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Offlinehighc
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dmt extract pissng me off
    #11901952 - 01/25/10 11:53 PM (3 years, 3 months ago)

after a first time failure with dmt i decided to get 500 grams and try again.

150 grams bark was mixed with 625 ml water with about 150 grams lye. it was left to sit a while before adding about 100ml solvent. this mix was left to sit about 24 hours mixing it up twice. the top layer was removed and is fan evaporating as i type. it's evaporating but it only looks to be about not even 50mg spice. what the fuck is goin on around here?


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OfflineNWlight
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Re: dmt extract pissng me off [Re: highc]
    #11902001 - 01/26/10 12:00 AM (3 years, 3 months ago)

What solvent are you using? Also I've heard that it is better to freeze/thaw/freeze/thaw the bark to get the maximum extraction. Try reading various how-to's, they will probably have some mention of this.


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Re: dmt extract pissng me off [Re: NWlight]
    #11902015 - 01/26/10 12:01 AM (3 years, 3 months ago)

using the old vm+p. i know about the freeze. i plan on doing that with the rest of my bark. i just wanted some for right now, so i used lazyman tek for a couple doses.


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OfflineNWlight
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Re: dmt extract pissng me off [Re: NWlight]
    #11902019 - 01/26/10 12:02 AM (3 years, 3 months ago)

Extraction of chemicals from a medium such as bark is similar to getting soap out of a sponge.  Even if you let a soapy sponge sit in water for 24 hours, if you don't rip up, stir, squeeze, chop, and otherwise mutilate the sponge, as soon as you pull it up out of the water and squeeze the center will still be full of soap! (in this case, DMT)


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OfflineIma Trooper
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Re: dmt extract pissng me off [Re: NWlight]
    #11902023 - 01/26/10 12:03 AM (3 years, 3 months ago)

Yeah grind your bark to a powder if you can RP.


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Re: dmt extract pissng me off [Re: Ima Trooper]
    #11902040 - 01/26/10 12:05 AM (3 years, 3 months ago)

I do have powder.And to the sponge thing i understand, but i vigurously stirred it for 30 minutes. then let it sit for hours and did the turn over end method a couple times before removing top layer. I just think i should be getting a lot more.


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OfflineNWlight
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Re: dmt extract pissng me off [Re: highc]
    #11902098 - 01/26/10 12:11 AM (3 years, 3 months ago)

Sorry about that, maybe it's also not the most efficient method? maybe you got a bad batch? :shrug:
I'll probably be posting my dmt extract problems soon too as I am going to attempt it in the near future as well.


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Offlinethe bizzle
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Re: dmt extract pissng me off [Re: NWlight]
    #11902131 - 01/26/10 12:14 AM (3 years, 3 months ago)

Maybe go for the real deal, make use of the plants you have instead of extracting, and possibly learn how to not get pissed off altogether :shrug:


although I could be out of my jurisdiction here, maybe you do already but want some DMT in addition to that, in which case, I hope you find a solution :shrug:


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Edited by the bizzle (01/26/10 12:15 AM)


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Offlinehighc
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Re: dmt extract pissng me off [Re: the bizzle]
    #11902166 - 01/26/10 12:19 AM (3 years, 3 months ago)

well its done and i have 350mg. thats ok i guess. new question though. its mostly an orange type goo. Should i still use 50mg as a good strong dose?

and i do use the plants. if your talking about aya. i love it.


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OfflineNWlight
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Re: dmt extract pissng me off [Re: highc]
    #11902179 - 01/26/10 12:20 AM (3 years, 3 months ago)

Quote:

highc said:
well its done and i have 350mg. thats ok i guess. new question though. its mostly an orange type goo. Should i still use 50mg as a good strong dose?

and i do use the plants. if your talking about aya. i love it.



I wouldn't start with a standard dose doing a drug of unknown purity.
Just a general rule :wink:


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Re: dmt extract pissng me off [Re: NWlight]
    #11902187 - 01/26/10 12:22 AM (3 years, 3 months ago)

Quote:

NWlight said:
Quote:

highc said:
well its done and i have 350mg. thats ok i guess. new question though. its mostly an orange type goo. Should i still use 50mg as a good strong dose?

and i do use the plants. if your talking about aya. i love it.



I wouldn't start with a standard dose doing a drug of unknown purity.
Just a general rule :wink:




i figure if anything its less pure?


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Re: dmt extract pissng me off [Re: NWlight]
    #11902190 - 01/26/10 12:22 AM (3 years, 3 months ago)

haha thats true, the thought did cross my mind. it can't be any more pure than 100% pure, right: :P
Let us know how it is!


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Re: dmt extract pissng me off [Re: highc]
    #11902192 - 01/26/10 12:23 AM (3 years, 3 months ago)

Quote:

highc said:
well its done and i have 350mg. thats ok i guess. new question though. its mostly an orange type goo. Should i still use 50mg as a good strong dose?

and i do use the plants. if your talking about aya. i love it.





If its orange goo then you have a lot of plant fats in there. Do the freeze precipitation and you'll have crystals/powder.


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Offlineoh_you_know
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Re: dmt extract pissng me off [Re: highc]
    #11902193 - 01/26/10 12:23 AM (3 years, 3 months ago)

orange is less pure than white


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Offlinethe bizzle
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Re: dmt extract pissng me off [Re: highc]
    #11902214 - 01/26/10 12:26 AM (3 years, 3 months ago)

Quote:

highc said:
and i do use the plants. if your talking about aya. i love it.




:thumbup: excellent. I didn't mean to seem condescending, I'm sure I came off that way, but I'm sure you can understand why I would want to remind people that it's not all about the DMT, or that DMT isn't quite doin thangs to the extent that aya is doin thangs. Anyways, I hope you have a blast!

                        :highfive:



:etbig:


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Offlinehighc
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Re: dmt extract pissng me off [Re: oh_you_know]
    #11902219 - 01/26/10 12:26 AM (3 years, 3 months ago)

well im gonna go ahead and try it. ive only smoked it once. 25mg of white. im a try 50-75. catch yall on the flip side.


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Re: dmt extract pissng me off [Re: highc]
    #11903432 - 01/26/10 04:46 AM (3 years, 3 months ago)

Well? How did it go?


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Re: dmt extract pissng me off [Re: Ima Trooper]
    #11903587 - 01/26/10 06:19 AM (3 years, 3 months ago)

Which tek are you following? Get a good one and follow it to the letter.


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Offlinehighc
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Re: dmt extract pissng me off [Re: turkeyphant]
    #11905977 - 01/26/10 04:50 PM (3 years, 3 months ago)

Quote:

turkeyphant said:
Which tek are you following? Get a good one and follow it to the letter.




well just to get a little bit real quick i used the lazyman tek to the t. just recalculated weight for 150 grams.

I'm going to continue to use this tek for the rest of the material except I'm going to freeze precipitate and use a sodium bicarbonate wash.


it went well btw. it was orange but little noticed difference in intensity compared to white.


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Re: dmt extract pissng me off [Re: highc]
    #11905999 - 01/26/10 04:53 PM (3 years, 3 months ago)

sodium carbonate not bicarbonate....one thing that is on your side, is time. You can keep tryin to extract over and over until your satisfied.


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Re: dmt extract pissng me off [Re: preschooler]
    #11906054 - 01/26/10 05:02 PM (3 years, 3 months ago)

Quote:

preschooler said:
sodium carbonate not bicarbonate....one thing that is on your side, is time. You can keep tryin to extract over and over until your satisfied.




corrected. washing soda


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Re: dmt extract pissng me off [Re: highc]
    #11906078 - 01/26/10 05:06 PM (3 years, 3 months ago)

It really is the difference between having crap product and good product...takes about 30 min tops with a decent pipette.


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Re: dmt extract pissng me off [Re: preschooler]
    #11916290 - 01/28/10 07:43 AM (3 years, 3 months ago)

Freeze precip is the way. And then recrystallise.


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Re: dmt extract pissng me off [Re: turkeyphant]
    #11927047 - 01/30/10 12:49 AM (3 years, 3 months ago)

Quote:

turkeyphant said:
Freeze precip is the way. And then recrystallise.





hell yeah. i freeze percipitated the rest of it. i pulled over 2 grams out today. mmmmmmm. dmt is the shit.


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Re: dmt extract pissng me off [Re: highc]
    #11927198 - 01/30/10 01:25 AM (3 years, 3 months ago)

Quote:

highc said:
Quote:

turkeyphant said:
Freeze precip is the way. And then recrystallise.





hell yeah. i freeze percipitated the rest of it. i pulled over 2 grams out today. mmmmmmm. dmt is the shit.



how many grams of MHRB did you use? and what tek?


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Re: dmt extract pissng me off [Re: highc]
    #11927264 - 01/30/10 01:41 AM (3 years, 3 months ago)

I have some of that Mimosa Hostilis bark.  I've had it for 5 years and I've never done anything with it because extracting it always seemed so difficult.  I need to make use of it.  Someone convince me to do it.












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Re: dmt extract pissng me off [Re: Learyfan]
    #11927302 - 01/30/10 01:52 AM (3 years, 3 months ago)

stb tek doesnt seem hard at all, im gonna try it once i get some supplies


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Re: dmt extract pissng me off [Re: highc]
    #11927307 - 01/30/10 01:54 AM (3 years, 3 months ago)

I didn't bother reading the whole thread but here is what I would do in your situation.

Once you add the naptha layer to the lye+water+MHRB mix, give it a hot water bath of at least 1 hour. After I would let the whole mix sit longer than usual, I used to do 48hrs. I would get 400mg per pull, and I got usually two pulls per mix.

Hope this helps.


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Re: dmt extract pissng me off [Re: Xobil3]
    #11927377 - 01/30/10 02:25 AM (3 years, 3 months ago)

I'm using the lazy man's tek for the first time too

I only had 45g of root bark

I have a glass plate with some of that orange goo in front of a fan

should I freeze it? and then what?

any useful links for the freeze/precip will be apreciated

:sun:


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Re: dmt extract pissng me off [Re: oh_you_know]
    #11928015 - 01/30/10 07:02 AM (3 years, 3 months ago)

Quote:

oh_you_know said:
Quote:

highc said:
Quote:

turkeyphant said:
Freeze precip is the way. And then recrystallise.





hell yeah. i freeze percipitated the rest of it. i pulled over 2 grams out today. mmmmmmm. dmt is the shit.



how many grams of MHRB did you use? and what tek?




500 grams. i mostly used lazyman tek except i freeze instead of just evaporate it and i also use a water baking soda wash, followed by a couple plain water washes.

the second pull is in the freezer now. i usually let the solvent sit in the jugs for at least 12 hours. shaking vigurously every 3 or 4. no matter how much you shake it up, the layers will seperate given time.

i puled out altogether now about 2 grams. maybe a little less. so i have a good 5 grams left to get. also im using powder material.


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Re: dmt extract pissng me off [Re: highc]
    #11928433 - 01/30/10 11:03 AM (3 years, 3 months ago)

thanks


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Re: dmt extract pissng me off [Re: highc]
    #11929114 - 01/30/10 01:39 PM (3 years, 3 months ago)

Quote:

highc said:
after a first time failure with dmt i decided to get 500 grams and try again.

150 grams bark was mixed with 625 ml water with about 150 grams lye. it was left to sit a while before adding about 100ml solvent. this mix was left to sit about 24 hours mixing it up twice. the top layer was removed and is fan evaporating as i type. it's evaporating but it only looks to be about not even 50mg spice. what the fuck is goin on around here?




I yielded about a gram, doing a similar extraction as you. Although my bark was finely grounded, and I only mixed for an hour or so.


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Re: dmt extract pissng me off [Re: Neuron]
    #11940272 - 02/01/10 06:33 AM (3 years, 3 months ago)



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Re: dmt extract pissng me off [Re: turkeyphant]
    #11945662 - 02/02/10 01:43 AM (3 years, 3 months ago)

yea that's all good but skip that ammonia shit. bicarbonate all the way.


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Re: dmt extract pissng me off [Re: highc]
    #11945863 - 02/02/10 02:38 AM (3 years, 3 months ago)

was the nap clear or yellow when you pulled it?


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Re: dmt extract pissng me off [Re: Seeker_22]
    #11948998 - 02/02/10 06:41 PM (3 years, 3 months ago)

it varies. if i leave it in their for at least 12 hours it start to turn a light yellow.


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Re: dmt extract pissng me off [Re: highc]
    #11949920 - 02/02/10 08:43 PM (3 years, 3 months ago)

its supposed to be very yellow from my understanding, or else youre doing it wrong


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Re: dmt extract pissng me off [Re: oh_you_know]
    #11951998 - 02/03/10 02:22 AM (3 years, 3 months ago)

NAture boy's got  a good tek.


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Re: dmt extract pissng me off [Re: Neuron]
    #11952076 - 02/03/10 02:40 AM (3 years, 3 months ago)

idk for sure but i have gotten good yields so far. i have one more pull. which would make 3. it has been sitting in the jug now for 3 days. leaving it at least another 1 and pulling it. I'm gonna evaporate it down, freeze it, then collect solvent and evaporate that completely.


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Re: dmt extract pissng me off [Re: highc]
    #11952742 - 02/03/10 08:05 AM (3 years, 3 months ago)

It should definitely be at least a little yellow.


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Re: dmt extract pissng me off [Re: turkeyphant]
    #11953205 - 02/03/10 11:26 AM (3 years, 3 months ago)



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