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Offlinekolizion
LucidMind

Registered: 02/04/04
Posts: 493
Last seen: 7 years, 7 months
Large scale salvia extraction TEK >>new pics<< JAN19th
    #5155611 - 01/08/06 06:32 PM (18 years, 3 months ago)

I'm extracting a kilo of salvia tonight for a customer.. so i'll be editing this and adding in all the steps to extract  Crystaline salvinorin from 1 kilo of salvia.

Needed

1 milk jug (cut off the top)
(or if your worried about melting plastic, then use a watering can of some sort.)
1 gal. of acetone
1 gal. of naptha (lighter fluid, or camp fuel)
1 kilo salvia
1 large pyrex glass bowl
some sort of large cleaning jar... a 1/2 pint ball jar will work.
some coffee filters
a mask for fumes
glass turkey baster... or syphon tube.
time / patience


First take a milk jug and cut the top off it, and cut through the handle to make sort of a spout... this will help illiminate a funnel for now.  I'm sure you'll lose a slight amount of product from it sticking to the plastic.... but it's minute..

so your milk jug should look like this


you'll also need a pyrex bowl, coffee filters and rubber bands.


and your kilo of salvia


start by taking a coffee filter and wrap it around your ghetto spout like this


Then pour in enough salvia to cover 1/4 of your jug


The pour in your acetone so it's slightly above your salvia mixture


Stir and shake your goo for about 10 minutes, then strain through your homemade spout... carefull when tipping the jug as salvia likes to flop over and splash into your bowl.

Repete this proccess 3 times to each amount you put in your jug.

then discard the amount in your jug.. it's crap now.

unfortunatly I didn't take pictures of a few steps after this.
let your bowl evap for roughly 30 minutes... then if you look at your bowl you'll notice a lot of settlement sitting on the bottom.

Clean out your jug as clean as you can get it, and dry it out...
carefully pour your liquid salvia/acetone back into the jug SLOWLY... leaving just the settlement behind in the dish.

Clean out your dish, wipe dry.

Place a new filter on your spout and pour your acetone/salvia back through into your dish...

and evap all the way. 

acetone likes to pull everything over... tons of black wax, tons of gooey shit.

scrape your plack wax out, and place in 1/2 pint jar.



then gently poor in your naptha to the first screw neck mark... you'll notice just by letting it sit there the naptha will start to pull out some of the gunky crap

then with a gentle swirl it will ake on a very darkcolor.. almost black.. give a swirl till all your goo is desolved in the naptha
 

replace the lid, and wait... you want to wait one hour (MIN!) per cleaning to let all your salvinorin fall to the bottom... as salvinorin is not soluable in naptha.


-=-=-=UPDATE=-=-=-

I am re-doing this extraction for the sake of betetr pictures,
and more step/by/steps

this is the result of the first extraction...
I did not clean it to it's full potential.. but another 2 - 3 washes would have left this almost entirly pure white.

 
and 2 points if you can name the video card to the right, and car to the left :wink:

Edited by kolizion (01/19/06 06:26 PM)

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InvisibleMezcal
Registered: 08/11/05
Posts: 1,980
Re: Large scale salvia extraction TEK [Re: kolizion]
    #5158003 - 01/09/06 11:35 AM (18 years, 3 months ago)

Any updates?

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Offlinekolizion
LucidMind

Registered: 02/04/04
Posts: 493
Last seen: 7 years, 7 months
Re: Large scale salvia extraction TEK [Re: Mezcal]
    #5158581 - 01/09/06 02:37 PM (18 years, 3 months ago)

pictures in a few minutes

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Offlinedarkice
Stranger
Registered: 03/31/05
Posts: 48
Last seen: 15 years, 7 months
Re: Large scale salvia extraction TEK [Re: kolizion]
    #5158678 - 01/09/06 03:05 PM (18 years, 3 months ago)

acetone and plastic doesn;t seem like a very good idea

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Offlinekolizion
LucidMind

Registered: 02/04/04
Posts: 493
Last seen: 7 years, 7 months
Re: Large scale salvia extraction TEK [Re: darkice]
    #5158682 - 01/09/06 03:06 PM (18 years, 3 months ago)

i've done this many many many a time... if in fact it does etch the plastic... it's minute, and un-detectable in the final steps.

plus this tek is to help noobs out... who don't own big expensive shit, I don't want to answer questions about sep funels.. and re-crystalization steps.

Edited by kolizion (01/09/06 03:10 PM)

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InvisibleAsante
Omnicyclion prophet
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Registered: 02/06/02
Posts: 87,330
Re: Large scale salvia extraction TEK [Re: kolizion]
    #5159311 - 01/09/06 05:51 PM (18 years, 3 months ago)

If you are thinking simplicity then a tin watering can could easily be used eliminating the plastic-acetone contact which i really don't approve of. If the plastic wont dissolve then the plasticizers may leach out.



A watering can could do your kilo, a teapot would be more suitable for smaller batches. These are designed as pouring devices so less chance of spilling.

Hey your pictorial tek looks really good. Please take a ton of pictures and add any and all scraps of info you can.


--------------------
Omnicyclion.org
higher knowledge starts here

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Offlinekolizion
LucidMind

Registered: 02/04/04
Posts: 493
Last seen: 7 years, 7 months
Re: Large scale salvia extraction TEK [Re: Asante]
    #5159343 - 01/09/06 06:01 PM (18 years, 3 months ago)

you can use whatever you need to use... however while purifing the crystals.... nothing but the crystals will carry over. So i'm not extremly worried about the plastic, but if using something metal makes one feel better, then use something metal.

I don't feel anything negative is being pulled through with the extraction.. as a test.. acetone was placed in another jug, sloshed for 10 minutes, and let evaperate on a glas plate... no resedue was left. leaving me to believe there is nothing negative being pulled through...

once again, it's whatever makes you feel more comfortable.

more pics and description will continue to come as i'm still evaping and reducing the first half of the extraction.

Edited by kolizion (01/09/06 06:09 PM)

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Offlinekolizion
LucidMind

Registered: 02/04/04
Posts: 493
Last seen: 7 years, 7 months
Re: Large scale salvia extraction TEK [Re: kolizion]
    #5160355 - 01/09/06 09:51 PM (18 years, 3 months ago)

this tek would be going so much faster if my 50 gallon salt water tank didn't decide it wanted to overflow....

now that the water is sucked out of my rug.. and stable again.. I can go back to finishing this.

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Offlinekolizion
LucidMind

Registered: 02/04/04
Posts: 493
Last seen: 7 years, 7 months
Re: Large scale salvia extraction TEK [Re: kolizion]
    #5168137 - 01/11/06 04:11 PM (18 years, 3 months ago)

new pics

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OfflineEkstaza
stranger than most
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Registered: 04/10/03
Posts: 4,324
Loc: Around the corner
Last seen: 1 year, 16 days
Re: Large scale salvia extraction TEK [Re: kolizion]
    #5173510 - 01/12/06 06:43 PM (18 years, 3 months ago)

Cool extraction. Hurry it up, I can't wait to see the whole thing.


--------------------
YOUR EXPERIENCE WITH ANY GIVEN DRUG ISN'T THE DEFINITIVE MEASURE OF THE DRUGS EFFECTS.

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Offlinekolizion
LucidMind

Registered: 02/04/04
Posts: 493
Last seen: 7 years, 7 months
Re: Large scale salvia extraction TEK [Re: Ekstaza]
    #5175311 - 01/13/06 02:18 AM (18 years, 3 months ago)

I had a near death accedent today accedently spillig the cup holding the solution and suspend salvia crystals onto a huge sheet of plastic.

The positive side.. minimal loss.. the down side. spending a ton of time scraping...

To make it more fair, to the customer.. i'm re-doing the extraction...
so I can
a. take better pictures of the process for you...
b. have a more acurate extraction..

freaken pissed me off, but was my fault.. no reason anyone should suffer for that. so it seems i'll have a bit of purified salvia crystals up for grabs soon. not sure how much was lost.... but it will be compaired when I re-extract another batch.


sorry for such a delay on this stuff guys. I think i've developed a new way to clean the remainging amount more thurough.. but more time consuming.

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InvisibleAsante
Omnicyclion prophet
Male User Gallery

Registered: 02/06/02
Posts: 87,330
Re: Large scale salvia extraction TEK [Re: kolizion]
    #5175614 - 01/13/06 06:23 AM (18 years, 3 months ago)

Kolizion, I hope you are being selective about whom you are doing these extractions for.

Don't indirectly add to the illegalization of Salvia, OK?


--------------------
Omnicyclion.org
higher knowledge starts here

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Offlinekolizion
LucidMind

Registered: 02/04/04
Posts: 493
Last seen: 7 years, 7 months
Re: Large scale salvia extraction TEK [Re: Asante]
    #5176796 - 01/13/06 01:20 PM (18 years, 3 months ago)

it's for an ethno trade.... not for sale.
It was kilo extraction for a kilo of peruvian torch.. powderized.

don't think it'll hurt it at all...

I don't usually do the extraction of the pure crystals to everyday folk.... I know what those crystals can do. I don't wish that on anyone.

LET THAT BE PRE-WARNING for everyone else who reads this tek.... if you decide to do it... re -extract back onto some leaf.... i'm not responcible in anyway if you decide to play superman with your brain.

Edited by kolizion (01/13/06 01:24 PM)

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Offlinekolizion
LucidMind

Registered: 02/04/04
Posts: 493
Last seen: 7 years, 7 months
Re: Large scale salvia extraction TEK [Re: kolizion]
    #5199898 - 01/19/06 06:31 PM (18 years, 2 months ago)

I'm re-doing the extraction for this tek....

I had too little time this run to take ppics in full... so..

extraction #2 I promise will have much more follow through and details.
also, video will be recorded for my new dvd
"Passage"

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Invisiblepoboy
On the bounce
Male

Registered: 03/08/05
Posts: 1,355
Re: Large scale salvia extraction TEK *DELETED* [Re: kolizion]
    #5201267 - 01/20/06 12:19 AM (18 years, 2 months ago)

Post deleted by poboy

Reason for deletion: d



--------------------
Burn the land and boil the sea but you can't take the sky from me.

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Offlinekolizion
LucidMind

Registered: 02/04/04
Posts: 493
Last seen: 7 years, 7 months
Re: Large scale salvia extraction TEK [Re: poboy]
    #5201485 - 01/20/06 02:15 AM (18 years, 2 months ago)

cold shake tek? are you talking about freaze -precipitating crystals out?

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OfflineTinkal
Green Thumb
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Folding@home Statistics
Registered: 06/01/05
Posts: 257
Loc: Europe
Last seen: 2 years, 11 months
Re: Large scale salvia extraction TEK [Re: kolizion]
    #5201634 - 01/20/06 04:37 AM (18 years, 2 months ago)

I think that this tek only works for cannabis


--------------------
Ask me about my seed collection and trading!

"Of all the things I love the most, my mind is what I miss the most"

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Offlinemr_minds_eye
Disposable Wage Whore
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Registered: 01/22/02
Posts: 1,948
Loc: Samsara
Last seen: 11 years, 3 months
Re: Large scale salvia extraction TEK [Re: kolizion]
    #5202508 - 01/20/06 11:56 AM (18 years, 2 months ago)

Quote:

kolizion said:
you can use whatever you need to use... however while purifing the crystals.... nothing but the crystals will carry over. So i'm not extremly worried about the plastic, but if using something metal makes one feel better, then use something metal.

I don't feel anything negative is being pulled through with the extraction.. as a test.. acetone was placed in another jug, sloshed for 10 minutes, and let evaperate on a glas plate... no resedue was left. leaving me to believe there is nothing negative being pulled through...

once again, it's whatever makes you feel more comfortable.

more pics and description will continue to come as i'm still evaping and reducing the first half of the extraction.



Take a few drops and splash just a little on some finished furniture or something painted that you won't mind fucking up a little. Wipe it off after a couple seconds and it will probably eat the shit off. Just saying that shit is strong and you would be suprised.


--------------------
Our quest for discovery fuels our creativity in all fields, not just science. If we reached the end of the line, the human spirit would shrivel and die. But I don't think we will ever stand still: we shall increase in complexity, if not in depth, and shall always be the center on an expanding horizon of possibilities.
-Stephen Hawking

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Offlinekolizion
LucidMind

Registered: 02/04/04
Posts: 493
Last seen: 7 years, 7 months
Re: Large scale salvia extraction TEK [Re: mr_minds_eye]
    #5203439 - 01/20/06 04:09 PM (18 years, 2 months ago)

if you think I don't know what i'm talking about..
don't do it. simple as that, but if you think I don't know very well what each chemical does, is capable of, and carrys over... your wrong.

this tek was slopped together for noobs.

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Invisibleredgreenvines
irregular verb
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Registered: 04/08/04
Posts: 38,173
Re: Large scale salvia extraction TEK [Re: kolizion]
    #5203658 - 01/20/06 05:03 PM (18 years, 2 months ago)

thrilling!


--------------------
:confused: _ :brainfart:🧠  _ :finger:

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