMT and this is the last of my rootbark :frown:

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OfflineFisherman
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Re: Final DMT Extraction Question [Re: Fisherman]
    #10683250 - 07/15/09 05:11 PM (14 years, 8 months ago)

Constant swirling around won't do any good? :b

mmhm, someone else gotta come with some input other than heating it up, kinda too tired to start digging sorry :x nite ;b


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OfflineShroom_dancer
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Re: Final DMT Extraction Question [Re: Fisherman]
    #10683317 - 07/15/09 05:27 PM (14 years, 8 months ago)

If it's clear that's an indication that there's no DMT right?

I've been waiting about an hour and a half for this to turn yellow and nothin' is happening :-\

Tek even said 20-30 minutes.

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OfflineFisherman
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683362 - 07/15/09 05:35 PM (14 years, 8 months ago)

Aight, I ended up toking more instead of going to bed :gethigh:

Well, either you have dmt in your naptha, you will just get a smaller amount of clear crystals - another case could be no dmt.

I suggest you go heat a bathtub or a sink with very hot water and let your jar/whatever you are using soak in it somehow for 10-60 minutes - i'm pretty sure this should yellow it up :b

If you still are very unsure about your DMT yield, don't throw anything away, add more lye, as I said, i'm sure you can get it going! :smile:


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OfflineShroom_dancer
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Re: Final DMT Extraction Question [Re: Fisherman]
    #10683396 - 07/15/09 05:41 PM (14 years, 8 months ago)

The bathtub/sink idea won't work.

his dad came home early and we're doing it in his room. I put it on top of an Xbox cable thing, but i don't think that will be too effective.

And I'm out of lye. Had about 400-500 grams of bark and added 212 grams of Lye.

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OfflineFisherman
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683447 - 07/15/09 05:52 PM (14 years, 8 months ago)

Hmm, well anyway, there is no reason to throw it out, try to take batch of the naptha in an hour or so and see if you get any crystals - if you get none, I suggest you add like 100g of lye whenever you have some more and some naptha - it'll work out.

Headin to bed, gl with everything


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Edited by Fisherman (07/15/09 05:53 PM)

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OfflineShroom_dancer
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683753 - 07/15/09 06:51 PM (14 years, 8 months ago)

Just took all the naphtha out.

Pretty clear... wish me luck I guess..

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OfflineShroom_dancer
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683770 - 07/15/09 06:55 PM (14 years, 8 months ago)

I have about 250-300 ml left of naphtha.

Should I just put it all in for a second pull and then get more lye/naphtha for more pulls?

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OfflineHumility
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683978 - 07/15/09 07:27 PM (14 years, 8 months ago)

Good luck with that dude.  Hopefully, as others have stated, clear naphtha = clear crystals and not no crystals, as NB states.

I guess you can tell us in about oh say 24 hours.


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OfflineShroom_dancer
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Re: Final DMT Extraction Question [Re: Shroom_dancer]
    #10683988 - 07/15/09 07:28 PM (14 years, 8 months ago)

LAST QUESTION

should I evap it?

it seems like it would take wayyyy too long. I have about 400 ml of naphtha from the mixture so should I freeze precipitate it all? (Put in freezer for 12-24 hours and pour off naphtha then scrape up crystals)

Or just wait for one fan to evap it all?

Also, does it have to be an airtight container? I have a pyrex glass dish that would work but it has no top - would seran wrap suffice?

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Offlinemoe.phan
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Re: Final DMT Extraction Question [Re: Humility]
    #10684057 - 07/15/09 07:38 PM (14 years, 8 months ago)

even if your naptha looks clear, once you evap down a bit, it will start getting some yellow appearance. just because it looks clear, that doesn't mean theres no crystals in it.

evap down to half volume. cellophane will be fine for a lid. you should start seeing crystals in about 4 hrs if your freezer is cold enough.

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