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Offline04281969
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Easy Three Step Mescaline Citrate
    #7875294 - 01/13/08 07:57 PM (10 months, 16 days ago)

Easy Three-Step Mescaline Citrate


Materials needed:



1) Peruvian torch or San Pedro cactus powder
2) Lye (use gloves and ventilation)
3) Xylene (use gloves and ventilation)
4) Glass gallon jug with lid or stopper
5) Glass funnel
6) Glass jars
7) Citric acid
8) Long dropper pipette
9) Glass turkey baster
10) Measuring cup and teaspoon
11) Square Pyrex dish and fan for evaporation



Step 1 - Extraction: (Base / Non-Polar)



Mix 1-cup (300 grams) lye into 3 quarts cold water, stirring constantly. Pour into jug. Caution HOT!
Add 2/3 cup (100 grams) powdered cactus to the jug. Mix well.
Add ~1 quart xylene to the jug. Shake and roll to mix well.
Mix occasionally over the next 24+ hours as the lye breaks down the cactus.
Allow enough time for separation into layers before proceeding to the next step.



Step 2 - Salt: (Acid / Polar)



Prepare acidic solution by diluting ½ teaspoon (2g) citric acid into ½ cup (120ml) distilled water.
Collect top xylene layer from the jug using the baster, putting the xylene into a new jar.
Add approximately one-fifth of the prepared acidic water to the xylene jar.
Put the lid on the xylene jar and shake it up a few times. Wait a couple minutes to settle.
Collect bottom water layer using a long dropper, putting the water into the evaporation dish.
Return xylene to the cactus solution and mix for another 24 hours.
(Optionally, you can add 1 Tbsp lye to the jug after the third extraction.)
Complete 5 extractions over 5 days to use all of the water.



Step 3 - Evaporation:



Pour liquid into a flat-bottomed glass dish under a fan in a low humidity/mild temp environment. After a few days, scrape the residue from the dish and powder using a razor blade. The powder will continue to dry over the next few days. Makes 3-10 doses depending on potency of cactus and dosage desired.



Edited by 04281969 (03/24/08 01:36 PM)


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Re: Easy Three Step Mescaline Citrate [Re: 04281969]
    #7875410 - 01/13/08 08:10 PM (10 months, 16 days ago)

cool tech but my understanding of it is that mescaline sulfate and hydrochloride are both much more potent than citrat. just thought id throw that outt there


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Offline04281969
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Re: Easy Three Step Mescaline Citrate [Re: awesomebastard]
    #7875444 - 01/13/08 08:15 PM (10 months, 16 days ago)

Since citric acid is food safe, this is the safest recipe to release to the public.
I bet you could choke down another 50 milligrams.


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Re: Easy Three Step Mescaline Citrate [Re: 04281969]
    #7875472 - 01/13/08 08:20 PM (10 months, 16 days ago)

for the salting step, it would probably be easier to freeze that water layer, then pour off the solvent wouldn't it?


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Re: Easy Three Step Mescaline Citrate [Re: enesi]
    #7877138 - 01/14/08 05:58 AM (10 months, 16 days ago)

I suppose, but with long (9") pipetes, you can get it done in 5 minutes instead of 5 hours.

BTW, just because citrate is a larger molecule, don't think you will end up with less mescaline.  You'll just get more product to work with. 


Edited by 04281969 (06/26/08 11:07 AM)


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Re: Easy Three Step Mescaline Citrate [Re: 04281969]
    #7877249 - 01/14/08 07:26 AM (10 months, 16 days ago)

Quote:

04281969 said:
Since citric acid is food safe, this is the safest recipe to release to the public.




This isn't necessarily safer than crystallizing with HCl, its the choice of almost all pharmaceutical companies and they release their product to the public as well. Perhaps procedure-wise it might be safer working with citric acid over HCl because of safety issues/risk of worse chemical burns, but as far as being food safe all of the HCl evaporates out of your final product for the most part.


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Re: Easy Three Step Mescaline Citrate [Re: 04281969]
    #7877262 - 01/14/08 07:31 AM (10 months, 16 days ago)

Quote:

04281969 said:




Oh and nice pic :smile:

Bottom of your pyrex pan,right? Do you have a picture of the scraped up product in a nice little pile? If so, it would be cool if you'd upload it. I haven't seen many pictures of Mescaline Citrate on the web, that would be cool to throw into my photo collection of stuff.


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Re: Easy Three Step Mescaline Citrate [Re: Omni]
    #7877273 - 01/14/08 07:45 AM (10 months, 16 days ago)

I just feel it's safest for people to make at home by themselves.
No chlorine fumes, no sulfuric acid burns, etc.


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Re: Easy Three Step Mescaline Citrate [Re: 04281969]
    #7877277 - 01/14/08 07:47 AM (10 months, 16 days ago)

No doubt :yesnod:


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Re: Easy Three Step Mescaline Citrate [Re: Omni]
    #7877278 - 01/14/08 07:47 AM (10 months, 16 days ago)

Quote:

Omni said:
Quote:

04281969 said:




Oh and nice pic :smile:

Bottom of your pyrex pan,right? Do you have a picture of the scraped up product in a nice little pile? If so, it would be cool if you'd upload it. I haven't seen many pictures of Mescaline Citrate on the web, that would be cool to throw into my photo collection of stuff.



Seconded


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Re: Easy Three Step Mescaline Citrate [Re: 04281969]
    #7877333 - 01/14/08 08:19 AM (10 months, 16 days ago)

Quote:

04281969 said:
I just feel it's safest for people to make at home by themselves.
No chlorine fumes, no sulfuric acid burns, etc.



its a good tech dont get me wrong, with the amount of cactus i have ill propably try it i just thought id throw it out there.
but since the dose is different would you happen to know how much to take?


Edited by awesomebastard (01/14/08 08:20 AM)


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Re: Easy Three Step Mescaline Citrate [Re: awesomebastard]
    #7877433 - 01/14/08 08:58 AM (10 months, 16 days ago)

I don't have a scale, so I've just been winging it. It's a pretty friendly substance, so a little more or less won't send you off the deep end.
Try filling a 00 capsule, and see what that does for you.
Two capsules is a pretty good dose.
I haven't tried three, but it would probably melt the world.


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Re: Easy Three Step Mescaline Citrate [Re: 04281969]
    #7877461 - 01/14/08 09:10 AM (10 months, 16 days ago)

how about that pic :naughty:


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Re: Easy Three Step Mescaline Citrate [Re: Omni]
    #7877472 - 01/14/08 09:15 AM (10 months, 16 days ago)

¿about how much cactus would be 100g?


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Re: Easy Three Step Mescaline Citrate [Re: drSE]
    #7877478 - 01/14/08 09:20 AM (10 months, 16 days ago)

That pic will have to wait until I have some more.
100 grams is a healthy 2/3 cup.


Edited by 04281969 (01/29/08 01:22 PM)


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Re: Easy Three Step Mescaline Citrate [Re: 04281969]
    #7994003 - 02/07/08 09:20 PM (9 months, 22 days ago)

Alright, here's a picture of some more crystals.
I put the mescaline-containing water from each extraction into a small jar overnight and allowed the crystals to precipitate out. I then removed the old water, and added clean water to the crystals and swirled it around to get them out of the jar. I then collected the crystals in the collection dish and evaporated.

Any particular shot that you are looking for?





Edited by 04281969 (03/13/08 07:01 PM)


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Re: Easy Three Step Mescaline Citrate [Re: 04281969]
    #7994008 - 02/07/08 09:21 PM (9 months, 22 days ago)

A shot like this



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Re: Easy Three Step Mescaline Citrate [Re: Omni]
    #7994024 - 02/07/08 09:26 PM (9 months, 22 days ago)

Looks like you have one like that already...
I took one similar to that, but the picture turned out yellow.
Darn digital cameras.


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Re: Easy Three Step Mescaline Citrate [Re: 04281969]
    #7994032 - 02/07/08 09:27 PM (9 months, 22 days ago)

That is Mescaline HCl


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Re: Easy Three Step Mescaline Citrate [Re: Omni]
    #7994038 - 02/07/08 09:30 PM (9 months, 22 days ago)

Ah, well, I'll take a pic in the morning when the light is good.


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